1-(2,3,4-Trihydroxybenzylidene)-4-ethylthiosemicarbazide
In the title molecule, C(10)H(13)N(3)O(3)S, the thiosemicarbazide =N-NH-C(=S)-NH- fragment is twisted with respect to the aromatic ring [dihedral angle = 20.5 (1)degrees]. A weak N-H center dot center dot center dot S hydrogen bond [3.480 (1) angstrom] links two molecules about a center of inversion...
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| Format: | Article |
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International Union of Crystallography
2010
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| _version_ | 1825720527572959232 |
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| author | Shawish, H.B. Maah, Mohd Jamil Ng, S.W. |
| author_facet | Shawish, H.B. Maah, Mohd Jamil Ng, S.W. |
| author_sort | Shawish, H.B. |
| collection | UM |
| description | In the title molecule, C(10)H(13)N(3)O(3)S, the thiosemicarbazide =N-NH-C(=S)-NH- fragment is twisted with respect to the aromatic ring [dihedral angle = 20.5 (1)degrees]. A weak N-H center dot center dot center dot S hydrogen bond [3.480 (1) angstrom] links two molecules about a center of inversion to generate a ring. The hydroxy groups are engaged in intermolecular hydrogen bonding; the O-H center dot center dot center dot O and O-H center dot center dot center dot S hydrogen bonds generate a layer motif. |
| first_indexed | 2024-03-06T05:36:30Z |
| format | Article |
| id | um.eprints-14462 |
| institution | Universiti Malaya |
| last_indexed | 2024-03-06T05:36:30Z |
| publishDate | 2010 |
| publisher | International Union of Crystallography |
| record_format | dspace |
| spelling | um.eprints-144622019-01-30T09:12:53Z http://eprints.um.edu.my/14462/ 1-(2,3,4-Trihydroxybenzylidene)-4-ethylthiosemicarbazide Shawish, H.B. Maah, Mohd Jamil Ng, S.W. QC Physics In the title molecule, C(10)H(13)N(3)O(3)S, the thiosemicarbazide =N-NH-C(=S)-NH- fragment is twisted with respect to the aromatic ring [dihedral angle = 20.5 (1)degrees]. A weak N-H center dot center dot center dot S hydrogen bond [3.480 (1) angstrom] links two molecules about a center of inversion to generate a ring. The hydroxy groups are engaged in intermolecular hydrogen bonding; the O-H center dot center dot center dot O and O-H center dot center dot center dot S hydrogen bonds generate a layer motif. International Union of Crystallography 2010 Article PeerReviewed Shawish, H.B. and Maah, Mohd Jamil and Ng, S.W. (2010) 1-(2,3,4-Trihydroxybenzylidene)-4-ethylthiosemicarbazide. Acta Crystallographica Section E: Structure Reports Online, 66 (5). O1151-U769. ISSN 1600-5368, |
| spellingShingle | QC Physics Shawish, H.B. Maah, Mohd Jamil Ng, S.W. 1-(2,3,4-Trihydroxybenzylidene)-4-ethylthiosemicarbazide |
| title | 1-(2,3,4-Trihydroxybenzylidene)-4-ethylthiosemicarbazide |
| title_full | 1-(2,3,4-Trihydroxybenzylidene)-4-ethylthiosemicarbazide |
| title_fullStr | 1-(2,3,4-Trihydroxybenzylidene)-4-ethylthiosemicarbazide |
| title_full_unstemmed | 1-(2,3,4-Trihydroxybenzylidene)-4-ethylthiosemicarbazide |
| title_short | 1-(2,3,4-Trihydroxybenzylidene)-4-ethylthiosemicarbazide |
| title_sort | 1 2 3 4 trihydroxybenzylidene 4 ethylthiosemicarbazide |
| topic | QC Physics |
| work_keys_str_mv | AT shawishhb 1234trihydroxybenzylidene4ethylthiosemicarbazide AT maahmohdjamil 1234trihydroxybenzylidene4ethylthiosemicarbazide AT ngsw 1234trihydroxybenzylidene4ethylthiosemicarbazide |