Synthesis, antibacterial and thermal studies of cellulose nanocrystal stabilized ZnO-Ag heterostructure nanoparticles

Synthesis of ZnO-Ag heterostructure nanoparticles was carried out by a precipitation method with cellulose nanocrystals (CNCs) as a stabilizer for antimicrobial and thermal studies. ZnO-Ag nanoparticles were obtained from various weight percentages of added AgNO3 relative to Zn precursors for evalua...

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Main Authors: Azizi, Susan, Ahmad, Mansor, Hussein, Mohd Zobir, Ibrahim, Nor Azowa
Format: Article
Language:English
English
Published: Multidisciplinary Digital Publishing Institute 2013
Online Access:http://psasir.upm.edu.my/id/eprint/30061/1/1Synthesis.pdf
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author Azizi, Susan
Ahmad, Mansor
Hussein, Mohd Zobir
Ibrahim, Nor Azowa
author_facet Azizi, Susan
Ahmad, Mansor
Hussein, Mohd Zobir
Ibrahim, Nor Azowa
author_sort Azizi, Susan
collection UPM
description Synthesis of ZnO-Ag heterostructure nanoparticles was carried out by a precipitation method with cellulose nanocrystals (CNCs) as a stabilizer for antimicrobial and thermal studies. ZnO-Ag nanoparticles were obtained from various weight percentages of added AgNO3 relative to Zn precursors for evaluating the best composition with enhanced functional properties. The ZnO-Ag/CNCs samples were characterized systematically by TEM, XRD, UV, TGA and DTG. From the TEM studies we observed that ZnO-Ag heterostructure nanoparticles have spherical shapes with size diameters in a 9–35 nm range. The antibacterial activities of samples were assessed against the bacterial species Salmonella choleraesuis and Staphylococcus aureus. The CNC-stabilized ZnO-Ag exhibited greater bactericidal activity compared to cellulose-free ZnO-Ag heterostructure nanoparticles of the same particle size. The incorporation of ZnO-Ag hetreostructure nanoparticles significantly increased the thermal stability of cellulose nanocrystals.
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spelling upm.eprints-300612015-09-07T03:37:06Z http://psasir.upm.edu.my/id/eprint/30061/ Synthesis, antibacterial and thermal studies of cellulose nanocrystal stabilized ZnO-Ag heterostructure nanoparticles Azizi, Susan Ahmad, Mansor Hussein, Mohd Zobir Ibrahim, Nor Azowa Synthesis of ZnO-Ag heterostructure nanoparticles was carried out by a precipitation method with cellulose nanocrystals (CNCs) as a stabilizer for antimicrobial and thermal studies. ZnO-Ag nanoparticles were obtained from various weight percentages of added AgNO3 relative to Zn precursors for evaluating the best composition with enhanced functional properties. The ZnO-Ag/CNCs samples were characterized systematically by TEM, XRD, UV, TGA and DTG. From the TEM studies we observed that ZnO-Ag heterostructure nanoparticles have spherical shapes with size diameters in a 9–35 nm range. The antibacterial activities of samples were assessed against the bacterial species Salmonella choleraesuis and Staphylococcus aureus. The CNC-stabilized ZnO-Ag exhibited greater bactericidal activity compared to cellulose-free ZnO-Ag heterostructure nanoparticles of the same particle size. The incorporation of ZnO-Ag hetreostructure nanoparticles significantly increased the thermal stability of cellulose nanocrystals. Multidisciplinary Digital Publishing Institute 2013-06 Article PeerReviewed application/pdf en http://psasir.upm.edu.my/id/eprint/30061/1/1Synthesis.pdf Azizi, Susan and Ahmad, Mansor and Hussein, Mohd Zobir and Ibrahim, Nor Azowa (2013) Synthesis, antibacterial and thermal studies of cellulose nanocrystal stabilized ZnO-Ag heterostructure nanoparticles. Molecules, 18 (5). pp. 6269-6280. ISSN 1420-3049 http://www.mdpi.com/1420-3049/18/6 10.3390/molecules18066269 English
spellingShingle Azizi, Susan
Ahmad, Mansor
Hussein, Mohd Zobir
Ibrahim, Nor Azowa
Synthesis, antibacterial and thermal studies of cellulose nanocrystal stabilized ZnO-Ag heterostructure nanoparticles
title Synthesis, antibacterial and thermal studies of cellulose nanocrystal stabilized ZnO-Ag heterostructure nanoparticles
title_full Synthesis, antibacterial and thermal studies of cellulose nanocrystal stabilized ZnO-Ag heterostructure nanoparticles
title_fullStr Synthesis, antibacterial and thermal studies of cellulose nanocrystal stabilized ZnO-Ag heterostructure nanoparticles
title_full_unstemmed Synthesis, antibacterial and thermal studies of cellulose nanocrystal stabilized ZnO-Ag heterostructure nanoparticles
title_short Synthesis, antibacterial and thermal studies of cellulose nanocrystal stabilized ZnO-Ag heterostructure nanoparticles
title_sort synthesis antibacterial and thermal studies of cellulose nanocrystal stabilized zno ag heterostructure nanoparticles
url http://psasir.upm.edu.my/id/eprint/30061/1/1Synthesis.pdf
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AT husseinmohdzobir synthesisantibacterialandthermalstudiesofcellulosenanocrystalstabilizedznoagheterostructurenanoparticles
AT ibrahimnorazowa synthesisantibacterialandthermalstudiesofcellulosenanocrystalstabilizedznoagheterostructurenanoparticles