Fabrication of magnesium-carbonate apatite by conventional sintering and spark plasma sintering for orthopedic implant applications

Magnesium-Carbonate Apatite (Mg-xCA) is one of the potential magnesium composites to be developed as an alternative biodegradable implant material. Several attempts were made to optimize its characteristics. In this study, Mg-xCA (x = 0, 5, 10, and 15% wt) was prepared by powder metallurgy through w...

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Main Authors: Setyadi, Iwan, Sudiro, Toto, Hermanto, Bambang, Oktari, Prima Rizky, Kamal, Achmad Fauzi, Rahyussalim, Ahmad Jabir, Suharno, Bambang, Supriadi, Sugeng
Format: Article
Language:English
Published: Penerbit Universiti Kebangsaan Malaysia 2022
Online Access:http://journalarticle.ukm.my/19173/1/22.pdf
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author Setyadi, Iwan
Sudiro, Toto
Hermanto, Bambang
Oktari, Prima Rizky
Kamal, Achmad Fauzi
Rahyussalim, Ahmad Jabir
Suharno, Bambang
Supriadi, Sugeng
author_facet Setyadi, Iwan
Sudiro, Toto
Hermanto, Bambang
Oktari, Prima Rizky
Kamal, Achmad Fauzi
Rahyussalim, Ahmad Jabir
Suharno, Bambang
Supriadi, Sugeng
author_sort Setyadi, Iwan
collection UKM
description Magnesium-Carbonate Apatite (Mg-xCA) is one of the potential magnesium composites to be developed as an alternative biodegradable implant material. Several attempts were made to optimize its characteristics. In this study, Mg-xCA (x = 0, 5, 10, and 15% wt) was prepared by powder metallurgy through warm compaction (WC) and further densified by 2 sintering process methods, namely conventional sintering (CS) and spark plasma sintering (SPS). The characterization included density test, XRD test, microstructure test (OM and SEM-EDS-Mapping), microhardness test, and electrochemical test. The SPS process improves the characteristics of Mg-xCA better than the CS process. The SPS process can increase the relative density by about 0.7-2.4%, increase the hardness by about 2-13%, and reduce the corrosion rate by about 32-49% compared to the initial condition before sintering (WC). The SPS structure has a lower oxygen elemental content than the CS structure. The sintered process with SPS is considered effective for the fabrication of Mg-xCA powder-based composites compared to the CS process.
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spelling ukm.eprints-191732022-08-01T04:29:14Z http://journalarticle.ukm.my/19173/ Fabrication of magnesium-carbonate apatite by conventional sintering and spark plasma sintering for orthopedic implant applications Setyadi, Iwan Sudiro, Toto Hermanto, Bambang Oktari, Prima Rizky Kamal, Achmad Fauzi Rahyussalim, Ahmad Jabir Suharno, Bambang Supriadi, Sugeng Magnesium-Carbonate Apatite (Mg-xCA) is one of the potential magnesium composites to be developed as an alternative biodegradable implant material. Several attempts were made to optimize its characteristics. In this study, Mg-xCA (x = 0, 5, 10, and 15% wt) was prepared by powder metallurgy through warm compaction (WC) and further densified by 2 sintering process methods, namely conventional sintering (CS) and spark plasma sintering (SPS). The characterization included density test, XRD test, microstructure test (OM and SEM-EDS-Mapping), microhardness test, and electrochemical test. The SPS process improves the characteristics of Mg-xCA better than the CS process. The SPS process can increase the relative density by about 0.7-2.4%, increase the hardness by about 2-13%, and reduce the corrosion rate by about 32-49% compared to the initial condition before sintering (WC). The SPS structure has a lower oxygen elemental content than the CS structure. The sintered process with SPS is considered effective for the fabrication of Mg-xCA powder-based composites compared to the CS process. Penerbit Universiti Kebangsaan Malaysia 2022-03 Article PeerReviewed application/pdf en http://journalarticle.ukm.my/19173/1/22.pdf Setyadi, Iwan and Sudiro, Toto and Hermanto, Bambang and Oktari, Prima Rizky and Kamal, Achmad Fauzi and Rahyussalim, Ahmad Jabir and Suharno, Bambang and Supriadi, Sugeng (2022) Fabrication of magnesium-carbonate apatite by conventional sintering and spark plasma sintering for orthopedic implant applications. Sains Malaysiana, 51 (3). pp. 883-894. ISSN 0126-6039 https://www.ukm.my/jsm/malay_journals/jilid51bil3_2022/KandunganJilid51Bil3_2022.html
spellingShingle Setyadi, Iwan
Sudiro, Toto
Hermanto, Bambang
Oktari, Prima Rizky
Kamal, Achmad Fauzi
Rahyussalim, Ahmad Jabir
Suharno, Bambang
Supriadi, Sugeng
Fabrication of magnesium-carbonate apatite by conventional sintering and spark plasma sintering for orthopedic implant applications
title Fabrication of magnesium-carbonate apatite by conventional sintering and spark plasma sintering for orthopedic implant applications
title_full Fabrication of magnesium-carbonate apatite by conventional sintering and spark plasma sintering for orthopedic implant applications
title_fullStr Fabrication of magnesium-carbonate apatite by conventional sintering and spark plasma sintering for orthopedic implant applications
title_full_unstemmed Fabrication of magnesium-carbonate apatite by conventional sintering and spark plasma sintering for orthopedic implant applications
title_short Fabrication of magnesium-carbonate apatite by conventional sintering and spark plasma sintering for orthopedic implant applications
title_sort fabrication of magnesium carbonate apatite by conventional sintering and spark plasma sintering for orthopedic implant applications
url http://journalarticle.ukm.my/19173/1/22.pdf
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