Preparation and characterisation of PVDF Sr₂.₅Yₒ.₅Fe₅O₁₂ particles composite

Polyvinylidene fluoride (PVDF)-Sr2.5Y0.5Fe5O12 (SrYIG) particles film is investigated under scanning electron microscopy (SEM) technique for its surface morphology and physical compatibility studies. Films were prepared via powdersolution- gel-film phases with magnetic stirring at about 200 r.p.m an...

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Main Authors: Mohd Saad, Mohd Hashim, Yahya, Noorhana, Shafie, Mohd Shamsul Ezzad, Ismail, Ismayadi, Bawa Waje, Samaila, Al-Habashi, Ramadan Masoud, Hashim, Mansor
Format: Conference or Workshop Item
Language:English
Published: Universiti Putra Malaysia Press 2005
Online Access:http://psasir.upm.edu.my/id/eprint/34005/1/34005.pdf
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author Mohd Saad, Mohd Hashim
Yahya, Noorhana
Shafie, Mohd Shamsul Ezzad
Ismail, Ismayadi
Bawa Waje, Samaila
Al-Habashi, Ramadan Masoud
Hashim, Mansor
author_facet Mohd Saad, Mohd Hashim
Yahya, Noorhana
Shafie, Mohd Shamsul Ezzad
Ismail, Ismayadi
Bawa Waje, Samaila
Al-Habashi, Ramadan Masoud
Hashim, Mansor
author_sort Mohd Saad, Mohd Hashim
collection UPM
description Polyvinylidene fluoride (PVDF)-Sr2.5Y0.5Fe5O12 (SrYIG) particles film is investigated under scanning electron microscopy (SEM) technique for its surface morphology and physical compatibility studies. Films were prepared via powdersolution- gel-film phases with magnetic stirring at about 200 r.p.m and heating at about 90°C for 1 hour before the hot gel is poured into a dish for formation of thick film followed with atmospheric cooling for another 24 hours. Four samples were prepared with different SrYIG filler content of 0, 1, 5 and 10 wt%. The thick films were coated with gold for SEM analysis. SEM images were taken with JEOL 6400 scanning electron microscope and energy dispersive X-ray (EDX) analyses were also done with the same equipment. Magnetic characteristics were done on Agilent 4291B RF Impedance/Material Analyzer from 1MHz to 1.8GHz. SEM images showed that PVDF in cyclopentanone has surface that is relatively smooth. PVDF with magnetic fillers lost its smoothness and have granulated-like surface morphology instead. There is no clear evidence that the PVDF rejected the magnetic fillers though EDX analysis does not show existence of magnetic particles in the PVDF films. Magnetic properties of PVDF films were reduced when SrYIG fillers were introduced into the films.
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spelling upm.eprints-340052015-05-08T03:07:24Z http://psasir.upm.edu.my/id/eprint/34005/ Preparation and characterisation of PVDF Sr₂.₅Yₒ.₅Fe₅O₁₂ particles composite Mohd Saad, Mohd Hashim Yahya, Noorhana Shafie, Mohd Shamsul Ezzad Ismail, Ismayadi Bawa Waje, Samaila Al-Habashi, Ramadan Masoud Hashim, Mansor Polyvinylidene fluoride (PVDF)-Sr2.5Y0.5Fe5O12 (SrYIG) particles film is investigated under scanning electron microscopy (SEM) technique for its surface morphology and physical compatibility studies. Films were prepared via powdersolution- gel-film phases with magnetic stirring at about 200 r.p.m and heating at about 90°C for 1 hour before the hot gel is poured into a dish for formation of thick film followed with atmospheric cooling for another 24 hours. Four samples were prepared with different SrYIG filler content of 0, 1, 5 and 10 wt%. The thick films were coated with gold for SEM analysis. SEM images were taken with JEOL 6400 scanning electron microscope and energy dispersive X-ray (EDX) analyses were also done with the same equipment. Magnetic characteristics were done on Agilent 4291B RF Impedance/Material Analyzer from 1MHz to 1.8GHz. SEM images showed that PVDF in cyclopentanone has surface that is relatively smooth. PVDF with magnetic fillers lost its smoothness and have granulated-like surface morphology instead. There is no clear evidence that the PVDF rejected the magnetic fillers though EDX analysis does not show existence of magnetic particles in the PVDF films. Magnetic properties of PVDF films were reduced when SrYIG fillers were introduced into the films. Universiti Putra Malaysia Press 2005 Conference or Workshop Item NonPeerReviewed application/pdf en http://psasir.upm.edu.my/id/eprint/34005/1/34005.pdf Mohd Saad, Mohd Hashim and Yahya, Noorhana and Shafie, Mohd Shamsul Ezzad and Ismail, Ismayadi and Bawa Waje, Samaila and Al-Habashi, Ramadan Masoud and Hashim, Mansor (2005) Preparation and characterisation of PVDF Sr₂.₅Yₒ.₅Fe₅O₁₂ particles composite. In: International Advanced Technology Congress: Conference on Advanced Materials (CAM 2005), 6 - 8 Dec. 2005, Putrajaya, Malaysia. (pp. 557-562).
spellingShingle Mohd Saad, Mohd Hashim
Yahya, Noorhana
Shafie, Mohd Shamsul Ezzad
Ismail, Ismayadi
Bawa Waje, Samaila
Al-Habashi, Ramadan Masoud
Hashim, Mansor
Preparation and characterisation of PVDF Sr₂.₅Yₒ.₅Fe₅O₁₂ particles composite
title Preparation and characterisation of PVDF Sr₂.₅Yₒ.₅Fe₅O₁₂ particles composite
title_full Preparation and characterisation of PVDF Sr₂.₅Yₒ.₅Fe₅O₁₂ particles composite
title_fullStr Preparation and characterisation of PVDF Sr₂.₅Yₒ.₅Fe₅O₁₂ particles composite
title_full_unstemmed Preparation and characterisation of PVDF Sr₂.₅Yₒ.₅Fe₅O₁₂ particles composite
title_short Preparation and characterisation of PVDF Sr₂.₅Yₒ.₅Fe₅O₁₂ particles composite
title_sort preparation and characterisation of pvdf sr₂ ₅yₒ ₅fe₅o₁₂ particles composite
url http://psasir.upm.edu.my/id/eprint/34005/1/34005.pdf
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