Optimization for development of carbon nanotubes using Taguchi method at constant temperature

In this study, an optimization of floating catalyst chemical vapor deposition (FC-CVD) using Taguchi method is done in developing multiwall nanotubes (MWNTs) at constant temperature. The reaction is run at the temperature of 850°C in atmospheric pressure with ferrocene as the catalyst precursor and...

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Main Authors: Sufian, Suriati, Yusup, Suzana, Ahmadun, Fakhru'l-Razi
Format: Article
Language:English
Published: Trans Tech Publications 2010
Online Access:http://psasir.upm.edu.my/id/eprint/22912/1/Optimization%20for%20development%20of%20carbon%20nanotubes%20using%20Taguchi%20method%20at%20constant%20temperature.pdf
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author Sufian, Suriati
Yusup, Suzana
Ahmadun, Fakhru'l-Razi
author_facet Sufian, Suriati
Yusup, Suzana
Ahmadun, Fakhru'l-Razi
author_sort Sufian, Suriati
collection UPM
description In this study, an optimization of floating catalyst chemical vapor deposition (FC-CVD) using Taguchi method is done in developing multiwall nanotubes (MWNTs) at constant temperature. The reaction is run at the temperature of 850°C in atmospheric pressure with ferrocene as the catalyst precursor and benzene as the carbon feedstock. By applying Taguchi’s method as the design of experiment, three parameters: namely reaction time, hydrogen flow rate and catalyst weight have been varied during the optimization of the experiment. The results show that the BET specific surface area increases as the reaction time increases, the degree of graphitization reduces as the mass of the catalyst increases and the relative value of amorphous carbon to graphite carbon decreases as the hydrogen flow rate increases.
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spelling upm.eprints-229122020-04-15T16:18:15Z http://psasir.upm.edu.my/id/eprint/22912/ Optimization for development of carbon nanotubes using Taguchi method at constant temperature Sufian, Suriati Yusup, Suzana Ahmadun, Fakhru'l-Razi In this study, an optimization of floating catalyst chemical vapor deposition (FC-CVD) using Taguchi method is done in developing multiwall nanotubes (MWNTs) at constant temperature. The reaction is run at the temperature of 850°C in atmospheric pressure with ferrocene as the catalyst precursor and benzene as the carbon feedstock. By applying Taguchi’s method as the design of experiment, three parameters: namely reaction time, hydrogen flow rate and catalyst weight have been varied during the optimization of the experiment. The results show that the BET specific surface area increases as the reaction time increases, the degree of graphitization reduces as the mass of the catalyst increases and the relative value of amorphous carbon to graphite carbon decreases as the hydrogen flow rate increases. Trans Tech Publications 2010 Article PeerReviewed text en http://psasir.upm.edu.my/id/eprint/22912/1/Optimization%20for%20development%20of%20carbon%20nanotubes%20using%20Taguchi%20method%20at%20constant%20temperature.pdf Sufian, Suriati and Yusup, Suzana and Ahmadun, Fakhru'l-Razi (2010) Optimization for development of carbon nanotubes using Taguchi method at constant temperature. Journal of Nano Research, 11. pp. 95-100. ISSN 1662-5250; ESSN: 1661-9897 https://www.scientific.net/JNanoR.11.95 10.4028/www.scientific.net/JNanoR.11.95
spellingShingle Sufian, Suriati
Yusup, Suzana
Ahmadun, Fakhru'l-Razi
Optimization for development of carbon nanotubes using Taguchi method at constant temperature
title Optimization for development of carbon nanotubes using Taguchi method at constant temperature
title_full Optimization for development of carbon nanotubes using Taguchi method at constant temperature
title_fullStr Optimization for development of carbon nanotubes using Taguchi method at constant temperature
title_full_unstemmed Optimization for development of carbon nanotubes using Taguchi method at constant temperature
title_short Optimization for development of carbon nanotubes using Taguchi method at constant temperature
title_sort optimization for development of carbon nanotubes using taguchi method at constant temperature
url http://psasir.upm.edu.my/id/eprint/22912/1/Optimization%20for%20development%20of%20carbon%20nanotubes%20using%20Taguchi%20method%20at%20constant%20temperature.pdf
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