Photocatalytic degradation of methylene blue dye under direct sunlight irradiation using SnO2 nanoparticles
In this work, we report the hydrothermal synthesis, characterization, and photocatalytic activity of SnO2 nanoparticles (NPs) towards methylene blue (MB) dye. The synthesized sample was characterized using X-ray diffraction (XRD), Fourier transform infrared (FTIR), ultraviolet–visible (UV–Vis), scan...
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Elsevier
2022
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author | Sagadevan, Suresh Anita Lett, J. Alshahateet, Solhe F. Fatimah, Is Weldegebrieal, Getu Kassegn Le, Minh-Vien Leonard, Estelle Paiman, Suriati Soga, Tetsuo |
author_facet | Sagadevan, Suresh Anita Lett, J. Alshahateet, Solhe F. Fatimah, Is Weldegebrieal, Getu Kassegn Le, Minh-Vien Leonard, Estelle Paiman, Suriati Soga, Tetsuo |
author_sort | Sagadevan, Suresh |
collection | UPM |
description | In this work, we report the hydrothermal synthesis, characterization, and photocatalytic activity of SnO2 nanoparticles (NPs) towards methylene blue (MB) dye. The synthesized sample was characterized using X-ray diffraction (XRD), Fourier transform infrared (FTIR), ultraviolet–visible (UV–Vis), scanning electron microscopy (SEM), transmission electron microscopy (TEM), and N2-sorption isotherm techniques. Results show that synthesized sample was tetragonal structure with an optical bandgap, average crystallite size, and degree of crystallinity equal to 3.67 eV, 21 nm, and 70%, respectively. The impacts of dye initial concentration, catalyst dose, and oxidant addition on the sunlight-assisted photodegradation performance were investigated. Degradation of 97% was achieved in 2 h of irradiation utilizing 10 ppm dye initial concentration and 40 mg catalyst dose at natural pH and in the absence of any oxidant. However, in the presence of the H2O2 oxidant complete removal was observed in just 90 min without changing other parameters. |
first_indexed | 2024-09-25T03:37:00Z |
format | Article |
id | upm.eprints-102750 |
institution | Universiti Putra Malaysia |
last_indexed | 2024-09-25T03:37:00Z |
publishDate | 2022 |
publisher | Elsevier |
record_format | dspace |
spelling | upm.eprints-1027502024-06-30T01:26:16Z http://psasir.upm.edu.my/id/eprint/102750/ Photocatalytic degradation of methylene blue dye under direct sunlight irradiation using SnO2 nanoparticles Sagadevan, Suresh Anita Lett, J. Alshahateet, Solhe F. Fatimah, Is Weldegebrieal, Getu Kassegn Le, Minh-Vien Leonard, Estelle Paiman, Suriati Soga, Tetsuo In this work, we report the hydrothermal synthesis, characterization, and photocatalytic activity of SnO2 nanoparticles (NPs) towards methylene blue (MB) dye. The synthesized sample was characterized using X-ray diffraction (XRD), Fourier transform infrared (FTIR), ultraviolet–visible (UV–Vis), scanning electron microscopy (SEM), transmission electron microscopy (TEM), and N2-sorption isotherm techniques. Results show that synthesized sample was tetragonal structure with an optical bandgap, average crystallite size, and degree of crystallinity equal to 3.67 eV, 21 nm, and 70%, respectively. The impacts of dye initial concentration, catalyst dose, and oxidant addition on the sunlight-assisted photodegradation performance were investigated. Degradation of 97% was achieved in 2 h of irradiation utilizing 10 ppm dye initial concentration and 40 mg catalyst dose at natural pH and in the absence of any oxidant. However, in the presence of the H2O2 oxidant complete removal was observed in just 90 min without changing other parameters. Elsevier 2022-07 Article PeerReviewed Sagadevan, Suresh and Anita Lett, J. and Alshahateet, Solhe F. and Fatimah, Is and Weldegebrieal, Getu Kassegn and Le, Minh-Vien and Leonard, Estelle and Paiman, Suriati and Soga, Tetsuo (2022) Photocatalytic degradation of methylene blue dye under direct sunlight irradiation using SnO2 nanoparticles. Inorganic Chemistry Communications, 141. art. no. 109547. pp. 1-10. ISSN 1387-7003; ESSN: 1879-0259 https://linkinghub.elsevier.com/retrieve/pii/S1387700322003550 10.1016/j.inoche.2022.109547 |
spellingShingle | Sagadevan, Suresh Anita Lett, J. Alshahateet, Solhe F. Fatimah, Is Weldegebrieal, Getu Kassegn Le, Minh-Vien Leonard, Estelle Paiman, Suriati Soga, Tetsuo Photocatalytic degradation of methylene blue dye under direct sunlight irradiation using SnO2 nanoparticles |
title | Photocatalytic degradation of methylene blue dye under direct sunlight irradiation using SnO2 nanoparticles |
title_full | Photocatalytic degradation of methylene blue dye under direct sunlight irradiation using SnO2 nanoparticles |
title_fullStr | Photocatalytic degradation of methylene blue dye under direct sunlight irradiation using SnO2 nanoparticles |
title_full_unstemmed | Photocatalytic degradation of methylene blue dye under direct sunlight irradiation using SnO2 nanoparticles |
title_short | Photocatalytic degradation of methylene blue dye under direct sunlight irradiation using SnO2 nanoparticles |
title_sort | photocatalytic degradation of methylene blue dye under direct sunlight irradiation using sno2 nanoparticles |
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