N-[(9-Ethyl-9H-carbazol-3-yl)methylidene]-3,4-dimethylisoxazol-5-amine

The azomethine double bond in the title Schiff base, C(20)H(19)N(3)O, has an E configuration. The 13-membered carbazolyl fused ring system [r.m.s. deviation = 0.023 (9) A] is nearly coplanar with the five-membered pyrazole ring [r.m.s. deviation = 0.003 (4) A]; the dihedral angle between the two sys...

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Main Authors: Tan, Kong Wai, Ng, S.W., Asiri, A.M., Khan, S.A.
Format: Article
Language:English
Published: International Union of Crystallography 2010
Subjects:
Online Access:http://eprints.um.edu.my/8015/1/Asiri-2010-N-_%289-Ethyl-9H-carba.pdf
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author Tan, Kong Wai
Ng, S.W.
Asiri, A.M.
Khan, S.A.
author_facet Tan, Kong Wai
Ng, S.W.
Asiri, A.M.
Khan, S.A.
author_sort Tan, Kong Wai
collection UM
description The azomethine double bond in the title Schiff base, C(20)H(19)N(3)O, has an E configuration. The 13-membered carbazolyl fused ring system [r.m.s. deviation = 0.023 (9) A] is nearly coplanar with the five-membered pyrazole ring [r.m.s. deviation = 0.003 (4) A]; the dihedral angle between the two systems is 10.8 (2)degrees. The crystal studied was a non-merohedral twin having a 35% minor component.
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spelling um.eprints-80152019-01-30T08:50:08Z http://eprints.um.edu.my/8015/ N-[(9-Ethyl-9H-carbazol-3-yl)methylidene]-3,4-dimethylisoxazol-5-amine Tan, Kong Wai Ng, S.W. Asiri, A.M. Khan, S.A. QD Chemistry The azomethine double bond in the title Schiff base, C(20)H(19)N(3)O, has an E configuration. The 13-membered carbazolyl fused ring system [r.m.s. deviation = 0.023 (9) A] is nearly coplanar with the five-membered pyrazole ring [r.m.s. deviation = 0.003 (4) A]; the dihedral angle between the two systems is 10.8 (2)degrees. The crystal studied was a non-merohedral twin having a 35% minor component. International Union of Crystallography 2010 Article PeerReviewed application/pdf en http://eprints.um.edu.my/8015/1/Asiri-2010-N-_%289-Ethyl-9H-carba.pdf Tan, Kong Wai and Ng, S.W. and Asiri, A.M. and Khan, S.A. (2010) N-[(9-Ethyl-9H-carbazol-3-yl)methylidene]-3,4-dimethylisoxazol-5-amine. Acta Crystallographica Section E: Structure Reports Online, 66. O2046-U1453. ISSN 1600-5368, DOI https://doi.org/10.1107/s1600536810027686 <https://doi.org/10.1107/s1600536810027686>. http://journals.iucr.org/e/issues/2010/08/00/rk2213/rk2213.pdf 10.1107/s1600536810027686
spellingShingle QD Chemistry
Tan, Kong Wai
Ng, S.W.
Asiri, A.M.
Khan, S.A.
N-[(9-Ethyl-9H-carbazol-3-yl)methylidene]-3,4-dimethylisoxazol-5-amine
title N-[(9-Ethyl-9H-carbazol-3-yl)methylidene]-3,4-dimethylisoxazol-5-amine
title_full N-[(9-Ethyl-9H-carbazol-3-yl)methylidene]-3,4-dimethylisoxazol-5-amine
title_fullStr N-[(9-Ethyl-9H-carbazol-3-yl)methylidene]-3,4-dimethylisoxazol-5-amine
title_full_unstemmed N-[(9-Ethyl-9H-carbazol-3-yl)methylidene]-3,4-dimethylisoxazol-5-amine
title_short N-[(9-Ethyl-9H-carbazol-3-yl)methylidene]-3,4-dimethylisoxazol-5-amine
title_sort n 9 ethyl 9h carbazol 3 yl methylidene 3 4 dimethylisoxazol 5 amine
topic QD Chemistry
url http://eprints.um.edu.my/8015/1/Asiri-2010-N-_%289-Ethyl-9H-carba.pdf
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AT ngsw n9ethyl9hcarbazol3ylmethylidene34dimethylisoxazol5amine
AT asiriam n9ethyl9hcarbazol3ylmethylidene34dimethylisoxazol5amine
AT khansa n9ethyl9hcarbazol3ylmethylidene34dimethylisoxazol5amine