Dependence of developing magnetic hysteresis characteristics on stages of evolving microstructure in polycrystalline yttrium iron garnet
The microstructure evolution in several polycrystalline yttrium iron garnet samples as a result of a sintering scheme was studied in detail, in parallel with the changes in their magnetic properties. Samples with nanometer sized starting powder were synthesized by employing the High-Energy Ball Mill...
| Main Authors: | , , , , , |
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| Format: | Article |
| Language: | English |
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Elsevier
2012
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| Online Access: | http://psasir.upm.edu.my/id/eprint/25204/1/Dependence%20of%20developing%20magnetic%20hysteresis%20characteristics%20on%20stages%20of%20evolving%20microstructure%20in%20polycrystalline%20yttrium%20iron%20garnet.pdf |
| _version_ | 1825925730431664128 |
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| author | Nazlan, Rodziah Hashim, Mansor Ibrahim, Idza Riati Ismail, Ismayadi Abdullah, Nor Hapishah Matori, Khamirul Amin |
| author_facet | Nazlan, Rodziah Hashim, Mansor Ibrahim, Idza Riati Ismail, Ismayadi Abdullah, Nor Hapishah Matori, Khamirul Amin |
| author_sort | Nazlan, Rodziah |
| collection | UPM |
| description | The microstructure evolution in several polycrystalline yttrium iron garnet samples as a result of a sintering scheme was studied in detail, in parallel with the changes in their magnetic properties. Samples with nanometer sized starting powder were synthesized by employing the High-Energy Ball Milling technique and then sintering toroidal compacts of the milled powder. Nine sintered samples were obtained, each corresponding to a particular sintering from 600 °C to 1400 °C. The samples were characterized for their evolution in crystalline phases, microstructure and magnetic hysteresis-loops parameters. The results showed an increasing tendency of the saturation magnetization and saturation induction with grain size, which is attributed to crystallinity increase and to reduction of demagnetizing fields in the grains. The variation in coercivity could be related to anisotropy field changes within the samples due to grain size changes. In particular, the starting appearance of room temperature ferromagnetic order suggested by the sigmoid-shaped B–H loops seems to be dependent on a sufficient number of large enough magnetic domain-containing grains having been formed in the microstructure. Viewed simultaneously, the hysteresis loops appear to belong to three groups with different magnetism-type dominance, respectively dependent on phase purity and three different groups of grain size distributions. |
| first_indexed | 2024-03-06T08:02:08Z |
| format | Article |
| id | upm.eprints-25204 |
| institution | Universiti Putra Malaysia |
| language | English |
| last_indexed | 2024-03-06T08:02:08Z |
| publishDate | 2012 |
| publisher | Elsevier |
| record_format | dspace |
| spelling | upm.eprints-252042016-05-10T08:53:39Z http://psasir.upm.edu.my/id/eprint/25204/ Dependence of developing magnetic hysteresis characteristics on stages of evolving microstructure in polycrystalline yttrium iron garnet Nazlan, Rodziah Hashim, Mansor Ibrahim, Idza Riati Ismail, Ismayadi Abdullah, Nor Hapishah Matori, Khamirul Amin The microstructure evolution in several polycrystalline yttrium iron garnet samples as a result of a sintering scheme was studied in detail, in parallel with the changes in their magnetic properties. Samples with nanometer sized starting powder were synthesized by employing the High-Energy Ball Milling technique and then sintering toroidal compacts of the milled powder. Nine sintered samples were obtained, each corresponding to a particular sintering from 600 °C to 1400 °C. The samples were characterized for their evolution in crystalline phases, microstructure and magnetic hysteresis-loops parameters. The results showed an increasing tendency of the saturation magnetization and saturation induction with grain size, which is attributed to crystallinity increase and to reduction of demagnetizing fields in the grains. The variation in coercivity could be related to anisotropy field changes within the samples due to grain size changes. In particular, the starting appearance of room temperature ferromagnetic order suggested by the sigmoid-shaped B–H loops seems to be dependent on a sufficient number of large enough magnetic domain-containing grains having been formed in the microstructure. Viewed simultaneously, the hysteresis loops appear to belong to three groups with different magnetism-type dominance, respectively dependent on phase purity and three different groups of grain size distributions. Elsevier 2012-01-15 Article PeerReviewed application/pdf en http://psasir.upm.edu.my/id/eprint/25204/1/Dependence%20of%20developing%20magnetic%20hysteresis%20characteristics%20on%20stages%20of%20evolving%20microstructure%20in%20polycrystalline%20yttrium%20iron%20garnet.pdf Nazlan, Rodziah and Hashim, Mansor and Ibrahim, Idza Riati and Ismail, Ismayadi and Abdullah, Nor Hapishah and Matori, Khamirul Amin (2012) Dependence of developing magnetic hysteresis characteristics on stages of evolving microstructure in polycrystalline yttrium iron garnet. Applied Surface Science, 258 (7). pp. 2679-2685. ISSN 0169-4332; ESSN: 1873-5584 http://www.sciencedirect.com/science/article/pii/S0169433211016862 10.1016/j.apsusc.2011.10.117 |
| spellingShingle | Nazlan, Rodziah Hashim, Mansor Ibrahim, Idza Riati Ismail, Ismayadi Abdullah, Nor Hapishah Matori, Khamirul Amin Dependence of developing magnetic hysteresis characteristics on stages of evolving microstructure in polycrystalline yttrium iron garnet |
| title | Dependence of developing magnetic hysteresis characteristics on stages of evolving microstructure in polycrystalline yttrium iron garnet |
| title_full | Dependence of developing magnetic hysteresis characteristics on stages of evolving microstructure in polycrystalline yttrium iron garnet |
| title_fullStr | Dependence of developing magnetic hysteresis characteristics on stages of evolving microstructure in polycrystalline yttrium iron garnet |
| title_full_unstemmed | Dependence of developing magnetic hysteresis characteristics on stages of evolving microstructure in polycrystalline yttrium iron garnet |
| title_short | Dependence of developing magnetic hysteresis characteristics on stages of evolving microstructure in polycrystalline yttrium iron garnet |
| title_sort | dependence of developing magnetic hysteresis characteristics on stages of evolving microstructure in polycrystalline yttrium iron garnet |
| url | http://psasir.upm.edu.my/id/eprint/25204/1/Dependence%20of%20developing%20magnetic%20hysteresis%20characteristics%20on%20stages%20of%20evolving%20microstructure%20in%20polycrystalline%20yttrium%20iron%20garnet.pdf |
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