Thermal decomposition pathway of undoped and doped zinc layered gallate nanohybrid with Fe3+, Co2+ and Ni2+ to produce mesoporous and high pore volume carbon material.
A series of brucite-like materials, undoped and doped zinc layered hydroxide nitrate with 2% (molar) Fe3+, Co2+ and Ni2+ were synthesized. Organic–inorganic nanohybrid material with gallate anion as a guest, and zinc hydroxide nitrate, as an inorganic layered host was prepared by the ion-exchange me...
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| Format: | Article |
| Language: | English |
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Malaysian Solid State Science and Technology Society (MASS)
2009
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| Online Access: | http://psasir.upm.edu.my/id/eprint/17386/1/Thermal%20decomposition%20pathway%20of%20undoped%20and%20doped%20zinc%20layered%20gallate%20nanohybrid%20with%20Fe3.pdf |
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| author | Ghotbi, Mohammad Yeganeh Hussein, Mohd. Zobir Yahya, Asmah Ab. Rahman, Mohamad Zaki |
| author_facet | Ghotbi, Mohammad Yeganeh Hussein, Mohd. Zobir Yahya, Asmah Ab. Rahman, Mohamad Zaki |
| author_sort | Ghotbi, Mohammad Yeganeh |
| collection | UPM |
| description | A series of brucite-like materials, undoped and doped zinc layered hydroxide nitrate with 2% (molar) Fe3+, Co2+ and Ni2+ were synthesized. Organic–inorganic nanohybrid material with gallate anion as a guest, and zinc hydroxide nitrate, as an inorganic layered host was prepared by the ion-exchange method. The nanohybrid materials were heat-treated at various temperatures, 400–700 °C. X-ray diffraction, thermal analysis and also Fourier transform infrared results showed that incorporation of the doping agents within the zinc layered hydroxide salt layers has enhanced the heat-resistivity of the nanohybrid materials in the thermal decomposition pathway. Porous carbon materials can be obtained from the heat-treating the nanohybrids at 600 and 700 °C. Calcination of the nanohybrids at 700 °C under nitrogen atmosphere produces mesoporous and high pore volume carbon materials.
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| first_indexed | 2024-03-06T07:40:16Z |
| format | Article |
| id | upm.eprints-17386 |
| institution | Universiti Putra Malaysia |
| language | English |
| last_indexed | 2024-03-06T07:40:16Z |
| publishDate | 2009 |
| publisher | Malaysian Solid State Science and Technology Society (MASS) |
| record_format | dspace |
| spelling | upm.eprints-173862015-11-30T06:50:42Z http://psasir.upm.edu.my/id/eprint/17386/ Thermal decomposition pathway of undoped and doped zinc layered gallate nanohybrid with Fe3+, Co2+ and Ni2+ to produce mesoporous and high pore volume carbon material. Ghotbi, Mohammad Yeganeh Hussein, Mohd. Zobir Yahya, Asmah Ab. Rahman, Mohamad Zaki A series of brucite-like materials, undoped and doped zinc layered hydroxide nitrate with 2% (molar) Fe3+, Co2+ and Ni2+ were synthesized. Organic–inorganic nanohybrid material with gallate anion as a guest, and zinc hydroxide nitrate, as an inorganic layered host was prepared by the ion-exchange method. The nanohybrid materials were heat-treated at various temperatures, 400–700 °C. X-ray diffraction, thermal analysis and also Fourier transform infrared results showed that incorporation of the doping agents within the zinc layered hydroxide salt layers has enhanced the heat-resistivity of the nanohybrid materials in the thermal decomposition pathway. Porous carbon materials can be obtained from the heat-treating the nanohybrids at 600 and 700 °C. Calcination of the nanohybrids at 700 °C under nitrogen atmosphere produces mesoporous and high pore volume carbon materials. Malaysian Solid State Science and Technology Society (MASS) 2009 Article PeerReviewed application/pdf en http://psasir.upm.edu.my/id/eprint/17386/1/Thermal%20decomposition%20pathway%20of%20undoped%20and%20doped%20zinc%20layered%20gallate%20nanohybrid%20with%20Fe3.pdf Ghotbi, Mohammad Yeganeh and Hussein, Mohd. Zobir and Yahya, Asmah and Ab. Rahman, Mohamad Zaki (2009) Thermal decomposition pathway of undoped and doped zinc layered gallate nanohybrid with Fe3+, Co2+ and Ni2+ to produce mesoporous and high pore volume carbon material. Solid State Science and Technology, 11 (12). pp. 2125-2132. ISSN 0128-7389 Nanostructures Metals - Heat treatment http://dx.doi.org/10.1016/j.solidstatesciences.2009.08.013 |
| spellingShingle | Nanostructures Metals - Heat treatment Ghotbi, Mohammad Yeganeh Hussein, Mohd. Zobir Yahya, Asmah Ab. Rahman, Mohamad Zaki Thermal decomposition pathway of undoped and doped zinc layered gallate nanohybrid with Fe3+, Co2+ and Ni2+ to produce mesoporous and high pore volume carbon material. |
| title | Thermal decomposition pathway of undoped and doped zinc layered gallate nanohybrid with Fe3+, Co2+ and Ni2+ to produce mesoporous and high pore volume carbon material. |
| title_full | Thermal decomposition pathway of undoped and doped zinc layered gallate nanohybrid with Fe3+, Co2+ and Ni2+ to produce mesoporous and high pore volume carbon material. |
| title_fullStr | Thermal decomposition pathway of undoped and doped zinc layered gallate nanohybrid with Fe3+, Co2+ and Ni2+ to produce mesoporous and high pore volume carbon material. |
| title_full_unstemmed | Thermal decomposition pathway of undoped and doped zinc layered gallate nanohybrid with Fe3+, Co2+ and Ni2+ to produce mesoporous and high pore volume carbon material. |
| title_short | Thermal decomposition pathway of undoped and doped zinc layered gallate nanohybrid with Fe3+, Co2+ and Ni2+ to produce mesoporous and high pore volume carbon material. |
| title_sort | thermal decomposition pathway of undoped and doped zinc layered gallate nanohybrid with fe3 co2 and ni2 to produce mesoporous and high pore volume carbon material |
| topic | Nanostructures Metals - Heat treatment |
| url | http://psasir.upm.edu.my/id/eprint/17386/1/Thermal%20decomposition%20pathway%20of%20undoped%20and%20doped%20zinc%20layered%20gallate%20nanohybrid%20with%20Fe3.pdf |
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