Synthesis and chemical interpretation of 4-((4-nonylphenyl) diazenyl) aniline and 4-((4-decylphenyl) diazenyl) aniline
4-((4-nonylphenyl)diazenyl)aniline and 4-(4-decylphenyl)diazenyl)aniline are an azo compounds with different terminal chains. The synthesis process was started via diazotization of 4- nitroaniline with phenol formed 4-(4-nitrophenyl)phenol (1). After that, 4-(4-nitrophenyl)phenol was alkylated with...
| Main Authors: | , , |
|---|---|
| Format: | Proceedings |
| Language: | English English |
| Published: |
Faculty of Science and Natural Resources
2021
|
| Subjects: | |
| Online Access: | https://eprints.ums.edu.my/id/eprint/32126/1/Synthesis%20and%20chemical%20interpretation%20of%204-%28%284-nonylphenyl%29%20diazenyl%29%20aniline%20and%204-%28%284-decylphenyl%29%20diazenyl%29%20aniline.ABSTRCT.pdf https://eprints.ums.edu.my/id/eprint/32126/2/SYNTHESIS%20AND%20CHEMICAL%20INTERPRETATION%20OF%204-%28%284-%20NONYLPHENYL%29%20DIAZENYL%29%20ANILINE%20AND%204-%28%284-DECYLPHENYL%29%20DIAZENYL%29%20ANILINE.pdf |
| _version_ | 1796911163759394816 |
|---|---|
| author | S. Habil Zuhair Jamain Mohamad Zul Hilmey Makmud |
| author_facet | S. Habil Zuhair Jamain Mohamad Zul Hilmey Makmud |
| author_sort | S. Habil |
| collection | UMS |
| description | 4-((4-nonylphenyl)diazenyl)aniline and 4-(4-decylphenyl)diazenyl)aniline are an azo compounds with different terminal chains. The synthesis process was started via diazotization of 4- nitroaniline with phenol formed 4-(4-nitrophenyl)phenol (1). After that, 4-(4-nitrophenyl)phenol was alkylated with 1-bromononane and 1-bromodecane to yield 1-(4-nitrophenyl)-2-(4-nonylphenyl)diazene (2) and 1-(4-decylphenyl)-2-(4-nitrophenyl)diazene (3), respectively. Finally, both molecules will undergo reduction to yield 4-((4-nonylphenyl)diazenyl)aniline (4) and 4-(4-decylphenyl)diazenyl)aniline (5), respectively. These two compounds were submitted to extensive spectroscopic examination, including Fourier Transform-Infrared (FT-IR) and Nuclear Magnetic Resonance (NMR). |
| first_indexed | 2024-03-06T03:14:47Z |
| format | Proceedings |
| id | ums.eprints-32126 |
| institution | Universiti Malaysia Sabah |
| language | English English |
| last_indexed | 2024-03-06T03:14:47Z |
| publishDate | 2021 |
| publisher | Faculty of Science and Natural Resources |
| record_format | dspace |
| spelling | ums.eprints-321262022-03-31T06:04:29Z https://eprints.ums.edu.my/id/eprint/32126/ Synthesis and chemical interpretation of 4-((4-nonylphenyl) diazenyl) aniline and 4-((4-decylphenyl) diazenyl) aniline S. Habil Zuhair Jamain Mohamad Zul Hilmey Makmud QD1-999 Chemistry 4-((4-nonylphenyl)diazenyl)aniline and 4-(4-decylphenyl)diazenyl)aniline are an azo compounds with different terminal chains. The synthesis process was started via diazotization of 4- nitroaniline with phenol formed 4-(4-nitrophenyl)phenol (1). After that, 4-(4-nitrophenyl)phenol was alkylated with 1-bromononane and 1-bromodecane to yield 1-(4-nitrophenyl)-2-(4-nonylphenyl)diazene (2) and 1-(4-decylphenyl)-2-(4-nitrophenyl)diazene (3), respectively. Finally, both molecules will undergo reduction to yield 4-((4-nonylphenyl)diazenyl)aniline (4) and 4-(4-decylphenyl)diazenyl)aniline (5), respectively. These two compounds were submitted to extensive spectroscopic examination, including Fourier Transform-Infrared (FT-IR) and Nuclear Magnetic Resonance (NMR). Faculty of Science and Natural Resources 2021-10 Proceedings PeerReviewed text en https://eprints.ums.edu.my/id/eprint/32126/1/Synthesis%20and%20chemical%20interpretation%20of%204-%28%284-nonylphenyl%29%20diazenyl%29%20aniline%20and%204-%28%284-decylphenyl%29%20diazenyl%29%20aniline.ABSTRCT.pdf text en https://eprints.ums.edu.my/id/eprint/32126/2/SYNTHESIS%20AND%20CHEMICAL%20INTERPRETATION%20OF%204-%28%284-%20NONYLPHENYL%29%20DIAZENYL%29%20ANILINE%20AND%204-%28%284-DECYLPHENYL%29%20DIAZENYL%29%20ANILINE.pdf S. Habil and Zuhair Jamain and Mohamad Zul Hilmey Makmud (2021) Synthesis and chemical interpretation of 4-((4-nonylphenyl) diazenyl) aniline and 4-((4-decylphenyl) diazenyl) aniline. https://drive.google977-2-73-522200-2.com/file/d/1zKEpSiYvg9vZHHzuKra49512D_AMLubu/view |
| spellingShingle | QD1-999 Chemistry S. Habil Zuhair Jamain Mohamad Zul Hilmey Makmud Synthesis and chemical interpretation of 4-((4-nonylphenyl) diazenyl) aniline and 4-((4-decylphenyl) diazenyl) aniline |
| title | Synthesis and chemical interpretation of 4-((4-nonylphenyl) diazenyl) aniline and 4-((4-decylphenyl) diazenyl) aniline |
| title_full | Synthesis and chemical interpretation of 4-((4-nonylphenyl) diazenyl) aniline and 4-((4-decylphenyl) diazenyl) aniline |
| title_fullStr | Synthesis and chemical interpretation of 4-((4-nonylphenyl) diazenyl) aniline and 4-((4-decylphenyl) diazenyl) aniline |
| title_full_unstemmed | Synthesis and chemical interpretation of 4-((4-nonylphenyl) diazenyl) aniline and 4-((4-decylphenyl) diazenyl) aniline |
| title_short | Synthesis and chemical interpretation of 4-((4-nonylphenyl) diazenyl) aniline and 4-((4-decylphenyl) diazenyl) aniline |
| title_sort | synthesis and chemical interpretation of 4 4 nonylphenyl diazenyl aniline and 4 4 decylphenyl diazenyl aniline |
| topic | QD1-999 Chemistry |
| url | https://eprints.ums.edu.my/id/eprint/32126/1/Synthesis%20and%20chemical%20interpretation%20of%204-%28%284-nonylphenyl%29%20diazenyl%29%20aniline%20and%204-%28%284-decylphenyl%29%20diazenyl%29%20aniline.ABSTRCT.pdf https://eprints.ums.edu.my/id/eprint/32126/2/SYNTHESIS%20AND%20CHEMICAL%20INTERPRETATION%20OF%204-%28%284-%20NONYLPHENYL%29%20DIAZENYL%29%20ANILINE%20AND%204-%28%284-DECYLPHENYL%29%20DIAZENYL%29%20ANILINE.pdf |
| work_keys_str_mv | AT shabil synthesisandchemicalinterpretationof44nonylphenyldiazenylanilineand44decylphenyldiazenylaniline AT zuhairjamain synthesisandchemicalinterpretationof44nonylphenyldiazenylanilineand44decylphenyldiazenylaniline AT mohamadzulhilmeymakmud synthesisandchemicalinterpretationof44nonylphenyldiazenylanilineand44decylphenyldiazenylaniline |