Synthesis of titanium dioxide nanoparticles via sucrose ester micelle-mediated hydrothermal processing route
Titanium dioxide nanoparticles were synthesized via low-temperature sucrose ester micelle-mediated hydrothermal processing route using titanium isopropoxide as the precursor. X-ray diffractometer revealed that the samples possessed a mixed crystalline phases consisting of anatase and brookite in whi...
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Format: | Article |
Language: | English |
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Penerbit Universiti Kebangsaan Malaysia
2010
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Online Access: | http://psasir.upm.edu.my/id/eprint/16952/1/synthesis%20of%20titanium%20dioxide.pdf |
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author | Anwar, Nor Sharina Kassim, Anuar Lim, Hong Ngee Zakarya, Salwani Asyikin Huang, Nay Ming |
author_facet | Anwar, Nor Sharina Kassim, Anuar Lim, Hong Ngee Zakarya, Salwani Asyikin Huang, Nay Ming |
author_sort | Anwar, Nor Sharina |
collection | UPM |
description | Titanium dioxide nanoparticles were synthesized via low-temperature sucrose ester micelle-mediated hydrothermal processing route using titanium isopropoxide as the precursor. X-ray diffractometer revealed that the samples possessed a mixed crystalline phases consisting of anatase and brookite in which anatase was the main phase. Upon increasing the hydrothermal reaction temperature, the degree of crystallinity of the nanoparticles improved and their morphology transformed from bundles of needles to rods and to spheres. Photocatalytic behaviour of the as-synthesized nanoparticles was investigated by photodegradation of methylene blue solution in an ultraviolet A irradiating photoreactor. The as-synthesized nanoparticles exhibited higher photocatalytic performance as compared to the commercial counterpart. |
first_indexed | 2024-03-06T07:38:56Z |
format | Article |
id | upm.eprints-16952 |
institution | Universiti Putra Malaysia |
language | English |
last_indexed | 2024-03-06T07:38:56Z |
publishDate | 2010 |
publisher | Penerbit Universiti Kebangsaan Malaysia |
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spelling | upm.eprints-169522016-03-21T13:46:06Z http://psasir.upm.edu.my/id/eprint/16952/ Synthesis of titanium dioxide nanoparticles via sucrose ester micelle-mediated hydrothermal processing route Anwar, Nor Sharina Kassim, Anuar Lim, Hong Ngee Zakarya, Salwani Asyikin Huang, Nay Ming Titanium dioxide nanoparticles were synthesized via low-temperature sucrose ester micelle-mediated hydrothermal processing route using titanium isopropoxide as the precursor. X-ray diffractometer revealed that the samples possessed a mixed crystalline phases consisting of anatase and brookite in which anatase was the main phase. Upon increasing the hydrothermal reaction temperature, the degree of crystallinity of the nanoparticles improved and their morphology transformed from bundles of needles to rods and to spheres. Photocatalytic behaviour of the as-synthesized nanoparticles was investigated by photodegradation of methylene blue solution in an ultraviolet A irradiating photoreactor. The as-synthesized nanoparticles exhibited higher photocatalytic performance as compared to the commercial counterpart. Penerbit Universiti Kebangsaan Malaysia 2010 Article PeerReviewed application/pdf en http://psasir.upm.edu.my/id/eprint/16952/1/synthesis%20of%20titanium%20dioxide.pdf Anwar, Nor Sharina and Kassim, Anuar and Lim, Hong Ngee and Zakarya, Salwani Asyikin and Huang, Nay Ming (2010) Synthesis of titanium dioxide nanoparticles via sucrose ester micelle-mediated hydrothermal processing route. Sains Malaysiana, 39 (2). pp. 261-265. ISSN 0126-6039 http://www.ukm.my/jsm/english_journals/vol39num2_2010/contentsVol39num2_2010.html |
spellingShingle | Anwar, Nor Sharina Kassim, Anuar Lim, Hong Ngee Zakarya, Salwani Asyikin Huang, Nay Ming Synthesis of titanium dioxide nanoparticles via sucrose ester micelle-mediated hydrothermal processing route |
title | Synthesis of titanium dioxide nanoparticles via sucrose ester micelle-mediated hydrothermal processing route |
title_full | Synthesis of titanium dioxide nanoparticles via sucrose ester micelle-mediated hydrothermal processing route |
title_fullStr | Synthesis of titanium dioxide nanoparticles via sucrose ester micelle-mediated hydrothermal processing route |
title_full_unstemmed | Synthesis of titanium dioxide nanoparticles via sucrose ester micelle-mediated hydrothermal processing route |
title_short | Synthesis of titanium dioxide nanoparticles via sucrose ester micelle-mediated hydrothermal processing route |
title_sort | synthesis of titanium dioxide nanoparticles via sucrose ester micelle mediated hydrothermal processing route |
url | http://psasir.upm.edu.my/id/eprint/16952/1/synthesis%20of%20titanium%20dioxide.pdf |
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