Nanowires Nickel Oxide and Nanospherical Manganese Oxide Synthesized via Low Temperature Hydrothermal Technique for Hydrogen Peroxide Sensor

Binary catalyst nickel oxides (NiO) and manganese oxides (MnO) were prepared individually via hydrothermal route. The catalysts were characterized by scanning electron microscope (SEM), Brunauer-Emmett-Teller (BET) analysis, cyclic voltammetry (CV), and amperometry. Morphology studies revealed physi...

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Main Authors: Ibrahim, S., Charinpanitkul, T., Kobatake, E., Sriyudthsak, M.
Format: Article
Language:English
Published: Hindawi Publishing Corporation 2016
Subjects:
Online Access:http://eprints.um.edu.my/17508/1/IbrahimS_%282016%29.pdf
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author Ibrahim, S.
Charinpanitkul, T.
Kobatake, E.
Sriyudthsak, M.
author_facet Ibrahim, S.
Charinpanitkul, T.
Kobatake, E.
Sriyudthsak, M.
author_sort Ibrahim, S.
collection UM
description Binary catalyst nickel oxides (NiO) and manganese oxides (MnO) were prepared individually via hydrothermal route. The catalysts were characterized by scanning electron microscope (SEM), Brunauer-Emmett-Teller (BET) analysis, cyclic voltammetry (CV), and amperometry. Morphology studies revealed physical structure of nanowires nickel oxide and spherical manganese oxide with estimated length of 0.3–2.3 μm and diameter of 0.2–0.8 μm, respectively. Surface areas obtained for nickel oxide and manganese oxide were 68.9 m2 g−1 and 45.2 m2 g−1, respectively. Cyclic voltammetry exhibits electrochemical responses corresponding to the electrode surfaces. The linear responses of the binary catalyst modified gold electrodes with NiO-MnO were observed in the concentration range from 31.8 μM to 0.5 mM with the detection limit of 62.5 μM.
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spelling um.eprints-175082017-07-14T03:57:34Z http://eprints.um.edu.my/17508/ Nanowires Nickel Oxide and Nanospherical Manganese Oxide Synthesized via Low Temperature Hydrothermal Technique for Hydrogen Peroxide Sensor Ibrahim, S. Charinpanitkul, T. Kobatake, E. Sriyudthsak, M. TA Engineering (General). Civil engineering (General) TJ Mechanical engineering and machinery TK Electrical engineering. Electronics Nuclear engineering TP Chemical technology Binary catalyst nickel oxides (NiO) and manganese oxides (MnO) were prepared individually via hydrothermal route. The catalysts were characterized by scanning electron microscope (SEM), Brunauer-Emmett-Teller (BET) analysis, cyclic voltammetry (CV), and amperometry. Morphology studies revealed physical structure of nanowires nickel oxide and spherical manganese oxide with estimated length of 0.3–2.3 μm and diameter of 0.2–0.8 μm, respectively. Surface areas obtained for nickel oxide and manganese oxide were 68.9 m2 g−1 and 45.2 m2 g−1, respectively. Cyclic voltammetry exhibits electrochemical responses corresponding to the electrode surfaces. The linear responses of the binary catalyst modified gold electrodes with NiO-MnO were observed in the concentration range from 31.8 μM to 0.5 mM with the detection limit of 62.5 μM. Hindawi Publishing Corporation 2016 Article PeerReviewed application/pdf en http://eprints.um.edu.my/17508/1/IbrahimS_%282016%29.pdf Ibrahim, S. and Charinpanitkul, T. and Kobatake, E. and Sriyudthsak, M. (2016) Nanowires Nickel Oxide and Nanospherical Manganese Oxide Synthesized via Low Temperature Hydrothermal Technique for Hydrogen Peroxide Sensor. Journal of Chemistry, 2016. pp. 1-6. ISSN 2090-9063, DOI https://doi.org/10.1155/2016/9138961 <https://doi.org/10.1155/2016/9138961>. http://dx.doi.org/10.1155/2016/9138961 doi:10.1155/2016/9138961
spellingShingle TA Engineering (General). Civil engineering (General)
TJ Mechanical engineering and machinery
TK Electrical engineering. Electronics Nuclear engineering
TP Chemical technology
Ibrahim, S.
Charinpanitkul, T.
Kobatake, E.
Sriyudthsak, M.
Nanowires Nickel Oxide and Nanospherical Manganese Oxide Synthesized via Low Temperature Hydrothermal Technique for Hydrogen Peroxide Sensor
title Nanowires Nickel Oxide and Nanospherical Manganese Oxide Synthesized via Low Temperature Hydrothermal Technique for Hydrogen Peroxide Sensor
title_full Nanowires Nickel Oxide and Nanospherical Manganese Oxide Synthesized via Low Temperature Hydrothermal Technique for Hydrogen Peroxide Sensor
title_fullStr Nanowires Nickel Oxide and Nanospherical Manganese Oxide Synthesized via Low Temperature Hydrothermal Technique for Hydrogen Peroxide Sensor
title_full_unstemmed Nanowires Nickel Oxide and Nanospherical Manganese Oxide Synthesized via Low Temperature Hydrothermal Technique for Hydrogen Peroxide Sensor
title_short Nanowires Nickel Oxide and Nanospherical Manganese Oxide Synthesized via Low Temperature Hydrothermal Technique for Hydrogen Peroxide Sensor
title_sort nanowires nickel oxide and nanospherical manganese oxide synthesized via low temperature hydrothermal technique for hydrogen peroxide sensor
topic TA Engineering (General). Civil engineering (General)
TJ Mechanical engineering and machinery
TK Electrical engineering. Electronics Nuclear engineering
TP Chemical technology
url http://eprints.um.edu.my/17508/1/IbrahimS_%282016%29.pdf
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AT kobatakee nanowiresnickeloxideandnanosphericalmanganeseoxidesynthesizedvialowtemperaturehydrothermaltechniqueforhydrogenperoxidesensor
AT sriyudthsakm nanowiresnickeloxideandnanosphericalmanganeseoxidesynthesizedvialowtemperaturehydrothermaltechniqueforhydrogenperoxidesensor