Study of thermal diffusivity of Zn/Al layered double hydroxide synthesized with different molar ratio of Zn/Al salts

Thermal diffusivity of zinc-aluminum layered double hydroxides synthesized at different molar ratios of Zn to Al; at pH 7, 8 and 10 were measured using polyvinlidene diflouride (PVDF) photoflash technique. The samples were prepared using Zn (NO3)2 and Al (NO3)3 solutions by dropwise addition of NaOH...

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Main Authors: Ranjbar, Maryam, Shameli, Kamyar, Ahmad @ Ayob, Mansor, Mat Yunus, Wan Mahmood, Hussein, Mohd Zobir, Shameli, Kaveh
Format: Article
Language:English
Published: Institute of Materials Physics 2014
Online Access:http://psasir.upm.edu.my/id/eprint/35512/1/35512.pdf
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author Ranjbar, Maryam
Shameli, Kamyar
Ahmad @ Ayob, Mansor
Mat Yunus, Wan Mahmood
Hussein, Mohd Zobir
Shameli, Kaveh
author_facet Ranjbar, Maryam
Shameli, Kamyar
Ahmad @ Ayob, Mansor
Mat Yunus, Wan Mahmood
Hussein, Mohd Zobir
Shameli, Kaveh
author_sort Ranjbar, Maryam
collection UPM
description Thermal diffusivity of zinc-aluminum layered double hydroxides synthesized at different molar ratios of Zn to Al; at pH 7, 8 and 10 were measured using polyvinlidene diflouride (PVDF) photoflash technique. The samples were prepared using Zn (NO3)2 and Al (NO3)3 solutions by dropwise addition of NaOH solution with vigorous stirring under nitrogen atmosphere. The different ratios of Zn to Al were obtained by changing the molar ratio of Zn (NO3)2 to Al (NO3)3 solutions. The slurry formed was kept at 70 °C in an oil bath shaker for 18 h and then filtered, washed and dried in an oven for another 48 h at 70 °C. A simple photoflash and PVDF transducer were used as light source and thermal wave detector, respectively. All the measurements of thermal diffusivity of Zn-Al layered double hydroxide were carried out at room temperature. Thermal diffusivity for all series of sample prepared at pH=7, 8 and 10 increase from R=3 to R=5. Thermal diffusivity values of zinc-aluminum layered doubled hydroxide synthesized at pH 8 are higher than the values obtained for samples prepared at pH=7 (except for R=5) and at pH 10 are highest than two other series at pH 7 and 8.
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spelling upm.eprints-355122018-10-11T03:53:06Z http://psasir.upm.edu.my/id/eprint/35512/ Study of thermal diffusivity of Zn/Al layered double hydroxide synthesized with different molar ratio of Zn/Al salts Ranjbar, Maryam Shameli, Kamyar Ahmad @ Ayob, Mansor Mat Yunus, Wan Mahmood Hussein, Mohd Zobir Shameli, Kaveh Thermal diffusivity of zinc-aluminum layered double hydroxides synthesized at different molar ratios of Zn to Al; at pH 7, 8 and 10 were measured using polyvinlidene diflouride (PVDF) photoflash technique. The samples were prepared using Zn (NO3)2 and Al (NO3)3 solutions by dropwise addition of NaOH solution with vigorous stirring under nitrogen atmosphere. The different ratios of Zn to Al were obtained by changing the molar ratio of Zn (NO3)2 to Al (NO3)3 solutions. The slurry formed was kept at 70 °C in an oil bath shaker for 18 h and then filtered, washed and dried in an oven for another 48 h at 70 °C. A simple photoflash and PVDF transducer were used as light source and thermal wave detector, respectively. All the measurements of thermal diffusivity of Zn-Al layered double hydroxide were carried out at room temperature. Thermal diffusivity for all series of sample prepared at pH=7, 8 and 10 increase from R=3 to R=5. Thermal diffusivity values of zinc-aluminum layered doubled hydroxide synthesized at pH 8 are higher than the values obtained for samples prepared at pH=7 (except for R=5) and at pH 10 are highest than two other series at pH 7 and 8. Institute of Materials Physics 2014 Article PeerReviewed text en http://psasir.upm.edu.my/id/eprint/35512/1/35512.pdf Ranjbar, Maryam and Shameli, Kamyar and Ahmad @ Ayob, Mansor and Mat Yunus, Wan Mahmood and Hussein, Mohd Zobir and Shameli, Kaveh (2014) Study of thermal diffusivity of Zn/Al layered double hydroxide synthesized with different molar ratio of Zn/Al salts. Digest Journal of Nanomaterials and Biostructures, 9 (2). pp. 585-592. ISSN 1842-3582 http://www.chalcogen.ro/index.php/journals/digest-journal-of-nanomaterials-and-biostructures/8-djnb/37-volume-9-number-2-april-june-2014
spellingShingle Ranjbar, Maryam
Shameli, Kamyar
Ahmad @ Ayob, Mansor
Mat Yunus, Wan Mahmood
Hussein, Mohd Zobir
Shameli, Kaveh
Study of thermal diffusivity of Zn/Al layered double hydroxide synthesized with different molar ratio of Zn/Al salts
title Study of thermal diffusivity of Zn/Al layered double hydroxide synthesized with different molar ratio of Zn/Al salts
title_full Study of thermal diffusivity of Zn/Al layered double hydroxide synthesized with different molar ratio of Zn/Al salts
title_fullStr Study of thermal diffusivity of Zn/Al layered double hydroxide synthesized with different molar ratio of Zn/Al salts
title_full_unstemmed Study of thermal diffusivity of Zn/Al layered double hydroxide synthesized with different molar ratio of Zn/Al salts
title_short Study of thermal diffusivity of Zn/Al layered double hydroxide synthesized with different molar ratio of Zn/Al salts
title_sort study of thermal diffusivity of zn al layered double hydroxide synthesized with different molar ratio of zn al salts
url http://psasir.upm.edu.my/id/eprint/35512/1/35512.pdf
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