Authentication analysis of cod liver oil from beef fat using fatty acid composition and FTIR spectra

This study aimed to authenticate cod liver oil (CLO) from beef fat (BF) by determining the level of BF as a fat adulterant in CLO. Two instrumental techniques, namely GC-FID for fatty acid analysis and Fourier transform infrared (FTIR) spectroscopy, were exploited for such authentication. The decrea...

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Main Authors: Abdul Rohman, Che Man, Yaakob
Format: Article
Language:English
Published: Taylor & Francis 2011
Online Access:http://psasir.upm.edu.my/id/eprint/24148/1/Authentication%20analysis%20of%20cod%20liver%20oil%20from%20beef%20fat%20using%20fatty%20acid%20composition%20and%20FTIR%20spectra.pdf
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author Abdul Rohman,
Che Man, Yaakob
author_facet Abdul Rohman,
Che Man, Yaakob
author_sort Abdul Rohman,
collection UPM
description This study aimed to authenticate cod liver oil (CLO) from beef fat (BF) by determining the level of BF as a fat adulterant in CLO. Two instrumental techniques, namely GC-FID for fatty acid analysis and Fourier transform infrared (FTIR) spectroscopy, were exploited for such authentication. The decreased level of some fatty acids, especially eicosapentaenoic acid (EPA) and docosahexaenoic acid (DHA), could be used as an indicative means to detect the adulteration of CLO with BF. In addition, FTIR spectroscopy combined with partial least-squares (PLS) at frequency regions of 1200-1000 cm -1 was successfully developed for the quantification of BF in CLO. Using the PLS model, the errors obtained in calibration and prediction samples were 0.55% and 0.82% v/v, respectively.
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spelling upm.eprints-241482016-04-22T07:56:46Z http://psasir.upm.edu.my/id/eprint/24148/ Authentication analysis of cod liver oil from beef fat using fatty acid composition and FTIR spectra Abdul Rohman, Che Man, Yaakob This study aimed to authenticate cod liver oil (CLO) from beef fat (BF) by determining the level of BF as a fat adulterant in CLO. Two instrumental techniques, namely GC-FID for fatty acid analysis and Fourier transform infrared (FTIR) spectroscopy, were exploited for such authentication. The decreased level of some fatty acids, especially eicosapentaenoic acid (EPA) and docosahexaenoic acid (DHA), could be used as an indicative means to detect the adulteration of CLO with BF. In addition, FTIR spectroscopy combined with partial least-squares (PLS) at frequency regions of 1200-1000 cm -1 was successfully developed for the quantification of BF in CLO. Using the PLS model, the errors obtained in calibration and prediction samples were 0.55% and 0.82% v/v, respectively. Taylor & Francis 2011 Article PeerReviewed application/pdf en http://psasir.upm.edu.my/id/eprint/24148/1/Authentication%20analysis%20of%20cod%20liver%20oil%20from%20beef%20fat%20using%20fatty%20acid%20composition%20and%20FTIR%20spectra.pdf Abdul Rohman, and Che Man, Yaakob (2011) Authentication analysis of cod liver oil from beef fat using fatty acid composition and FTIR spectra. Food Additives & Contaminants: Part A, 28 (11). pp. 1469-1474. ISSN 1944-0049; ESSN: 1944-0057 http://www.tandfonline.com/doi/abs/10.1080/19440049.2011.600727 10.1080/19440049.2011.600727
spellingShingle Abdul Rohman,
Che Man, Yaakob
Authentication analysis of cod liver oil from beef fat using fatty acid composition and FTIR spectra
title Authentication analysis of cod liver oil from beef fat using fatty acid composition and FTIR spectra
title_full Authentication analysis of cod liver oil from beef fat using fatty acid composition and FTIR spectra
title_fullStr Authentication analysis of cod liver oil from beef fat using fatty acid composition and FTIR spectra
title_full_unstemmed Authentication analysis of cod liver oil from beef fat using fatty acid composition and FTIR spectra
title_short Authentication analysis of cod liver oil from beef fat using fatty acid composition and FTIR spectra
title_sort authentication analysis of cod liver oil from beef fat using fatty acid composition and ftir spectra
url http://psasir.upm.edu.my/id/eprint/24148/1/Authentication%20analysis%20of%20cod%20liver%20oil%20from%20beef%20fat%20using%20fatty%20acid%20composition%20and%20FTIR%20spectra.pdf
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AT chemanyaakob authenticationanalysisofcodliveroilfrombeeffatusingfattyacidcompositionandftirspectra