Triethanolamine - solution for rapid hydrothermal synthesis of titanate nanotubes

Titanate nanotubes were prepared by a rapid hydrothermal method in the presence of triethanolamine (TEA) using TiO2 nanoparticles as a precursor. The addition of TEA significantly reduced the formation time of the titanate nanotubes from 24 to 6 h. The crystalline structure of the titanate nanotubes...

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Main Authors: Mohamed Noor, An'amt, Huang, Nay Ming, Radiman, Shahidan, Lim, Hong Ngee, Muhamad, Muhamad Rasat
Format: Article
Published: Penerbit Universiti Kebangsaan Malaysia 2014
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author Mohamed Noor, An'amt
Huang, Nay Ming
Radiman, Shahidan
Lim, Hong Ngee
Muhamad, Muhamad Rasat
author_facet Mohamed Noor, An'amt
Huang, Nay Ming
Radiman, Shahidan
Lim, Hong Ngee
Muhamad, Muhamad Rasat
author_sort Mohamed Noor, An'amt
collection UPM
description Titanate nanotubes were prepared by a rapid hydrothermal method in the presence of triethanolamine (TEA) using TiO2 nanoparticles as a precursor. The addition of TEA significantly reduced the formation time of the titanate nanotubes from 24 to 6 h. The crystalline structure of the titanate nanotubes was revealed to be H2Ti2O5 through the X-ray diffraction (XRD) measurement. The morphology of the titanate nanotubes was confirmed using transmission electron microscopy (TEM) while the surface area was characterized using Brunauer-Emmett-Teller (BET) surface area analysis. The titanate nanotubes produced were several hundred nanometers in length and had an average outer diameter of ~ 11.5 nm, inner diameter of ~5.0 nm, interlayer spacing of 0.93 nm and surface area of >250 m2/g. The photocatalytic activity of the titanate nanotubes was studied using methylene blue as a model dye; the titanate nanotubes showed better photocatalytic performance as compared to TiO2 nanoparticles.
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spelling upm.eprints-358992016-03-03T14:07:49Z http://psasir.upm.edu.my/id/eprint/35899/ Triethanolamine - solution for rapid hydrothermal synthesis of titanate nanotubes Mohamed Noor, An'amt Huang, Nay Ming Radiman, Shahidan Lim, Hong Ngee Muhamad, Muhamad Rasat Titanate nanotubes were prepared by a rapid hydrothermal method in the presence of triethanolamine (TEA) using TiO2 nanoparticles as a precursor. The addition of TEA significantly reduced the formation time of the titanate nanotubes from 24 to 6 h. The crystalline structure of the titanate nanotubes was revealed to be H2Ti2O5 through the X-ray diffraction (XRD) measurement. The morphology of the titanate nanotubes was confirmed using transmission electron microscopy (TEM) while the surface area was characterized using Brunauer-Emmett-Teller (BET) surface area analysis. The titanate nanotubes produced were several hundred nanometers in length and had an average outer diameter of ~ 11.5 nm, inner diameter of ~5.0 nm, interlayer spacing of 0.93 nm and surface area of >250 m2/g. The photocatalytic activity of the titanate nanotubes was studied using methylene blue as a model dye; the titanate nanotubes showed better photocatalytic performance as compared to TiO2 nanoparticles. Penerbit Universiti Kebangsaan Malaysia 2014 Article NonPeerReviewed Mohamed Noor, An'amt and Huang, Nay Ming and Radiman, Shahidan and Lim, Hong Ngee and Muhamad, Muhamad Rasat (2014) Triethanolamine - solution for rapid hydrothermal synthesis of titanate nanotubes. Sains Malaysiana, 43 (1). pp. 137-144. ISSN 0026-6039 http://www.ukm.my/jsm/english_journals/vol43num1_2014/vol43num1_2014p137-144.html
spellingShingle Mohamed Noor, An'amt
Huang, Nay Ming
Radiman, Shahidan
Lim, Hong Ngee
Muhamad, Muhamad Rasat
Triethanolamine - solution for rapid hydrothermal synthesis of titanate nanotubes
title Triethanolamine - solution for rapid hydrothermal synthesis of titanate nanotubes
title_full Triethanolamine - solution for rapid hydrothermal synthesis of titanate nanotubes
title_fullStr Triethanolamine - solution for rapid hydrothermal synthesis of titanate nanotubes
title_full_unstemmed Triethanolamine - solution for rapid hydrothermal synthesis of titanate nanotubes
title_short Triethanolamine - solution for rapid hydrothermal synthesis of titanate nanotubes
title_sort triethanolamine solution for rapid hydrothermal synthesis of titanate nanotubes
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