Determining optimum conditions for lipase-catalyzed synthesis of triethanolamine (TEA)-based esterquat cationic surfactant by a Taguchi Robust design method.
A Taguchi robust design method with an L₉ orthogonal array was implemented to optimize experimental conditions for the biosynthesis of triethanolamine (TEA)-based esterquat cationic surfactants using an enzymatic reaction method. The esterification reaction conversion% was considered as the response...
| Main Authors: | , , , |
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| Format: | Article |
| Language: | English English |
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MDPI
2011
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| Online Access: | http://psasir.upm.edu.my/id/eprint/24951/1/Determining%20optimum%20conditions%20for%20lipase.pdf |
| _version_ | 1825925677697728512 |
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| author | Fard Masoumi, Hamid Reza Kassim, Anuar Basri, Mahiran Abdullah, Dzulkefly Kuang |
| author_facet | Fard Masoumi, Hamid Reza Kassim, Anuar Basri, Mahiran Abdullah, Dzulkefly Kuang |
| author_sort | Fard Masoumi, Hamid Reza |
| collection | UPM |
| description | A Taguchi robust design method with an L₉ orthogonal array was implemented to optimize experimental conditions for the biosynthesis of triethanolamine (TEA)-based esterquat cationic surfactants using an enzymatic reaction method. The esterification reaction conversion% was considered as the response. Enzyme amount, reaction time, reaction temperature and molar ratio of substrates, [oleic acid: triethanolamine (OA:TEA)] were chosen as main parameters. As a result of the Taguchi analysis in this study, the molar ratio of substrates was found to be the most influential parameter on the esterification reaction conversion%. The amount of enzyme in the reaction had also a significant effect on reaction conversion%. |
| first_indexed | 2024-03-06T08:01:23Z |
| format | Article |
| id | upm.eprints-24951 |
| institution | Universiti Putra Malaysia |
| language | English English |
| last_indexed | 2024-03-06T08:01:23Z |
| publishDate | 2011 |
| publisher | MDPI |
| record_format | dspace |
| spelling | upm.eprints-249512015-09-18T08:19:40Z http://psasir.upm.edu.my/id/eprint/24951/ Determining optimum conditions for lipase-catalyzed synthesis of triethanolamine (TEA)-based esterquat cationic surfactant by a Taguchi Robust design method. Fard Masoumi, Hamid Reza Kassim, Anuar Basri, Mahiran Abdullah, Dzulkefly Kuang A Taguchi robust design method with an L₉ orthogonal array was implemented to optimize experimental conditions for the biosynthesis of triethanolamine (TEA)-based esterquat cationic surfactants using an enzymatic reaction method. The esterification reaction conversion% was considered as the response. Enzyme amount, reaction time, reaction temperature and molar ratio of substrates, [oleic acid: triethanolamine (OA:TEA)] were chosen as main parameters. As a result of the Taguchi analysis in this study, the molar ratio of substrates was found to be the most influential parameter on the esterification reaction conversion%. The amount of enzyme in the reaction had also a significant effect on reaction conversion%. MDPI 2011-06-03 Article PeerReviewed application/pdf en http://psasir.upm.edu.my/id/eprint/24951/1/Determining%20optimum%20conditions%20for%20lipase.pdf Fard Masoumi, Hamid Reza and Kassim, Anuar and Basri, Mahiran and Abdullah, Dzulkefly Kuang (2011) Determining optimum conditions for lipase-catalyzed synthesis of triethanolamine (TEA)-based esterquat cationic surfactant by a Taguchi Robust design method. Molecules, 16 (6). pp. 4672-4680. ISSN 1431-5157; ESSN:1420-3049 http://www.mdpi.com/ 10.3390/molecules16064672 English |
| spellingShingle | Fard Masoumi, Hamid Reza Kassim, Anuar Basri, Mahiran Abdullah, Dzulkefly Kuang Determining optimum conditions for lipase-catalyzed synthesis of triethanolamine (TEA)-based esterquat cationic surfactant by a Taguchi Robust design method. |
| title | Determining optimum conditions for lipase-catalyzed synthesis of triethanolamine (TEA)-based esterquat cationic surfactant by a Taguchi Robust design method. |
| title_full | Determining optimum conditions for lipase-catalyzed synthesis of triethanolamine (TEA)-based esterquat cationic surfactant by a Taguchi Robust design method. |
| title_fullStr | Determining optimum conditions for lipase-catalyzed synthesis of triethanolamine (TEA)-based esterquat cationic surfactant by a Taguchi Robust design method. |
| title_full_unstemmed | Determining optimum conditions for lipase-catalyzed synthesis of triethanolamine (TEA)-based esterquat cationic surfactant by a Taguchi Robust design method. |
| title_short | Determining optimum conditions for lipase-catalyzed synthesis of triethanolamine (TEA)-based esterquat cationic surfactant by a Taguchi Robust design method. |
| title_sort | determining optimum conditions for lipase catalyzed synthesis of triethanolamine tea based esterquat cationic surfactant by a taguchi robust design method |
| url | http://psasir.upm.edu.my/id/eprint/24951/1/Determining%20optimum%20conditions%20for%20lipase.pdf |
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