Superparamagnetic magnesium ferrite nanoparticles fabricated by a simple, thermal-treatment method
This study investigated the synthesis of magnesium ferrite (MgFe2O4) nanoparticles with cubic symmetry that were prepared by a thermal-treatment method by using a solution that contained poly (vinyl alcohol) (PVA) as a capping agent and Mg and Fe nitrates as alternative sources of metal. Heat treatm...
| Main Authors: | , , , |
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| 格式: | 文件 |
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Elsevier
2014
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| _version_ | 1825948665680756736 |
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| author | Naseri, Mahmoud Goodarz Majles Ara, Mohammad Hossein Saion, Elias Shaari, Abdul Halim |
| author_facet | Naseri, Mahmoud Goodarz Majles Ara, Mohammad Hossein Saion, Elias Shaari, Abdul Halim |
| author_sort | Naseri, Mahmoud Goodarz |
| collection | UPM |
| description | This study investigated the synthesis of magnesium ferrite (MgFe2O4) nanoparticles with cubic symmetry that were prepared by a thermal-treatment method by using a solution that contained poly (vinyl alcohol) (PVA) as a capping agent and Mg and Fe nitrates as alternative sources of metal. Heat treatment was conducted using an electric cylinder furnace in an air atmosphere at temperatures between 673 and 973 K, and magnesium ferrite nanoparticles were produced that had different crystallite sizes ranging from5 to 8 nm. The products were well characterized by X-ray diffraction (XRD), transmission electron microscopy (TEM), field emission scanning electron microscope (FESEM), X-ray analysis (EDXA), and Fourier transform infrared spectroscopy (FT-IR). All the samples calcined from 673 to 973 K exhibited super paramagnetic behavior with unpaired electrons spins, which was confirmed by using a vibrating sample magnetometer (VSM) and electron paramagnetic resonance (EPR) spectroscopy. |
| first_indexed | 2024-03-06T08:32:37Z |
| format | Article |
| id | upm.eprints-35534 |
| institution | Universiti Putra Malaysia |
| last_indexed | 2024-03-06T08:32:37Z |
| publishDate | 2014 |
| publisher | Elsevier |
| record_format | dspace |
| spelling | upm.eprints-355342016-01-14T03:39:42Z http://psasir.upm.edu.my/id/eprint/35534/ Superparamagnetic magnesium ferrite nanoparticles fabricated by a simple, thermal-treatment method Naseri, Mahmoud Goodarz Majles Ara, Mohammad Hossein Saion, Elias Shaari, Abdul Halim This study investigated the synthesis of magnesium ferrite (MgFe2O4) nanoparticles with cubic symmetry that were prepared by a thermal-treatment method by using a solution that contained poly (vinyl alcohol) (PVA) as a capping agent and Mg and Fe nitrates as alternative sources of metal. Heat treatment was conducted using an electric cylinder furnace in an air atmosphere at temperatures between 673 and 973 K, and magnesium ferrite nanoparticles were produced that had different crystallite sizes ranging from5 to 8 nm. The products were well characterized by X-ray diffraction (XRD), transmission electron microscopy (TEM), field emission scanning electron microscope (FESEM), X-ray analysis (EDXA), and Fourier transform infrared spectroscopy (FT-IR). All the samples calcined from 673 to 973 K exhibited super paramagnetic behavior with unpaired electrons spins, which was confirmed by using a vibrating sample magnetometer (VSM) and electron paramagnetic resonance (EPR) spectroscopy. Elsevier 2014-01 Article PeerReviewed Naseri, Mahmoud Goodarz and Majles Ara, Mohammad Hossein and Saion, Elias and Shaari, Abdul Halim (2014) Superparamagnetic magnesium ferrite nanoparticles fabricated by a simple, thermal-treatment method. Journal of Magnetism and Magnetic Materials, 350. pp. 141-147. ISSN 0304-8853 http://www.sciencedirect.com/science/article/pii/S0304885313005970 10.1016/j.jmmm.2013.08.032 |
| spellingShingle | Naseri, Mahmoud Goodarz Majles Ara, Mohammad Hossein Saion, Elias Shaari, Abdul Halim Superparamagnetic magnesium ferrite nanoparticles fabricated by a simple, thermal-treatment method |
| title | Superparamagnetic magnesium ferrite nanoparticles fabricated by a simple, thermal-treatment method |
| title_full | Superparamagnetic magnesium ferrite nanoparticles fabricated by a simple, thermal-treatment method |
| title_fullStr | Superparamagnetic magnesium ferrite nanoparticles fabricated by a simple, thermal-treatment method |
| title_full_unstemmed | Superparamagnetic magnesium ferrite nanoparticles fabricated by a simple, thermal-treatment method |
| title_short | Superparamagnetic magnesium ferrite nanoparticles fabricated by a simple, thermal-treatment method |
| title_sort | superparamagnetic magnesium ferrite nanoparticles fabricated by a simple thermal treatment method |
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