Photocatalytic degradation of methylene blue dye under direct sunlight irradiation using SnO2 nanoparticles

In this work, we report the hydrothermal synthesis, characterization, and photocatalytic activity of SnO2 nanoparticles (NPs) towards methylene blue (MB) dye. The synthesized sample was characterized using X-ray diffraction (XRD), Fourier transform infrared (FTIR), ultraviolet–visible (UV–Vis), scan...

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Main Authors: Sagadevan, Suresh, Anita Lett, J., Alshahateet, Solhe F., Fatimah, Is, Weldegebrieal, Getu Kassegn, Le, Minh-Vien, Leonard, Estelle, Paiman, Suriati, Soga, Tetsuo
Format: Article
Published: Elsevier 2022
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author Sagadevan, Suresh
Anita Lett, J.
Alshahateet, Solhe F.
Fatimah, Is
Weldegebrieal, Getu Kassegn
Le, Minh-Vien
Leonard, Estelle
Paiman, Suriati
Soga, Tetsuo
author_facet Sagadevan, Suresh
Anita Lett, J.
Alshahateet, Solhe F.
Fatimah, Is
Weldegebrieal, Getu Kassegn
Le, Minh-Vien
Leonard, Estelle
Paiman, Suriati
Soga, Tetsuo
author_sort Sagadevan, Suresh
collection UPM
description In this work, we report the hydrothermal synthesis, characterization, and photocatalytic activity of SnO2 nanoparticles (NPs) towards methylene blue (MB) dye. The synthesized sample was characterized using X-ray diffraction (XRD), Fourier transform infrared (FTIR), ultraviolet–visible (UV–Vis), scanning electron microscopy (SEM), transmission electron microscopy (TEM), and N2-sorption isotherm techniques. Results show that synthesized sample was tetragonal structure with an optical bandgap, average crystallite size, and degree of crystallinity equal to 3.67 eV, 21 nm, and 70%, respectively. The impacts of dye initial concentration, catalyst dose, and oxidant addition on the sunlight-assisted photodegradation performance were investigated. Degradation of 97% was achieved in 2 h of irradiation utilizing 10 ppm dye initial concentration and 40 mg catalyst dose at natural pH and in the absence of any oxidant. However, in the presence of the H2O2 oxidant complete removal was observed in just 90 min without changing other parameters.
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spelling upm.eprints-1027502024-06-30T01:26:16Z http://psasir.upm.edu.my/id/eprint/102750/ Photocatalytic degradation of methylene blue dye under direct sunlight irradiation using SnO2 nanoparticles Sagadevan, Suresh Anita Lett, J. Alshahateet, Solhe F. Fatimah, Is Weldegebrieal, Getu Kassegn Le, Minh-Vien Leonard, Estelle Paiman, Suriati Soga, Tetsuo In this work, we report the hydrothermal synthesis, characterization, and photocatalytic activity of SnO2 nanoparticles (NPs) towards methylene blue (MB) dye. The synthesized sample was characterized using X-ray diffraction (XRD), Fourier transform infrared (FTIR), ultraviolet–visible (UV–Vis), scanning electron microscopy (SEM), transmission electron microscopy (TEM), and N2-sorption isotherm techniques. Results show that synthesized sample was tetragonal structure with an optical bandgap, average crystallite size, and degree of crystallinity equal to 3.67 eV, 21 nm, and 70%, respectively. The impacts of dye initial concentration, catalyst dose, and oxidant addition on the sunlight-assisted photodegradation performance were investigated. Degradation of 97% was achieved in 2 h of irradiation utilizing 10 ppm dye initial concentration and 40 mg catalyst dose at natural pH and in the absence of any oxidant. However, in the presence of the H2O2 oxidant complete removal was observed in just 90 min without changing other parameters. Elsevier 2022-07 Article PeerReviewed Sagadevan, Suresh and Anita Lett, J. and Alshahateet, Solhe F. and Fatimah, Is and Weldegebrieal, Getu Kassegn and Le, Minh-Vien and Leonard, Estelle and Paiman, Suriati and Soga, Tetsuo (2022) Photocatalytic degradation of methylene blue dye under direct sunlight irradiation using SnO2 nanoparticles. Inorganic Chemistry Communications, 141. art. no. 109547. pp. 1-10. ISSN 1387-7003; ESSN: 1879-0259 https://linkinghub.elsevier.com/retrieve/pii/S1387700322003550 10.1016/j.inoche.2022.109547
spellingShingle Sagadevan, Suresh
Anita Lett, J.
Alshahateet, Solhe F.
Fatimah, Is
Weldegebrieal, Getu Kassegn
Le, Minh-Vien
Leonard, Estelle
Paiman, Suriati
Soga, Tetsuo
Photocatalytic degradation of methylene blue dye under direct sunlight irradiation using SnO2 nanoparticles
title Photocatalytic degradation of methylene blue dye under direct sunlight irradiation using SnO2 nanoparticles
title_full Photocatalytic degradation of methylene blue dye under direct sunlight irradiation using SnO2 nanoparticles
title_fullStr Photocatalytic degradation of methylene blue dye under direct sunlight irradiation using SnO2 nanoparticles
title_full_unstemmed Photocatalytic degradation of methylene blue dye under direct sunlight irradiation using SnO2 nanoparticles
title_short Photocatalytic degradation of methylene blue dye under direct sunlight irradiation using SnO2 nanoparticles
title_sort photocatalytic degradation of methylene blue dye under direct sunlight irradiation using sno2 nanoparticles
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