Synthesis of titanium dioxide microstructures via sucrose ester microemulsion-mediated hydrothermal method

Titanium dioxide particles were successfully prepared using microemulsion-mediated hydrothermal processing route, with sucrose ester as a stabilising agent. X-ray diffraction patterns revealed that the particles possessed anatase crystal phase. Scanning electron micrographs showed micron-sized spher...

Full description

Bibliographic Details
Main Authors: S.A. Zakarya, A. Kassim, H.N. Lim, N.S. Anwar, N.M. Huang
Format: Article
Language:English
Published: Universiti Kebangsaan Malaysia 2010
Online Access:http://journalarticle.ukm.my/7442/1/26_Ayiesah.pdf
_version_ 1825726033781850112
author S.A. Zakarya,
A. Kassim,
H.N. Lim,
N.S. Anwar,
N.M. Huang,
author_facet S.A. Zakarya,
A. Kassim,
H.N. Lim,
N.S. Anwar,
N.M. Huang,
author_sort S.A. Zakarya,
collection UKM
description Titanium dioxide particles were successfully prepared using microemulsion-mediated hydrothermal processing route, with sucrose ester as a stabilising agent. X-ray diffraction patterns revealed that the particles possessed anatase crystal phase. Scanning electron micrographs showed micron-sized spherical particles with rough and smooth surfaces, which eventually interconnected with one another. The formation mechanism of the titanium dioxide microstructures was postulated. The as-prepared particles were subjected to photocatalytic degradation of methylene blue, which exhibited higher photocatalytic activity compared to their commercial counterpart.
first_indexed 2024-03-06T04:04:41Z
format Article
id ukm.eprints-7442
institution Universiti Kebangsaan Malaysia
language English
last_indexed 2024-03-06T04:04:41Z
publishDate 2010
publisher Universiti Kebangsaan Malaysia
record_format dspace
spelling ukm.eprints-74422016-12-14T06:44:06Z http://journalarticle.ukm.my/7442/ Synthesis of titanium dioxide microstructures via sucrose ester microemulsion-mediated hydrothermal method S.A. Zakarya, A. Kassim, H.N. Lim, N.S. Anwar, N.M. Huang, Titanium dioxide particles were successfully prepared using microemulsion-mediated hydrothermal processing route, with sucrose ester as a stabilising agent. X-ray diffraction patterns revealed that the particles possessed anatase crystal phase. Scanning electron micrographs showed micron-sized spherical particles with rough and smooth surfaces, which eventually interconnected with one another. The formation mechanism of the titanium dioxide microstructures was postulated. The as-prepared particles were subjected to photocatalytic degradation of methylene blue, which exhibited higher photocatalytic activity compared to their commercial counterpart. Universiti Kebangsaan Malaysia 2010-12 Article PeerReviewed application/pdf en http://journalarticle.ukm.my/7442/1/26_Ayiesah.pdf S.A. Zakarya, and A. Kassim, and H.N. Lim, and N.S. Anwar, and N.M. Huang, (2010) Synthesis of titanium dioxide microstructures via sucrose ester microemulsion-mediated hydrothermal method. Sains Malaysiana, 39 (6). pp. 975-979. ISSN 0126-6039 http://www.ukm.my/jsm/english_journals/vol39num6_2010/contentsVol39num6_2010.html
spellingShingle S.A. Zakarya,
A. Kassim,
H.N. Lim,
N.S. Anwar,
N.M. Huang,
Synthesis of titanium dioxide microstructures via sucrose ester microemulsion-mediated hydrothermal method
title Synthesis of titanium dioxide microstructures via sucrose ester microemulsion-mediated hydrothermal method
title_full Synthesis of titanium dioxide microstructures via sucrose ester microemulsion-mediated hydrothermal method
title_fullStr Synthesis of titanium dioxide microstructures via sucrose ester microemulsion-mediated hydrothermal method
title_full_unstemmed Synthesis of titanium dioxide microstructures via sucrose ester microemulsion-mediated hydrothermal method
title_short Synthesis of titanium dioxide microstructures via sucrose ester microemulsion-mediated hydrothermal method
title_sort synthesis of titanium dioxide microstructures via sucrose ester microemulsion mediated hydrothermal method
url http://journalarticle.ukm.my/7442/1/26_Ayiesah.pdf
work_keys_str_mv AT sazakarya synthesisoftitaniumdioxidemicrostructuresviasucroseestermicroemulsionmediatedhydrothermalmethod
AT akassim synthesisoftitaniumdioxidemicrostructuresviasucroseestermicroemulsionmediatedhydrothermalmethod
AT hnlim synthesisoftitaniumdioxidemicrostructuresviasucroseestermicroemulsionmediatedhydrothermalmethod
AT nsanwar synthesisoftitaniumdioxidemicrostructuresviasucroseestermicroemulsionmediatedhydrothermalmethod
AT nmhuang synthesisoftitaniumdioxidemicrostructuresviasucroseestermicroemulsionmediatedhydrothermalmethod