Effects of sintering temperature on grain growth and the complex permeability of Co0.2Ni0.3Zn0.5Fe2O4 material prepared using mechanically alloyed nanoparticles.

Nanoparticle-sized Co0.2Ni0.3Zn0.5Fe2O4 was prepared using mechanical alloying and sintering. The starting raw materials were milled in air and subsequently sintered at various temperatures from 600 to 1300 °C. The effects of sintering temperature on physical, magnetic and electrical characteristics...

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Main Authors: Waje, Samaila Bawa, Hashim, Mansor, Ismail, Ismayadi
Format: Article
Language:English
English
Published: Elsevier 2011
Online Access:http://psasir.upm.edu.my/id/eprint/25106/1/Effects%20of%20sintering%20temperature%20on%20grain%20growth%20and%20the%20complex%20permeability%20of%20Co0.pdf
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author Waje, Samaila Bawa
Hashim, Mansor
Ismail, Ismayadi
author_facet Waje, Samaila Bawa
Hashim, Mansor
Ismail, Ismayadi
author_sort Waje, Samaila Bawa
collection UPM
description Nanoparticle-sized Co0.2Ni0.3Zn0.5Fe2O4 was prepared using mechanical alloying and sintering. The starting raw materials were milled in air and subsequently sintered at various temperatures from 600 to 1300 °C. The effects of sintering temperature on physical, magnetic and electrical characteristics were studied. The complex permittivity and permeability were investigated in the frequency range 10 MHz to 1.0 GHz. The results show that single phase Co0.2Ni0.3Zn0.5Fe2O4 could not be formed during milling alone and therefore requires sintering. The crystallization of the ferrite sample increases with increasing sintering temperature; which decrease the porosity and increase the density, crystallite size and the shrinkage of the material. The maximum magnetization value of 83.1 emu/g was obtained for a sample sintered at 1200 °C, while both the retentivity and the coercivity decrease with increasing the sintering temperature. The permeability values vary with both the sintering temperature and the frequency and the absolute value of the permeability decreased after the natural resonance frequency. The real part of the permittivity was constant within the measured frequency, while the loss tangent values decreased gradually with increasing frequency.
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spelling upm.eprints-251062015-10-09T07:47:52Z http://psasir.upm.edu.my/id/eprint/25106/ Effects of sintering temperature on grain growth and the complex permeability of Co0.2Ni0.3Zn0.5Fe2O4 material prepared using mechanically alloyed nanoparticles. Waje, Samaila Bawa Hashim, Mansor Ismail, Ismayadi Nanoparticle-sized Co0.2Ni0.3Zn0.5Fe2O4 was prepared using mechanical alloying and sintering. The starting raw materials were milled in air and subsequently sintered at various temperatures from 600 to 1300 °C. The effects of sintering temperature on physical, magnetic and electrical characteristics were studied. The complex permittivity and permeability were investigated in the frequency range 10 MHz to 1.0 GHz. The results show that single phase Co0.2Ni0.3Zn0.5Fe2O4 could not be formed during milling alone and therefore requires sintering. The crystallization of the ferrite sample increases with increasing sintering temperature; which decrease the porosity and increase the density, crystallite size and the shrinkage of the material. The maximum magnetization value of 83.1 emu/g was obtained for a sample sintered at 1200 °C, while both the retentivity and the coercivity decrease with increasing the sintering temperature. The permeability values vary with both the sintering temperature and the frequency and the absolute value of the permeability decreased after the natural resonance frequency. The real part of the permittivity was constant within the measured frequency, while the loss tangent values decreased gradually with increasing frequency. Elsevier 2011-06 Article PeerReviewed application/pdf en http://psasir.upm.edu.my/id/eprint/25106/1/Effects%20of%20sintering%20temperature%20on%20grain%20growth%20and%20the%20complex%20permeability%20of%20Co0.pdf Waje, Samaila Bawa and Hashim, Mansor and Ismail, Ismayadi (2011) Effects of sintering temperature on grain growth and the complex permeability of Co0.2Ni0.3Zn0.5Fe2O4 material prepared using mechanically alloyed nanoparticles. Journal of Magnetism and Magnetic Materials, 323 (11). pp. 1433-1439. ISSN 0304-8853 http://www.elsevier.com/ 10.1016/j.jmmm.2010.12.032 English
spellingShingle Waje, Samaila Bawa
Hashim, Mansor
Ismail, Ismayadi
Effects of sintering temperature on grain growth and the complex permeability of Co0.2Ni0.3Zn0.5Fe2O4 material prepared using mechanically alloyed nanoparticles.
title Effects of sintering temperature on grain growth and the complex permeability of Co0.2Ni0.3Zn0.5Fe2O4 material prepared using mechanically alloyed nanoparticles.
title_full Effects of sintering temperature on grain growth and the complex permeability of Co0.2Ni0.3Zn0.5Fe2O4 material prepared using mechanically alloyed nanoparticles.
title_fullStr Effects of sintering temperature on grain growth and the complex permeability of Co0.2Ni0.3Zn0.5Fe2O4 material prepared using mechanically alloyed nanoparticles.
title_full_unstemmed Effects of sintering temperature on grain growth and the complex permeability of Co0.2Ni0.3Zn0.5Fe2O4 material prepared using mechanically alloyed nanoparticles.
title_short Effects of sintering temperature on grain growth and the complex permeability of Co0.2Ni0.3Zn0.5Fe2O4 material prepared using mechanically alloyed nanoparticles.
title_sort effects of sintering temperature on grain growth and the complex permeability of co0 2ni0 3zn0 5fe2o4 material prepared using mechanically alloyed nanoparticles
url http://psasir.upm.edu.my/id/eprint/25106/1/Effects%20of%20sintering%20temperature%20on%20grain%20growth%20and%20the%20complex%20permeability%20of%20Co0.pdf
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