Commercial silicate glass-ceramics: characterization by xrd And tem on crystallization

Crystallization in commercial spodumene glass-ceramic, Corningware® and commercial fluosilicate glass-ceramic, Macor® were characterized by comparing with the quench studies of in-house melted glasses using XRD and advanced microscopy techniques (TEM). XRD, Energy Dispersive X-Ray Analysis (EDAX) an...

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Main Authors: Sazmal E. Arshad, William E. Lee, Peter F. James
Format: Article
Language:English
English
Published: Borneo Science 2011
Subjects:
Online Access:https://eprints.ums.edu.my/id/eprint/36071/1/ABSTRACT.pdf
https://eprints.ums.edu.my/id/eprint/36071/2/FULL%20TEXT.pdf
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author Sazmal E. Arshad
William E. Lee
Peter F. James
author_facet Sazmal E. Arshad
William E. Lee
Peter F. James
author_sort Sazmal E. Arshad
collection UMS
description Crystallization in commercial spodumene glass-ceramic, Corningware® and commercial fluosilicate glass-ceramic, Macor® were characterized by comparing with the quench studies of in-house melted glasses using XRD and advanced microscopy techniques (TEM). XRD, Energy Dispersive X-Ray Analysis (EDAX) and Selected Area Diffraction Pattern (SADP) by TEM confirmed the crystallization of the β-spodumene s.s. with minor needle-like rutile and also precipitation of cuboidal spinel in in-house spodumene glass-ceramics. The techniques were also used in confirming crystallization in the in-house fluosilicate glassceramics where different microstructure based on the early-formed fluorophlogopite crystals were observed with minor cuboidal mullite present as compared to the commercial fluosilicate glass-ceramics.
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spelling ums.eprints-360712023-07-20T01:02:24Z https://eprints.ums.edu.my/id/eprint/36071/ Commercial silicate glass-ceramics: characterization by xrd And tem on crystallization Sazmal E. Arshad William E. Lee Peter F. James TN1-997 Mining engineering. Metallurgy TP785-869 Clay industries. Ceramics. Glass Crystallization in commercial spodumene glass-ceramic, Corningware® and commercial fluosilicate glass-ceramic, Macor® were characterized by comparing with the quench studies of in-house melted glasses using XRD and advanced microscopy techniques (TEM). XRD, Energy Dispersive X-Ray Analysis (EDAX) and Selected Area Diffraction Pattern (SADP) by TEM confirmed the crystallization of the β-spodumene s.s. with minor needle-like rutile and also precipitation of cuboidal spinel in in-house spodumene glass-ceramics. The techniques were also used in confirming crystallization in the in-house fluosilicate glassceramics where different microstructure based on the early-formed fluorophlogopite crystals were observed with minor cuboidal mullite present as compared to the commercial fluosilicate glass-ceramics. Borneo Science 2011 Article NonPeerReviewed text en https://eprints.ums.edu.my/id/eprint/36071/1/ABSTRACT.pdf text en https://eprints.ums.edu.my/id/eprint/36071/2/FULL%20TEXT.pdf Sazmal E. Arshad and William E. Lee and Peter F. James (2011) Commercial silicate glass-ceramics: characterization by xrd And tem on crystallization. The journal of science & technology, 29. pp. 1-13.
spellingShingle TN1-997 Mining engineering. Metallurgy
TP785-869 Clay industries. Ceramics. Glass
Sazmal E. Arshad
William E. Lee
Peter F. James
Commercial silicate glass-ceramics: characterization by xrd And tem on crystallization
title Commercial silicate glass-ceramics: characterization by xrd And tem on crystallization
title_full Commercial silicate glass-ceramics: characterization by xrd And tem on crystallization
title_fullStr Commercial silicate glass-ceramics: characterization by xrd And tem on crystallization
title_full_unstemmed Commercial silicate glass-ceramics: characterization by xrd And tem on crystallization
title_short Commercial silicate glass-ceramics: characterization by xrd And tem on crystallization
title_sort commercial silicate glass ceramics characterization by xrd and tem on crystallization
topic TN1-997 Mining engineering. Metallurgy
TP785-869 Clay industries. Ceramics. Glass
url https://eprints.ums.edu.my/id/eprint/36071/1/ABSTRACT.pdf
https://eprints.ums.edu.my/id/eprint/36071/2/FULL%20TEXT.pdf
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