Synthesis, antibacterial and thermal studies of cellulose nanocrystal stabilized ZnO-Ag heterostructure nanoparticles
Synthesis of ZnO-Ag heterostructure nanoparticles was carried out by a precipitation method with cellulose nanocrystals (CNCs) as a stabilizer for antimicrobial and thermal studies. ZnO-Ag nanoparticles were obtained from various weight percentages of added AgNO3 relative to Zn precursors for evalua...
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Format: | Article |
Language: | English English |
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Multidisciplinary Digital Publishing Institute
2013
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Online Access: | http://psasir.upm.edu.my/id/eprint/30061/1/1Synthesis.pdf |
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author | Azizi, Susan Ahmad, Mansor Hussein, Mohd Zobir Ibrahim, Nor Azowa |
author_facet | Azizi, Susan Ahmad, Mansor Hussein, Mohd Zobir Ibrahim, Nor Azowa |
author_sort | Azizi, Susan |
collection | UPM |
description | Synthesis of ZnO-Ag heterostructure nanoparticles was carried out by a precipitation method with cellulose nanocrystals (CNCs) as a stabilizer for antimicrobial and thermal studies. ZnO-Ag nanoparticles were obtained from various weight percentages of added AgNO3 relative to Zn precursors for evaluating the best composition with enhanced functional properties. The ZnO-Ag/CNCs samples were characterized systematically by TEM, XRD, UV, TGA and DTG. From the TEM studies we observed that ZnO-Ag heterostructure nanoparticles have spherical shapes with size diameters in a 9–35 nm range. The antibacterial activities of samples were assessed against the bacterial species Salmonella choleraesuis and Staphylococcus aureus. The CNC-stabilized ZnO-Ag exhibited greater bactericidal activity compared to cellulose-free ZnO-Ag heterostructure nanoparticles of the same particle size. The incorporation of ZnO-Ag hetreostructure nanoparticles significantly increased the thermal stability of cellulose nanocrystals. |
first_indexed | 2024-03-06T08:16:22Z |
format | Article |
id | upm.eprints-30061 |
institution | Universiti Putra Malaysia |
language | English English |
last_indexed | 2024-03-06T08:16:22Z |
publishDate | 2013 |
publisher | Multidisciplinary Digital Publishing Institute |
record_format | dspace |
spelling | upm.eprints-300612015-09-07T03:37:06Z http://psasir.upm.edu.my/id/eprint/30061/ Synthesis, antibacterial and thermal studies of cellulose nanocrystal stabilized ZnO-Ag heterostructure nanoparticles Azizi, Susan Ahmad, Mansor Hussein, Mohd Zobir Ibrahim, Nor Azowa Synthesis of ZnO-Ag heterostructure nanoparticles was carried out by a precipitation method with cellulose nanocrystals (CNCs) as a stabilizer for antimicrobial and thermal studies. ZnO-Ag nanoparticles were obtained from various weight percentages of added AgNO3 relative to Zn precursors for evaluating the best composition with enhanced functional properties. The ZnO-Ag/CNCs samples were characterized systematically by TEM, XRD, UV, TGA and DTG. From the TEM studies we observed that ZnO-Ag heterostructure nanoparticles have spherical shapes with size diameters in a 9–35 nm range. The antibacterial activities of samples were assessed against the bacterial species Salmonella choleraesuis and Staphylococcus aureus. The CNC-stabilized ZnO-Ag exhibited greater bactericidal activity compared to cellulose-free ZnO-Ag heterostructure nanoparticles of the same particle size. The incorporation of ZnO-Ag hetreostructure nanoparticles significantly increased the thermal stability of cellulose nanocrystals. Multidisciplinary Digital Publishing Institute 2013-06 Article PeerReviewed application/pdf en http://psasir.upm.edu.my/id/eprint/30061/1/1Synthesis.pdf Azizi, Susan and Ahmad, Mansor and Hussein, Mohd Zobir and Ibrahim, Nor Azowa (2013) Synthesis, antibacterial and thermal studies of cellulose nanocrystal stabilized ZnO-Ag heterostructure nanoparticles. Molecules, 18 (5). pp. 6269-6280. ISSN 1420-3049 http://www.mdpi.com/1420-3049/18/6 10.3390/molecules18066269 English |
spellingShingle | Azizi, Susan Ahmad, Mansor Hussein, Mohd Zobir Ibrahim, Nor Azowa Synthesis, antibacterial and thermal studies of cellulose nanocrystal stabilized ZnO-Ag heterostructure nanoparticles |
title | Synthesis, antibacterial and thermal studies of cellulose nanocrystal stabilized ZnO-Ag heterostructure nanoparticles |
title_full | Synthesis, antibacterial and thermal studies of cellulose nanocrystal stabilized ZnO-Ag heterostructure nanoparticles |
title_fullStr | Synthesis, antibacterial and thermal studies of cellulose nanocrystal stabilized ZnO-Ag heterostructure nanoparticles |
title_full_unstemmed | Synthesis, antibacterial and thermal studies of cellulose nanocrystal stabilized ZnO-Ag heterostructure nanoparticles |
title_short | Synthesis, antibacterial and thermal studies of cellulose nanocrystal stabilized ZnO-Ag heterostructure nanoparticles |
title_sort | synthesis antibacterial and thermal studies of cellulose nanocrystal stabilized zno ag heterostructure nanoparticles |
url | http://psasir.upm.edu.my/id/eprint/30061/1/1Synthesis.pdf |
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