Jatropha curcas seed oil as new substrate for enzymatic methylhydroxylaminolysis.
Synthesis of methyl fatty hydroxamic acids (MFHAs) was carried out using lipozyme RM IM based on Jatropha Curcas seed oil. Optimized conditions were obtained at a mole ratio of 6/1 of methyl hydroxylamine/oil, temperature at 41˚C, enzyme 30mg/mmol and 72 h of reaction time. At this optimal con...
| Main Authors: | , , , |
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| Format: | Article |
| Language: | English English |
| Published: |
National Institute R and D of Materials Physics
2013
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| Online Access: | http://psasir.upm.edu.my/id/eprint/30014/1/Jatropha%20curcas%20seed%20oil%20as%20new%20substrate%20for%20enzymatic%20methylhydroxylaminolysis.pdf |
| Summary: | Synthesis of methyl fatty hydroxamic acids (MFHAs) was carried out using lipozyme RM
IM based on Jatropha Curcas seed oil. Optimized conditions were obtained at a mole ratio
of 6/1 of methyl hydroxylamine/oil, temperature at 41˚C, enzyme 30mg/mmol and 72 h of
reaction time. At this optimal condition, the yield% of methyl fatty hydroxamic based on
Jatropha Curcas seed oil was 93.92%. The product was characterized by Fourier
transform infrared (FTIR), and proton and carbon nuclear magnetic resonance (¹H-NMR
and ¹³C NMR) spectra. |
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