Hydrolysis of microcrystalline cellulose isolated from waste seeds of Leucaena leucocephala for glucose production
The waste seeds of Leucaena leucocephala (LLS) used in this study were unused residues obtained after oil and polysaccharides extraction. The microcrystalline cellulose (MCC) was isolated from LLS by acid treatment. MCC produced was, then, further converted to glucose by using sulphuric acid at 121...
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Penerbit UTM Press, Universiti Teknologi Malaysia
2019
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Online Access: | http://eprints.um.edu.my/24162/1/Husin_M_MJFAS_2019.pdf |
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author | Husin, Maryam Rahim, Nurnadiah Ahmad, Mohd Radzi Romli, Ahmad Zafir Ilham, Zul |
author_facet | Husin, Maryam Rahim, Nurnadiah Ahmad, Mohd Radzi Romli, Ahmad Zafir Ilham, Zul |
author_sort | Husin, Maryam |
collection | UM |
description | The waste seeds of Leucaena leucocephala (LLS) used in this study were unused residues obtained after oil and polysaccharides extraction. The microcrystalline cellulose (MCC) was isolated from LLS by acid treatment. MCC produced was, then, further converted to glucose by using sulphuric acid at 121 °C by varying the acid concentration and reaction time. The sugar composition was analyzed by using the phenol-sulfuric acid method and pre-column derivatization HPLC technique. The yield of glucose ranging from 70–85% could be obtained from MCC hydrolyzates, depending on the hydrolysis factors, which corresponding to around 57-75% of the percentage conversion of MCC to glucose.Cellulose isolated from LLS was, therefore, potentially suitable to be utilized in liquid biofuels and other value-added chemicals such as bioethanol, 5-hydroxymethylfurfural(HMF), and levulinic acid. |
first_indexed | 2024-03-06T06:01:58Z |
format | Article |
id | um.eprints-24162 |
institution | Universiti Malaya |
language | English |
last_indexed | 2024-03-06T06:01:58Z |
publishDate | 2019 |
publisher | Penerbit UTM Press, Universiti Teknologi Malaysia |
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spelling | um.eprints-241622020-04-09T04:33:10Z http://eprints.um.edu.my/24162/ Hydrolysis of microcrystalline cellulose isolated from waste seeds of Leucaena leucocephala for glucose production Husin, Maryam Rahim, Nurnadiah Ahmad, Mohd Radzi Romli, Ahmad Zafir Ilham, Zul Q Science (General) QK Botany T Technology (General) TD Environmental technology. Sanitary engineering TP Chemical technology The waste seeds of Leucaena leucocephala (LLS) used in this study were unused residues obtained after oil and polysaccharides extraction. The microcrystalline cellulose (MCC) was isolated from LLS by acid treatment. MCC produced was, then, further converted to glucose by using sulphuric acid at 121 °C by varying the acid concentration and reaction time. The sugar composition was analyzed by using the phenol-sulfuric acid method and pre-column derivatization HPLC technique. The yield of glucose ranging from 70–85% could be obtained from MCC hydrolyzates, depending on the hydrolysis factors, which corresponding to around 57-75% of the percentage conversion of MCC to glucose.Cellulose isolated from LLS was, therefore, potentially suitable to be utilized in liquid biofuels and other value-added chemicals such as bioethanol, 5-hydroxymethylfurfural(HMF), and levulinic acid. Penerbit UTM Press, Universiti Teknologi Malaysia 2019 Article PeerReviewed text en http://eprints.um.edu.my/24162/1/Husin_M_MJFAS_2019.pdf Husin, Maryam and Rahim, Nurnadiah and Ahmad, Mohd Radzi and Romli, Ahmad Zafir and Ilham, Zul (2019) Hydrolysis of microcrystalline cellulose isolated from waste seeds of Leucaena leucocephala for glucose production. Malaysian Journal of Fundamental and Applied Sciences, 15 (2). pp. 200-205. ISSN 2289-5981, DOI https://doi.org/10.11113/mjfas.v15n2.1165 <https://doi.org/10.11113/mjfas.v15n2.1165>. https://doi.org/10.11113/mjfas.v15n2.1165 doi:10.11113/mjfas.v15n2.1165 |
spellingShingle | Q Science (General) QK Botany T Technology (General) TD Environmental technology. Sanitary engineering TP Chemical technology Husin, Maryam Rahim, Nurnadiah Ahmad, Mohd Radzi Romli, Ahmad Zafir Ilham, Zul Hydrolysis of microcrystalline cellulose isolated from waste seeds of Leucaena leucocephala for glucose production |
title | Hydrolysis of microcrystalline cellulose isolated from waste seeds of Leucaena leucocephala for glucose production |
title_full | Hydrolysis of microcrystalline cellulose isolated from waste seeds of Leucaena leucocephala for glucose production |
title_fullStr | Hydrolysis of microcrystalline cellulose isolated from waste seeds of Leucaena leucocephala for glucose production |
title_full_unstemmed | Hydrolysis of microcrystalline cellulose isolated from waste seeds of Leucaena leucocephala for glucose production |
title_short | Hydrolysis of microcrystalline cellulose isolated from waste seeds of Leucaena leucocephala for glucose production |
title_sort | hydrolysis of microcrystalline cellulose isolated from waste seeds of leucaena leucocephala for glucose production |
topic | Q Science (General) QK Botany T Technology (General) TD Environmental technology. Sanitary engineering TP Chemical technology |
url | http://eprints.um.edu.my/24162/1/Husin_M_MJFAS_2019.pdf |
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