Preparation and characterization of iron sulphide thin films by chemical bath deposition method

FeS2 thin films have been deposited by using low cost chemical bath deposition technique. The films obtained under deposition parameters such as bath temperature (90°C), deposition period (90 min), electrolyte concentration(0.15 M)and pH of the reactive mixture (pH 2.5). The thin films were charact...

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Main Authors: Kassim, Anuar, Tan, Wee Tee, Abdullah, Dzulkefly Kuang, Mohd. Sharif, Atan, Ho, Soon Min, Gwee, Siew Yong, Nagalingam, Saravanan
Format: Article
Language:English
English
Published: The Department of Chemistry, Universitas Gadjah Mada 2010
Subjects:
Online Access:http://psasir.upm.edu.my/id/eprint/16311/1/Preparation%20and%20characterization%20of%20iron%20sulphide%20thin%20films%20by%20chemical%20bath%20deposition%20method.pdf
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author Kassim, Anuar
Tan, Wee Tee
Abdullah, Dzulkefly Kuang
Mohd. Sharif, Atan
Ho, Soon Min
Gwee, Siew Yong
Nagalingam, Saravanan
author_facet Kassim, Anuar
Tan, Wee Tee
Abdullah, Dzulkefly Kuang
Mohd. Sharif, Atan
Ho, Soon Min
Gwee, Siew Yong
Nagalingam, Saravanan
author_sort Kassim, Anuar
collection UPM
description FeS2 thin films have been deposited by using low cost chemical bath deposition technique. The films obtained under deposition parameters such as bath temperature (90°C), deposition period (90 min), electrolyte concentration(0.15 M)and pH of the reactive mixture (pH 2.5). The thin films were characterized using X-ray diffraction and atomic force microscopy in order to study the structural and morphological properties. The band gap energy, transition type and absorption properties were determined using UV-Vis Spectrophotometer. X-ray diffraction displayed a pattern consistent with the formation of an orthorhombic structure, with a strong (110) preferred orientation. Atomic force microscopy image showed the substrate surface is well covered with irregular grains. A direct band gap of 1.85 eV was obtained according to optical absorption studies.
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spelling upm.eprints-163112015-09-27T23:37:29Z http://psasir.upm.edu.my/id/eprint/16311/ Preparation and characterization of iron sulphide thin films by chemical bath deposition method Kassim, Anuar Tan, Wee Tee Abdullah, Dzulkefly Kuang Mohd. Sharif, Atan Ho, Soon Min Gwee, Siew Yong Nagalingam, Saravanan FeS2 thin films have been deposited by using low cost chemical bath deposition technique. The films obtained under deposition parameters such as bath temperature (90°C), deposition period (90 min), electrolyte concentration(0.15 M)and pH of the reactive mixture (pH 2.5). The thin films were characterized using X-ray diffraction and atomic force microscopy in order to study the structural and morphological properties. The band gap energy, transition type and absorption properties were determined using UV-Vis Spectrophotometer. X-ray diffraction displayed a pattern consistent with the formation of an orthorhombic structure, with a strong (110) preferred orientation. Atomic force microscopy image showed the substrate surface is well covered with irregular grains. A direct band gap of 1.85 eV was obtained according to optical absorption studies. The Department of Chemistry, Universitas Gadjah Mada 2010 Article PeerReviewed application/pdf en http://psasir.upm.edu.my/id/eprint/16311/1/Preparation%20and%20characterization%20of%20iron%20sulphide%20thin%20films%20by%20chemical%20bath%20deposition%20method.pdf Kassim, Anuar and Tan, Wee Tee and Abdullah, Dzulkefly Kuang and Mohd. Sharif, Atan and Ho, Soon Min and Gwee, Siew Yong and Nagalingam, Saravanan (2010) Preparation and characterization of iron sulphide thin films by chemical bath deposition method. Indonesian Journal of Chemistry, 10 (1). pp. 8-11. ISSN 1411-9420 http://pdm-mipa.ugm.ac.id/ojs/index.php/ijc/article/viewFile/477/494 Thin films Iron compounds X-rays - Diffraction English
spellingShingle Thin films
Iron compounds
X-rays - Diffraction
Kassim, Anuar
Tan, Wee Tee
Abdullah, Dzulkefly Kuang
Mohd. Sharif, Atan
Ho, Soon Min
Gwee, Siew Yong
Nagalingam, Saravanan
Preparation and characterization of iron sulphide thin films by chemical bath deposition method
title Preparation and characterization of iron sulphide thin films by chemical bath deposition method
title_full Preparation and characterization of iron sulphide thin films by chemical bath deposition method
title_fullStr Preparation and characterization of iron sulphide thin films by chemical bath deposition method
title_full_unstemmed Preparation and characterization of iron sulphide thin films by chemical bath deposition method
title_short Preparation and characterization of iron sulphide thin films by chemical bath deposition method
title_sort preparation and characterization of iron sulphide thin films by chemical bath deposition method
topic Thin films
Iron compounds
X-rays - Diffraction
url http://psasir.upm.edu.my/id/eprint/16311/1/Preparation%20and%20characterization%20of%20iron%20sulphide%20thin%20films%20by%20chemical%20bath%20deposition%20method.pdf
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