Effect of different mineralizers in the sonochemical synthesis of self-assembled nanorods vanadium oxide

The effects of different potassium salts (KNO(3) and KCl) as mineralizer on the synthesis of self-assembled nanorods vanadium pentoxide, V(2)O(5) via sonochemical treatment were studied at different duration i.e., 30, 60, 90 and 120 min. All the materials synthesized were further characterized by x-...

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Bibliographic Details
Main Authors: Yap, Taufiq Yun Hin, Hoh, Joshua J. R., Wong, Yee Ching
Format: Article
Language:English
Published: Asian Publication Corporation 2011
Online Access:http://psasir.upm.edu.my/id/eprint/25273/1/Effect%20of%20different%20mineralizers%20in%20the%20sonochemical%20synthesis%20of%20self-assembled%20nanorods%20vanadium%20oxide.pdf
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Summary:The effects of different potassium salts (KNO(3) and KCl) as mineralizer on the synthesis of self-assembled nanorods vanadium pentoxide, V(2)O(5) via sonochemical treatment were studied at different duration i.e., 30, 60, 90 and 120 min. All the materials synthesized were further characterized by x-ray diffraction, scanning electron microscopy and transmission electron microscopy. X-ray diffraction patterns revealed that the potassium ion from the mineralizers reacted with the V(2)O(5) after prolonged sonochemical treatment duration. The morphology of the V(2)O(5) changed from platelet-like structures into nanorods after 90 min of sonochemical treatment. TEM micrographs show the process of formation of the self-assembled V(2)O(5) nanorod bundles with increased sonochemical treatment duration.