Effect of ultrasonic pre-treatment on low temperature acid hydrolysis of oil palm empty fruit bunch

Various pre-treatment techniques change the physical and chemical structure of the lignocellulosic biomass and improve hydrolysis rates. The effect of ultrasonic pre-treatment on oil palm empty fruit bunch (OPEFB) fibre prior to acid hydrolysis has been evaluated. The main objective of this study wa...

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Main Authors: Yunus, Robiah, Salleh, Shanti Faridah, Abdullah, Norhafizah, Awang Biak, Dayang Radiah
Format: Article
Language:English
Published: Elsevier 2010
Online Access:http://psasir.upm.edu.my/id/eprint/14324/1/Effect%20of%20ultrasonic%20pre-treatment%20on%20low%20temperature%20acid%20hydrolysis%20of%20oil%20palm%20empty%20fruit%20bunch.pdf
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author Yunus, Robiah
Salleh, Shanti Faridah
Abdullah, Norhafizah
Awang Biak, Dayang Radiah
author_facet Yunus, Robiah
Salleh, Shanti Faridah
Abdullah, Norhafizah
Awang Biak, Dayang Radiah
author_sort Yunus, Robiah
collection UPM
description Various pre-treatment techniques change the physical and chemical structure of the lignocellulosic biomass and improve hydrolysis rates. The effect of ultrasonic pre-treatment on oil palm empty fruit bunch (OPEFB) fibre prior to acid hydrolysis has been evaluated. The main objective of this study was to determine if ultrasonic pre-treatment could function as a pre-treatment method for the acid hydrolysis of OPEFB fibre at a low temperature and pressure. Hydrolysis at a low temperature was studied using 2% sulphuric acid; 1:25 solid liquid ratio and 100 °C operating temperature. A maximum xylose yield of 58% was achieved when the OPEFB fibre was ultrasonicated at 90% amplitude for 45 min. In the absence of ultrasonic pre-treatment only 22% of xylose was obtained. However, no substantial increase of xylose formation was observed for acid hydrolysis at higher temperatures of 120 and 140 °C on ultrasonicated OPEFB fibre. The samples were then analysed using a scanning electron microscope (SEM) to describe the morphological changes of the OPEFB fibre. The SEM observations show interesting morphological changes within the OPEFB fibre for different acid hydrolysis conditions.
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spelling upm.eprints-143242019-03-08T06:30:04Z http://psasir.upm.edu.my/id/eprint/14324/ Effect of ultrasonic pre-treatment on low temperature acid hydrolysis of oil palm empty fruit bunch Yunus, Robiah Salleh, Shanti Faridah Abdullah, Norhafizah Awang Biak, Dayang Radiah Various pre-treatment techniques change the physical and chemical structure of the lignocellulosic biomass and improve hydrolysis rates. The effect of ultrasonic pre-treatment on oil palm empty fruit bunch (OPEFB) fibre prior to acid hydrolysis has been evaluated. The main objective of this study was to determine if ultrasonic pre-treatment could function as a pre-treatment method for the acid hydrolysis of OPEFB fibre at a low temperature and pressure. Hydrolysis at a low temperature was studied using 2% sulphuric acid; 1:25 solid liquid ratio and 100 °C operating temperature. A maximum xylose yield of 58% was achieved when the OPEFB fibre was ultrasonicated at 90% amplitude for 45 min. In the absence of ultrasonic pre-treatment only 22% of xylose was obtained. However, no substantial increase of xylose formation was observed for acid hydrolysis at higher temperatures of 120 and 140 °C on ultrasonicated OPEFB fibre. The samples were then analysed using a scanning electron microscope (SEM) to describe the morphological changes of the OPEFB fibre. The SEM observations show interesting morphological changes within the OPEFB fibre for different acid hydrolysis conditions. Elsevier 2010 Article PeerReviewed text en http://psasir.upm.edu.my/id/eprint/14324/1/Effect%20of%20ultrasonic%20pre-treatment%20on%20low%20temperature%20acid%20hydrolysis%20of%20oil%20palm%20empty%20fruit%20bunch.pdf Yunus, Robiah and Salleh, Shanti Faridah and Abdullah, Norhafizah and Awang Biak, Dayang Radiah (2010) Effect of ultrasonic pre-treatment on low temperature acid hydrolysis of oil palm empty fruit bunch. Bioresource Technology, 101 (24). pp. 9792-9796. ISSN 0960-8524; ESSN: 1873-2976 https://www.sciencedirect.com/science/article/pii/S0960852410012642#! 10.1016/j.biortech.2010.07.074
spellingShingle Yunus, Robiah
Salleh, Shanti Faridah
Abdullah, Norhafizah
Awang Biak, Dayang Radiah
Effect of ultrasonic pre-treatment on low temperature acid hydrolysis of oil palm empty fruit bunch
title Effect of ultrasonic pre-treatment on low temperature acid hydrolysis of oil palm empty fruit bunch
title_full Effect of ultrasonic pre-treatment on low temperature acid hydrolysis of oil palm empty fruit bunch
title_fullStr Effect of ultrasonic pre-treatment on low temperature acid hydrolysis of oil palm empty fruit bunch
title_full_unstemmed Effect of ultrasonic pre-treatment on low temperature acid hydrolysis of oil palm empty fruit bunch
title_short Effect of ultrasonic pre-treatment on low temperature acid hydrolysis of oil palm empty fruit bunch
title_sort effect of ultrasonic pre treatment on low temperature acid hydrolysis of oil palm empty fruit bunch
url http://psasir.upm.edu.my/id/eprint/14324/1/Effect%20of%20ultrasonic%20pre-treatment%20on%20low%20temperature%20acid%20hydrolysis%20of%20oil%20palm%20empty%20fruit%20bunch.pdf
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AT abdullahnorhafizah effectofultrasonicpretreatmentonlowtemperatureacidhydrolysisofoilpalmemptyfruitbunch
AT awangbiakdayangradiah effectofultrasonicpretreatmentonlowtemperatureacidhydrolysisofoilpalmemptyfruitbunch