Synthesis of chloro-substituted liquid crystal containing Azobenzene moieties
The synthesis of chloro -substituted liquid crystal containing azobenzene moieties was carried out by coupling reaction and Williamson ether synthesis. The (4-(3-chloro-4- acetylphenylazo)phenoxy) alkane were orange in colour which indicated the presence of azo group. For characterization techniq...
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Format: | Academic Exercise |
Language: | English |
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2008
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Online Access: | https://eprints.ums.edu.my/id/eprint/20471/1/Synthesis%20of%20chloro-substituted%20liquid.pdf |
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author | Sylvester Julius |
author_facet | Sylvester Julius |
author_sort | Sylvester Julius |
collection | UMS |
description | The synthesis of chloro -substituted liquid crystal containing azobenzene moieties was
carried out by coupling reaction and Williamson ether synthesis. The (4-(3-chloro-4-
acetylphenylazo)phenoxy) alkane were orange in colour which indicated the presence of
azo group. For characterization techniques of synthesized liquid crystal, differential
scanning calorimetry (DSC) was used to investigate the mesomorphic properties and its is
found that the (4-(3-chloro-4acetylphenylazo)phenoxy) hexane and (4-(3-chloro-4-
acetylphenylazo)phenoxy) decane to have mesophase. The structural investigation was
done by Fourier Transform Infrared (FT-IR) in KBr pellets and nuclear magnetic
resonance (NMR) with CDCl₃ as a solvent. Results show that the synthesized liquid
crystals have the functional group and the structure as expected |
first_indexed | 2024-03-06T02:57:51Z |
format | Academic Exercise |
id | ums.eprints-20471 |
institution | Universiti Malaysia Sabah |
language | English |
last_indexed | 2024-03-06T02:57:51Z |
publishDate | 2008 |
record_format | dspace |
spelling | ums.eprints-204712018-07-12T06:39:01Z https://eprints.ums.edu.my/id/eprint/20471/ Synthesis of chloro-substituted liquid crystal containing Azobenzene moieties Sylvester Julius QD Chemistry The synthesis of chloro -substituted liquid crystal containing azobenzene moieties was carried out by coupling reaction and Williamson ether synthesis. The (4-(3-chloro-4- acetylphenylazo)phenoxy) alkane were orange in colour which indicated the presence of azo group. For characterization techniques of synthesized liquid crystal, differential scanning calorimetry (DSC) was used to investigate the mesomorphic properties and its is found that the (4-(3-chloro-4acetylphenylazo)phenoxy) hexane and (4-(3-chloro-4- acetylphenylazo)phenoxy) decane to have mesophase. The structural investigation was done by Fourier Transform Infrared (FT-IR) in KBr pellets and nuclear magnetic resonance (NMR) with CDCl₃ as a solvent. Results show that the synthesized liquid crystals have the functional group and the structure as expected 2008 Academic Exercise NonPeerReviewed text en https://eprints.ums.edu.my/id/eprint/20471/1/Synthesis%20of%20chloro-substituted%20liquid.pdf Sylvester Julius (2008) Synthesis of chloro-substituted liquid crystal containing Azobenzene moieties. Universiti Malaysia Sabah. (Unpublished) |
spellingShingle | QD Chemistry Sylvester Julius Synthesis of chloro-substituted liquid crystal containing Azobenzene moieties |
title | Synthesis of chloro-substituted liquid crystal containing Azobenzene moieties |
title_full | Synthesis of chloro-substituted liquid crystal containing Azobenzene moieties |
title_fullStr | Synthesis of chloro-substituted liquid crystal containing Azobenzene moieties |
title_full_unstemmed | Synthesis of chloro-substituted liquid crystal containing Azobenzene moieties |
title_short | Synthesis of chloro-substituted liquid crystal containing Azobenzene moieties |
title_sort | synthesis of chloro substituted liquid crystal containing azobenzene moieties |
topic | QD Chemistry |
url | https://eprints.ums.edu.my/id/eprint/20471/1/Synthesis%20of%20chloro-substituted%20liquid.pdf |
work_keys_str_mv | AT sylvesterjulius synthesisofchlorosubstitutedliquidcrystalcontainingazobenzenemoieties |