The effect of crystallization time and temperature on Hydrothermal Synthesis of Zeolite Nax from Bongawan Kaolin

Hydrothermally synthesised zeolite NaX was produced by using kaolin procured from Kg. Gading, Bongawan. The kaolin was treated using sodium hexametaphosphate and calcined at 800oC to form metakaolin. Treated kaolin and prepared metakaolin were characterized using X-ray Fluorescence (XRF) and X-ray D...

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Main Authors: Johnson, EB, Jahimin Asik @ Abd. Rashid, Sazmal Effendi Arshad
Format: Article
Language:English
English
Published: 2016
Subjects:
Online Access:https://eprints.ums.edu.my/id/eprint/18739/1/The%20Effect%20Of%20Crystallization%20Time%20And%20Temperature%20On%20Hydrothermal%20Synthesis%20Of%20Zeolite%20Nax%20From%20Bongawan%20Kaolin.pdf
https://eprints.ums.edu.my/id/eprint/18739/7/THE%20EFFECT%20OF%20CRYSTALLIZATION%20TIME%20AND%20TEMPERATURE%20ON.pdf
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author Johnson, EB
Jahimin Asik @ Abd. Rashid
Sazmal Effendi Arshad
author_facet Johnson, EB
Jahimin Asik @ Abd. Rashid
Sazmal Effendi Arshad
author_sort Johnson, EB
collection UMS
description Hydrothermally synthesised zeolite NaX was produced by using kaolin procured from Kg. Gading, Bongawan. The kaolin was treated using sodium hexametaphosphate and calcined at 800oC to form metakaolin. Treated kaolin and prepared metakaolin were characterized using X-ray Fluorescence (XRF) and X-ray Diffraction (XRD). Reaction mixture was obtained by mixing metakaolin, sodium hydroxide and sodium silicate. The reaction mixture underwent aging for 15 hours before they were crystallized at various crystallization times (0 - 48 hours) and temperatures (80 – 130oC). The effect of crystallization time and temperature was studied using SEM and XRD. Optimum time and temperature for the synthesis was found to be 8 hours at 100 oC, respectively.
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spelling ums.eprints-187392020-12-20T03:56:58Z https://eprints.ums.edu.my/id/eprint/18739/ The effect of crystallization time and temperature on Hydrothermal Synthesis of Zeolite Nax from Bongawan Kaolin Johnson, EB Jahimin Asik @ Abd. Rashid Sazmal Effendi Arshad QE Geology Hydrothermally synthesised zeolite NaX was produced by using kaolin procured from Kg. Gading, Bongawan. The kaolin was treated using sodium hexametaphosphate and calcined at 800oC to form metakaolin. Treated kaolin and prepared metakaolin were characterized using X-ray Fluorescence (XRF) and X-ray Diffraction (XRD). Reaction mixture was obtained by mixing metakaolin, sodium hydroxide and sodium silicate. The reaction mixture underwent aging for 15 hours before they were crystallized at various crystallization times (0 - 48 hours) and temperatures (80 – 130oC). The effect of crystallization time and temperature was studied using SEM and XRD. Optimum time and temperature for the synthesis was found to be 8 hours at 100 oC, respectively. 2016 Article PeerReviewed text en https://eprints.ums.edu.my/id/eprint/18739/1/The%20Effect%20Of%20Crystallization%20Time%20And%20Temperature%20On%20Hydrothermal%20Synthesis%20Of%20Zeolite%20Nax%20From%20Bongawan%20Kaolin.pdf text en https://eprints.ums.edu.my/id/eprint/18739/7/THE%20EFFECT%20OF%20CRYSTALLIZATION%20TIME%20AND%20TEMPERATURE%20ON.pdf Johnson, EB and Jahimin Asik @ Abd. Rashid and Sazmal Effendi Arshad (2016) The effect of crystallization time and temperature on Hydrothermal Synthesis of Zeolite Nax from Bongawan Kaolin. FEIIC International Journal of Engineering and Technology (FIJET)., 13 (1). pp. 33-39.
spellingShingle QE Geology
Johnson, EB
Jahimin Asik @ Abd. Rashid
Sazmal Effendi Arshad
The effect of crystallization time and temperature on Hydrothermal Synthesis of Zeolite Nax from Bongawan Kaolin
title The effect of crystallization time and temperature on Hydrothermal Synthesis of Zeolite Nax from Bongawan Kaolin
title_full The effect of crystallization time and temperature on Hydrothermal Synthesis of Zeolite Nax from Bongawan Kaolin
title_fullStr The effect of crystallization time and temperature on Hydrothermal Synthesis of Zeolite Nax from Bongawan Kaolin
title_full_unstemmed The effect of crystallization time and temperature on Hydrothermal Synthesis of Zeolite Nax from Bongawan Kaolin
title_short The effect of crystallization time and temperature on Hydrothermal Synthesis of Zeolite Nax from Bongawan Kaolin
title_sort effect of crystallization time and temperature on hydrothermal synthesis of zeolite nax from bongawan kaolin
topic QE Geology
url https://eprints.ums.edu.my/id/eprint/18739/1/The%20Effect%20Of%20Crystallization%20Time%20And%20Temperature%20On%20Hydrothermal%20Synthesis%20Of%20Zeolite%20Nax%20From%20Bongawan%20Kaolin.pdf
https://eprints.ums.edu.my/id/eprint/18739/7/THE%20EFFECT%20OF%20CRYSTALLIZATION%20TIME%20AND%20TEMPERATURE%20ON.pdf
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