A preliminary study on the synthesis of poly(vinylbenzyl chloride) with different solvents
Polyvinyl benzyl chloride (PVBC) was synthesized by free radical polymerization of 4-vinylbenzyl chloride using benzoyl peroxide initiator at 60 ℃. PVBC was synthesised in different solvents such as toluene, xylene, 1,4-dioxane, and tetrahydrofuran. The polymers were structurally characterized by 1H...
| Main Authors: | , , , , |
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| Format: | Article |
| Language: | English |
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Penerbit Universiti Kebangsaan Malaysia
2021
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| Online Access: | http://journalarticle.ukm.my/17540/1/22.pdf |
| _version_ | 1796932671982534656 |
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| author | Manjusha Elizabeth Mathew, Ishak Ahmad, Sabu Thomas, Mohammad Kassim, Rusli Daik, |
| author_facet | Manjusha Elizabeth Mathew, Ishak Ahmad, Sabu Thomas, Mohammad Kassim, Rusli Daik, |
| author_sort | Manjusha Elizabeth Mathew, |
| collection | UKM |
| description | Polyvinyl benzyl chloride (PVBC) was synthesized by free radical polymerization of 4-vinylbenzyl chloride using benzoyl peroxide initiator at 60 ℃. PVBC was synthesised in different solvents such as toluene, xylene, 1,4-dioxane, and tetrahydrofuran. The polymers were structurally characterized by 1H NMR and FTIR spectroscopic techniques. The thermal property of the polymer was investigated by thermogravimetric analysis (TGA) and differential thermogravimetric analysis (DTA). The number average molecular weight, weight average molecular weight and polydispersity index of PVBC synthesised in different solvents were determined and compared by gel permeation chromatography technique. |
| first_indexed | 2024-03-06T04:36:01Z |
| format | Article |
| id | ukm.eprints-17540 |
| institution | Universiti Kebangsaan Malaysia |
| language | English |
| last_indexed | 2024-03-06T04:36:01Z |
| publishDate | 2021 |
| publisher | Penerbit Universiti Kebangsaan Malaysia |
| record_format | dspace |
| spelling | ukm.eprints-175402021-10-26T06:24:48Z http://journalarticle.ukm.my/17540/ A preliminary study on the synthesis of poly(vinylbenzyl chloride) with different solvents Manjusha Elizabeth Mathew, Ishak Ahmad, Sabu Thomas, Mohammad Kassim, Rusli Daik, Polyvinyl benzyl chloride (PVBC) was synthesized by free radical polymerization of 4-vinylbenzyl chloride using benzoyl peroxide initiator at 60 ℃. PVBC was synthesised in different solvents such as toluene, xylene, 1,4-dioxane, and tetrahydrofuran. The polymers were structurally characterized by 1H NMR and FTIR spectroscopic techniques. The thermal property of the polymer was investigated by thermogravimetric analysis (TGA) and differential thermogravimetric analysis (DTA). The number average molecular weight, weight average molecular weight and polydispersity index of PVBC synthesised in different solvents were determined and compared by gel permeation chromatography technique. Penerbit Universiti Kebangsaan Malaysia 2021-06 Article PeerReviewed application/pdf en http://journalarticle.ukm.my/17540/1/22.pdf Manjusha Elizabeth Mathew, and Ishak Ahmad, and Sabu Thomas, and Mohammad Kassim, and Rusli Daik, (2021) A preliminary study on the synthesis of poly(vinylbenzyl chloride) with different solvents. Sains Malaysiana, 50 (6). pp. 1767-1773. ISSN 0126-6039 https://www.ukm.my/jsm/malay_journals/jilid50bil6_2021/KandunganJilid50Bil6_2021.html |
| spellingShingle | Manjusha Elizabeth Mathew, Ishak Ahmad, Sabu Thomas, Mohammad Kassim, Rusli Daik, A preliminary study on the synthesis of poly(vinylbenzyl chloride) with different solvents |
| title | A preliminary study on the synthesis of poly(vinylbenzyl chloride) with different solvents |
| title_full | A preliminary study on the synthesis of poly(vinylbenzyl chloride) with different solvents |
| title_fullStr | A preliminary study on the synthesis of poly(vinylbenzyl chloride) with different solvents |
| title_full_unstemmed | A preliminary study on the synthesis of poly(vinylbenzyl chloride) with different solvents |
| title_short | A preliminary study on the synthesis of poly(vinylbenzyl chloride) with different solvents |
| title_sort | preliminary study on the synthesis of poly vinylbenzyl chloride with different solvents |
| url | http://journalarticle.ukm.my/17540/1/22.pdf |
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