Preparation of palm oil methyl esters for alkenyl succinic anhydride production
The fractions of fatty acid methyl esters (FAME) i.e. crude palm oil methyl esters (CPOME), RBD palm olein methyl esters (RBD Palm Olein ME) and used frying oil methyl esters (UFOME) rich in unsaturated fatty esters were used to prepare alkenyl succinic anhydrides (ASA). The fractions were obtained...
| Main Authors: | , , , |
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| Format: | Article |
| Language: | English |
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Universiti Kebangsaan Malaysia
2010
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| Online Access: | http://journalarticle.ukm.my/7411/1/01_Md_Yeaminhossain.pdf |
| _version_ | 1825726023846592512 |
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| author | Nur Azreena Idris, Loh, Soh Kheang Choo, Yuen May Boey, Peng Lim |
| author_facet | Nur Azreena Idris, Loh, Soh Kheang Choo, Yuen May Boey, Peng Lim |
| author_sort | Nur Azreena Idris, |
| collection | UKM |
| description | The fractions of fatty acid methyl esters (FAME) i.e. crude palm oil methyl esters (CPOME), RBD palm olein methyl esters (RBD Palm Olein ME) and used frying oil methyl esters (UFOME) rich in unsaturated fatty esters were used to prepare alkenyl succinic anhydrides (ASA). The fractions were obtained via fractional distillation that separated the unsaturated fatty esters from the saturated fatty esters. The fractions with the highest content of unsaturated fatty esters were reacted with maleic anhydride (MA) for 8 hours at 240oC with the MA/FAME ratio of 1.5. The reaction was conducted without catalyst and solvent. The crude alkenyl succinic anhydride (ASA) obtained was purified by column chromatography. The purified compound was characterised by FTIR. |
| first_indexed | 2024-03-06T04:04:32Z |
| format | Article |
| id | ukm.eprints-7411 |
| institution | Universiti Kebangsaan Malaysia |
| language | English |
| last_indexed | 2024-03-06T04:04:32Z |
| publishDate | 2010 |
| publisher | Universiti Kebangsaan Malaysia |
| record_format | dspace |
| spelling | ukm.eprints-74112016-12-14T06:44:00Z http://journalarticle.ukm.my/7411/ Preparation of palm oil methyl esters for alkenyl succinic anhydride production Nur Azreena Idris, Loh, Soh Kheang Choo, Yuen May Boey, Peng Lim The fractions of fatty acid methyl esters (FAME) i.e. crude palm oil methyl esters (CPOME), RBD palm olein methyl esters (RBD Palm Olein ME) and used frying oil methyl esters (UFOME) rich in unsaturated fatty esters were used to prepare alkenyl succinic anhydrides (ASA). The fractions were obtained via fractional distillation that separated the unsaturated fatty esters from the saturated fatty esters. The fractions with the highest content of unsaturated fatty esters were reacted with maleic anhydride (MA) for 8 hours at 240oC with the MA/FAME ratio of 1.5. The reaction was conducted without catalyst and solvent. The crude alkenyl succinic anhydride (ASA) obtained was purified by column chromatography. The purified compound was characterised by FTIR. Universiti Kebangsaan Malaysia 2010-10 Article PeerReviewed application/pdf en http://journalarticle.ukm.my/7411/1/01_Md_Yeaminhossain.pdf Nur Azreena Idris, and Loh, Soh Kheang and Choo, Yuen May and Boey, Peng Lim (2010) Preparation of palm oil methyl esters for alkenyl succinic anhydride production. Sains Malaysiana, 39 (5). pp. 817-820. ISSN 0126-6039 http://www.ukm.my/jsm/english_journals/vol39num5_2010/contentsVol39num5_2010.html |
| spellingShingle | Nur Azreena Idris, Loh, Soh Kheang Choo, Yuen May Boey, Peng Lim Preparation of palm oil methyl esters for alkenyl succinic anhydride production |
| title | Preparation of palm oil methyl esters for alkenyl succinic anhydride production |
| title_full | Preparation of palm oil methyl esters for alkenyl succinic anhydride production |
| title_fullStr | Preparation of palm oil methyl esters for alkenyl succinic anhydride production |
| title_full_unstemmed | Preparation of palm oil methyl esters for alkenyl succinic anhydride production |
| title_short | Preparation of palm oil methyl esters for alkenyl succinic anhydride production |
| title_sort | preparation of palm oil methyl esters for alkenyl succinic anhydride production |
| url | http://journalarticle.ukm.my/7411/1/01_Md_Yeaminhossain.pdf |
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