Optimization of supercritical CO2 extraction of fish oil from viscera of African catfish (Clarias gariepinus)

Fish oil was extracted from the viscera of African Catfish using supercritical carbon dioxide (SC-CO2). A Central Composite Design of Response Surface methodology (RSM) was employed to optimize the SC-CO2 extraction parameters. The oil yield (Y) as response variable was executed against the four ind...

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Main Authors: Sarker, Md. Zaidul Islam, Selamat, Jinap, Md. Ahsan Habib, Abu Sayem, Ferdosh, Sahena, Akanda, Mohamed Jahurul Haque, Mohamed Jaffri, Juliana
Format: Article
Language:English
Published: MDPI 2012
Online Access:http://psasir.upm.edu.my/id/eprint/12951/1/ijms-13-11312.pdf
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author Sarker, Md. Zaidul Islam
Selamat, Jinap
Md. Ahsan Habib, Abu Sayem
Ferdosh, Sahena
Akanda, Mohamed Jahurul Haque
Mohamed Jaffri, Juliana
author_facet Sarker, Md. Zaidul Islam
Selamat, Jinap
Md. Ahsan Habib, Abu Sayem
Ferdosh, Sahena
Akanda, Mohamed Jahurul Haque
Mohamed Jaffri, Juliana
author_sort Sarker, Md. Zaidul Islam
collection UPM
description Fish oil was extracted from the viscera of African Catfish using supercritical carbon dioxide (SC-CO2). A Central Composite Design of Response Surface methodology (RSM) was employed to optimize the SC-CO2 extraction parameters. The oil yield (Y) as response variable was executed against the four independent variables, namely pressure, temperature, flow rate and soaking time. The oil yield varied with the linear, quadratic and interaction of pressure, temperature, flow rate and soaking time. Optimum points were observed within the variables of temperature from 35 °C to 80 °C, pressure from 10 MPa to 40 MPa, flow rate from 1 mL/min to 3 mL/min and soaking time from 1 h to 4 h. However, the extraction parameters were found to be optimized at temperature 57.5 °C, pressure 40 MPa, flow rate 2.0 mL/min and soaking time 2.5 h. At this optimized condition, the highest oil yields were found to be 67.0% (g oil/100 g sample on dry basis) in the viscera of catfish which was reasonable to the yields of 78.0% extracted using the Soxhlet method.
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spelling upm.eprints-129512016-02-10T04:09:14Z http://psasir.upm.edu.my/id/eprint/12951/ Optimization of supercritical CO2 extraction of fish oil from viscera of African catfish (Clarias gariepinus) Sarker, Md. Zaidul Islam Selamat, Jinap Md. Ahsan Habib, Abu Sayem Ferdosh, Sahena Akanda, Mohamed Jahurul Haque Mohamed Jaffri, Juliana Fish oil was extracted from the viscera of African Catfish using supercritical carbon dioxide (SC-CO2). A Central Composite Design of Response Surface methodology (RSM) was employed to optimize the SC-CO2 extraction parameters. The oil yield (Y) as response variable was executed against the four independent variables, namely pressure, temperature, flow rate and soaking time. The oil yield varied with the linear, quadratic and interaction of pressure, temperature, flow rate and soaking time. Optimum points were observed within the variables of temperature from 35 °C to 80 °C, pressure from 10 MPa to 40 MPa, flow rate from 1 mL/min to 3 mL/min and soaking time from 1 h to 4 h. However, the extraction parameters were found to be optimized at temperature 57.5 °C, pressure 40 MPa, flow rate 2.0 mL/min and soaking time 2.5 h. At this optimized condition, the highest oil yields were found to be 67.0% (g oil/100 g sample on dry basis) in the viscera of catfish which was reasonable to the yields of 78.0% extracted using the Soxhlet method. MDPI 2012 Article PeerReviewed application/pdf en http://psasir.upm.edu.my/id/eprint/12951/1/ijms-13-11312.pdf Sarker, Md. Zaidul Islam and Selamat, Jinap and Md. Ahsan Habib, Abu Sayem and Ferdosh, Sahena and Akanda, Mohamed Jahurul Haque and Mohamed Jaffri, Juliana (2012) Optimization of supercritical CO2 extraction of fish oil from viscera of African catfish (Clarias gariepinus). International Journal of Molecular Sciences, 13 (9). pp. 11312-11322. ISSN 1661-6596; ESSN: 1422-0067 http://www.mdpi.com/1422-0067/13/9/11312 10.3390/ijms130911312
spellingShingle Sarker, Md. Zaidul Islam
Selamat, Jinap
Md. Ahsan Habib, Abu Sayem
Ferdosh, Sahena
Akanda, Mohamed Jahurul Haque
Mohamed Jaffri, Juliana
Optimization of supercritical CO2 extraction of fish oil from viscera of African catfish (Clarias gariepinus)
title Optimization of supercritical CO2 extraction of fish oil from viscera of African catfish (Clarias gariepinus)
title_full Optimization of supercritical CO2 extraction of fish oil from viscera of African catfish (Clarias gariepinus)
title_fullStr Optimization of supercritical CO2 extraction of fish oil from viscera of African catfish (Clarias gariepinus)
title_full_unstemmed Optimization of supercritical CO2 extraction of fish oil from viscera of African catfish (Clarias gariepinus)
title_short Optimization of supercritical CO2 extraction of fish oil from viscera of African catfish (Clarias gariepinus)
title_sort optimization of supercritical co2 extraction of fish oil from viscera of african catfish clarias gariepinus
url http://psasir.upm.edu.my/id/eprint/12951/1/ijms-13-11312.pdf
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