The impact of polyvinylpyrrolidone on properties of cadmium oxide semiconductor nanoparticles manufactured by heat treatment technique
Cadmium oxide semiconductor nanoparticles were produced using a water based mixture, incorporating cadmium nitrates, polyvinyl pyrrolidone (PVP), and calcination temperature. An X-ray diffraction (XRD) evaluation was conducted to determine the degree of crystallization of the semiconductor nanoparti...
| Main Authors: | , , , |
|---|---|
| Format: | Article |
| Language: | English |
| Published: |
MDPI
2016
|
| Online Access: | http://psasir.upm.edu.my/id/eprint/27977/1/27977.pdf |
| _version_ | 1825947226649657344 |
|---|---|
| author | Al-Hada, Naif Mohammed Saion, Elias Talib, Zainal Abidin Shaari, Abdul Halim |
| author_facet | Al-Hada, Naif Mohammed Saion, Elias Talib, Zainal Abidin Shaari, Abdul Halim |
| author_sort | Al-Hada, Naif Mohammed |
| collection | UPM |
| description | Cadmium oxide semiconductor nanoparticles were produced using a water based mixture, incorporating cadmium nitrates, polyvinyl pyrrolidone (PVP), and calcination temperature. An X-ray diffraction (XRD) evaluation was conducted to determine the degree of crystallization of the semiconductor nanoparticles. In addition, scanning electron microscopy (SEM) was conducted to identify the morphological features of the nanoparticles. The typical particle sizes and particle dispersal were analyzed via the use of transmission electron microscopy (TEM). The findings provided further support for the XRD outcomes. To determine the composition phase, Fourier transform infrared spectroscopy (FT-IR) was conducted, as it indicated the existence of not only metal oxide ionic band in the selection of samples, but also the efficient removal of organic compounds following calcinations. The optical characteristics were demonstrated, so as to analyze the energy band gap via the use of a UV–Vis spectrophotometer. A reduced particle size resulted in diminution of the intensity of photoluminescence, was demonstrated by PL spectra. Plus, the magnetic characteristics were examined using an electron spin resonance (ESR) spectroscopy, which affirmed the existence of unpaired electrons. |
| first_indexed | 2024-03-06T08:09:59Z |
| format | Article |
| id | upm.eprints-27977 |
| institution | Universiti Putra Malaysia |
| language | English |
| last_indexed | 2024-03-06T08:09:59Z |
| publishDate | 2016 |
| publisher | MDPI |
| record_format | dspace |
| spelling | upm.eprints-279772016-06-20T05:55:38Z http://psasir.upm.edu.my/id/eprint/27977/ The impact of polyvinylpyrrolidone on properties of cadmium oxide semiconductor nanoparticles manufactured by heat treatment technique Al-Hada, Naif Mohammed Saion, Elias Talib, Zainal Abidin Shaari, Abdul Halim Cadmium oxide semiconductor nanoparticles were produced using a water based mixture, incorporating cadmium nitrates, polyvinyl pyrrolidone (PVP), and calcination temperature. An X-ray diffraction (XRD) evaluation was conducted to determine the degree of crystallization of the semiconductor nanoparticles. In addition, scanning electron microscopy (SEM) was conducted to identify the morphological features of the nanoparticles. The typical particle sizes and particle dispersal were analyzed via the use of transmission electron microscopy (TEM). The findings provided further support for the XRD outcomes. To determine the composition phase, Fourier transform infrared spectroscopy (FT-IR) was conducted, as it indicated the existence of not only metal oxide ionic band in the selection of samples, but also the efficient removal of organic compounds following calcinations. The optical characteristics were demonstrated, so as to analyze the energy band gap via the use of a UV–Vis spectrophotometer. A reduced particle size resulted in diminution of the intensity of photoluminescence, was demonstrated by PL spectra. Plus, the magnetic characteristics were examined using an electron spin resonance (ESR) spectroscopy, which affirmed the existence of unpaired electrons. MDPI 2016 Article PeerReviewed application/pdf en http://psasir.upm.edu.my/id/eprint/27977/1/27977.pdf Al-Hada, Naif Mohammed and Saion, Elias and Talib, Zainal Abidin and Shaari, Abdul Halim (2016) The impact of polyvinylpyrrolidone on properties of cadmium oxide semiconductor nanoparticles manufactured by heat treatment technique. Polymers, 8 (4). art. no. 113. pp. 1-15. ISSN 2073-4360 http://www.mdpi.com/2073-4360/8/4/113 10.3390/polym8040113 |
| spellingShingle | Al-Hada, Naif Mohammed Saion, Elias Talib, Zainal Abidin Shaari, Abdul Halim The impact of polyvinylpyrrolidone on properties of cadmium oxide semiconductor nanoparticles manufactured by heat treatment technique |
| title | The impact of polyvinylpyrrolidone on properties of cadmium oxide semiconductor nanoparticles manufactured by heat treatment technique |
| title_full | The impact of polyvinylpyrrolidone on properties of cadmium oxide semiconductor nanoparticles manufactured by heat treatment technique |
| title_fullStr | The impact of polyvinylpyrrolidone on properties of cadmium oxide semiconductor nanoparticles manufactured by heat treatment technique |
| title_full_unstemmed | The impact of polyvinylpyrrolidone on properties of cadmium oxide semiconductor nanoparticles manufactured by heat treatment technique |
| title_short | The impact of polyvinylpyrrolidone on properties of cadmium oxide semiconductor nanoparticles manufactured by heat treatment technique |
| title_sort | impact of polyvinylpyrrolidone on properties of cadmium oxide semiconductor nanoparticles manufactured by heat treatment technique |
| url | http://psasir.upm.edu.my/id/eprint/27977/1/27977.pdf |
| work_keys_str_mv | AT alhadanaifmohammed theimpactofpolyvinylpyrrolidoneonpropertiesofcadmiumoxidesemiconductornanoparticlesmanufacturedbyheattreatmenttechnique AT saionelias theimpactofpolyvinylpyrrolidoneonpropertiesofcadmiumoxidesemiconductornanoparticlesmanufacturedbyheattreatmenttechnique AT talibzainalabidin theimpactofpolyvinylpyrrolidoneonpropertiesofcadmiumoxidesemiconductornanoparticlesmanufacturedbyheattreatmenttechnique AT shaariabdulhalim theimpactofpolyvinylpyrrolidoneonpropertiesofcadmiumoxidesemiconductornanoparticlesmanufacturedbyheattreatmenttechnique AT alhadanaifmohammed impactofpolyvinylpyrrolidoneonpropertiesofcadmiumoxidesemiconductornanoparticlesmanufacturedbyheattreatmenttechnique AT saionelias impactofpolyvinylpyrrolidoneonpropertiesofcadmiumoxidesemiconductornanoparticlesmanufacturedbyheattreatmenttechnique AT talibzainalabidin impactofpolyvinylpyrrolidoneonpropertiesofcadmiumoxidesemiconductornanoparticlesmanufacturedbyheattreatmenttechnique AT shaariabdulhalim impactofpolyvinylpyrrolidoneonpropertiesofcadmiumoxidesemiconductornanoparticlesmanufacturedbyheattreatmenttechnique |