Synthesis and electrochemical characterization of amorphous manganese-nickel oxide as supercapacitor electrode material
An amorphous composite film consisted of manganese and nickel oxide was synthesized using simple chronopotentiometry method and tested as electrode material for supercapacitor. The composite film was examined using X-ray diffraction, transmission electron microscopy, and electrochemical characteriza...
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| Format: | Article |
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Springer Verlag (Germany)
2018
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| _version_ | 1796961597586931712 |
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| author | Chan, Pei Yi Majid, Siti Rohana |
| author_facet | Chan, Pei Yi Majid, Siti Rohana |
| author_sort | Chan, Pei Yi |
| collection | UM |
| description | An amorphous composite film consisted of manganese and nickel oxide was synthesized using simple chronopotentiometry method and tested as electrode material for supercapacitor. The composite film was examined using X-ray diffraction, transmission electron microscopy, and electrochemical characterizations. The electrochemical characterization was performed using cyclic voltammetry, galvanostatic charge-discharge, and frequency response analyzer by a three-electrode configuration. The prepared composite electrode remained amorphous until 400 °C. The composite film deposited at 13 min and annealed at 300 °C was found to perform the best. It exhibited a good specific capacitance of 670 F g−1 over a potential window of 1 V in 1 M Na2SO4. Annealing temperature higher than 300 °C brought about a rapid decrease in specific capacitance. The composite electrode remained 61% of initial specific capacitance after 1000 cycles. |
| first_indexed | 2024-03-06T05:56:29Z |
| format | Article |
| id | um.eprints-22278 |
| institution | Universiti Malaya |
| last_indexed | 2024-03-06T05:56:29Z |
| publishDate | 2018 |
| publisher | Springer Verlag (Germany) |
| record_format | dspace |
| spelling | um.eprints-222782019-09-06T06:32:26Z http://eprints.um.edu.my/22278/ Synthesis and electrochemical characterization of amorphous manganese-nickel oxide as supercapacitor electrode material Chan, Pei Yi Majid, Siti Rohana Q Science (General) QC Physics An amorphous composite film consisted of manganese and nickel oxide was synthesized using simple chronopotentiometry method and tested as electrode material for supercapacitor. The composite film was examined using X-ray diffraction, transmission electron microscopy, and electrochemical characterizations. The electrochemical characterization was performed using cyclic voltammetry, galvanostatic charge-discharge, and frequency response analyzer by a three-electrode configuration. The prepared composite electrode remained amorphous until 400 °C. The composite film deposited at 13 min and annealed at 300 °C was found to perform the best. It exhibited a good specific capacitance of 670 F g−1 over a potential window of 1 V in 1 M Na2SO4. Annealing temperature higher than 300 °C brought about a rapid decrease in specific capacitance. The composite electrode remained 61% of initial specific capacitance after 1000 cycles. Springer Verlag (Germany) 2018 Article PeerReviewed Chan, Pei Yi and Majid, Siti Rohana (2018) Synthesis and electrochemical characterization of amorphous manganese-nickel oxide as supercapacitor electrode material. Ionics, 24 (2). pp. 539-548. ISSN 0947-7047, DOI https://doi.org/10.1007/s11581-017-2227-2 <https://doi.org/10.1007/s11581-017-2227-2>. https://doi.org/10.1007/s11581-017-2227-2 doi:10.1007/s11581-017-2227-2 |
| spellingShingle | Q Science (General) QC Physics Chan, Pei Yi Majid, Siti Rohana Synthesis and electrochemical characterization of amorphous manganese-nickel oxide as supercapacitor electrode material |
| title | Synthesis and electrochemical characterization of amorphous manganese-nickel oxide as supercapacitor electrode material |
| title_full | Synthesis and electrochemical characterization of amorphous manganese-nickel oxide as supercapacitor electrode material |
| title_fullStr | Synthesis and electrochemical characterization of amorphous manganese-nickel oxide as supercapacitor electrode material |
| title_full_unstemmed | Synthesis and electrochemical characterization of amorphous manganese-nickel oxide as supercapacitor electrode material |
| title_short | Synthesis and electrochemical characterization of amorphous manganese-nickel oxide as supercapacitor electrode material |
| title_sort | synthesis and electrochemical characterization of amorphous manganese nickel oxide as supercapacitor electrode material |
| topic | Q Science (General) QC Physics |
| work_keys_str_mv | AT chanpeiyi synthesisandelectrochemicalcharacterizationofamorphousmanganesenickeloxideassupercapacitorelectrodematerial AT majidsitirohana synthesisandelectrochemicalcharacterizationofamorphousmanganesenickeloxideassupercapacitorelectrodematerial |