Borotellurite bio-silica glasses doped by erbium nanoparticles: structural and thermal properties

[(TeO2)0.8 (B2O3)0.2]0.8 (SiO2)0.2}0.99 (Ag2O)0.01]1-y - (Er2O3 NPs)y, and y=0.01,0.02,0.03,0.04 and 0.05 mole% were fabricated by the melt quenching technique. X-ray diffraction (XRD) was used to verify and confirm the glasses’ non-crystallinity. X-ray fluorescence (XRF) proved the achievement of s...

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主要な著者: Muhammad Hamza, Abdulkarim, Aliyu, Umar Sa’ad, Mohamed Kamari, Halimah, Geidam, Ibrahim Gana, El-Mallawany, Raouf, Nazrin, Nazrin, Baba, Muhammad Nasirudeen
フォーマット: 論文
出版事項: Springer 2022
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author Muhammad Hamza, Abdulkarim
Aliyu, Umar Sa’ad
Mohamed Kamari, Halimah
Geidam, Ibrahim Gana
El-Mallawany, Raouf
Nazrin, Nazrin
Baba, Muhammad Nasirudeen
author_facet Muhammad Hamza, Abdulkarim
Aliyu, Umar Sa’ad
Mohamed Kamari, Halimah
Geidam, Ibrahim Gana
El-Mallawany, Raouf
Nazrin, Nazrin
Baba, Muhammad Nasirudeen
author_sort Muhammad Hamza, Abdulkarim
collection UPM
description [(TeO2)0.8 (B2O3)0.2]0.8 (SiO2)0.2}0.99 (Ag2O)0.01]1-y - (Er2O3 NPs)y, and y=0.01,0.02,0.03,0.04 and 0.05 mole% were fabricated by the melt quenching technique. X-ray diffraction (XRD) was used to verify and confirm the glasses’ non-crystallinity. X-ray fluorescence (XRF) proved the achievement of silicate of 98.6% quality from rice husk. Fourier transform infrared d (FTIR) results exposed the basic structural units such as TeO4, TeO3, BO4, BO3, Si-O-Si, and O-Si-O within the network. The concentration of Er2O3 nanoparticles’ effects on the thermal properties of ErDBST glasses was duly discussed. From the profiling of the differential scanning calorimetry (DSC), the glass crystallization temperature Tc, and transition temperature Tg are estimated. Also, the thermal stability factor, defined as Ts = Tc - Tg, was higher than 100 oC. From room temperature above the Tg for all the sample glasses, specific heat capacity Cq (≥1.4 J/gK-1) was obtained. The results showed that the glass thermal stability and the transition temperature increase with the addition of Er2O3 nanoparticles (NPs). These suggest that an ErDBST glass exhibit good thermal stability and consequently is a suitable candidate for fiber drawing.
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spelling upm.eprints-1005632023-10-10T02:11:51Z http://psasir.upm.edu.my/id/eprint/100563/ Borotellurite bio-silica glasses doped by erbium nanoparticles: structural and thermal properties Muhammad Hamza, Abdulkarim Aliyu, Umar Sa’ad Mohamed Kamari, Halimah Geidam, Ibrahim Gana El-Mallawany, Raouf Nazrin, Nazrin Baba, Muhammad Nasirudeen [(TeO2)0.8 (B2O3)0.2]0.8 (SiO2)0.2}0.99 (Ag2O)0.01]1-y - (Er2O3 NPs)y, and y=0.01,0.02,0.03,0.04 and 0.05 mole% were fabricated by the melt quenching technique. X-ray diffraction (XRD) was used to verify and confirm the glasses’ non-crystallinity. X-ray fluorescence (XRF) proved the achievement of silicate of 98.6% quality from rice husk. Fourier transform infrared d (FTIR) results exposed the basic structural units such as TeO4, TeO3, BO4, BO3, Si-O-Si, and O-Si-O within the network. The concentration of Er2O3 nanoparticles’ effects on the thermal properties of ErDBST glasses was duly discussed. From the profiling of the differential scanning calorimetry (DSC), the glass crystallization temperature Tc, and transition temperature Tg are estimated. Also, the thermal stability factor, defined as Ts = Tc - Tg, was higher than 100 oC. From room temperature above the Tg for all the sample glasses, specific heat capacity Cq (≥1.4 J/gK-1) was obtained. The results showed that the glass thermal stability and the transition temperature increase with the addition of Er2O3 nanoparticles (NPs). These suggest that an ErDBST glass exhibit good thermal stability and consequently is a suitable candidate for fiber drawing. Springer 2022-06 Article PeerReviewed Muhammad Hamza, Abdulkarim and Aliyu, Umar Sa’ad and Mohamed Kamari, Halimah and Geidam, Ibrahim Gana and El-Mallawany, Raouf and Nazrin, Nazrin and Baba, Muhammad Nasirudeen (2022) Borotellurite bio-silica glasses doped by erbium nanoparticles: structural and thermal properties. Journal of Theoretical and Applied Physics (JTAP), 16 (2). art. no. 162220. pp. 1-7. ISSN 2251-7227;ESSN: 2251-7235 https://jtap.srbiau.ac.ir/article_19868.html 10.30495/JTAP.162220
spellingShingle Muhammad Hamza, Abdulkarim
Aliyu, Umar Sa’ad
Mohamed Kamari, Halimah
Geidam, Ibrahim Gana
El-Mallawany, Raouf
Nazrin, Nazrin
Baba, Muhammad Nasirudeen
Borotellurite bio-silica glasses doped by erbium nanoparticles: structural and thermal properties
title Borotellurite bio-silica glasses doped by erbium nanoparticles: structural and thermal properties
title_full Borotellurite bio-silica glasses doped by erbium nanoparticles: structural and thermal properties
title_fullStr Borotellurite bio-silica glasses doped by erbium nanoparticles: structural and thermal properties
title_full_unstemmed Borotellurite bio-silica glasses doped by erbium nanoparticles: structural and thermal properties
title_short Borotellurite bio-silica glasses doped by erbium nanoparticles: structural and thermal properties
title_sort borotellurite bio silica glasses doped by erbium nanoparticles structural and thermal properties
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AT mohamedkamarihalimah borotelluritebiosilicaglassesdopedbyerbiumnanoparticlesstructuralandthermalproperties
AT geidamibrahimgana borotelluritebiosilicaglassesdopedbyerbiumnanoparticlesstructuralandthermalproperties
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