Comparison of citronella oil extraction methods from Cymbopogon nardus grass by ohmic-heated hydro-distillation, hydro-distillation, and steam distillation

A proposed method for citronella oil extraction was developed with the application of ohmic heated hydro-distillation. The objective was to compare the performance of three different extraction methods, viz. ohmic heated hydro-distillation, hydro-distillation, and steam distillation. The maximum amo...

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Main Authors: Hamzah, Muhammad Hazwan, Che Man, Hasfalina, Zainal Abidin, Zurina, Jamaludin, Hishamuddin
Format: Article
Language:English
Published: North Carolina State University 2014
Online Access:http://psasir.upm.edu.my/id/eprint/36836/1/Comparison%20of%20citronella%20oil%20extraction%20methods%20from%20Cymbopogon%20nardus%20grass%20by%20ohmic.pdf
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author Hamzah, Muhammad Hazwan
Che Man, Hasfalina
Zainal Abidin, Zurina
Jamaludin, Hishamuddin
author_facet Hamzah, Muhammad Hazwan
Che Man, Hasfalina
Zainal Abidin, Zurina
Jamaludin, Hishamuddin
author_sort Hamzah, Muhammad Hazwan
collection UPM
description A proposed method for citronella oil extraction was developed with the application of ohmic heated hydro-distillation. The objective was to compare the performance of three different extraction methods, viz. ohmic heated hydro-distillation, hydro-distillation, and steam distillation. The maximum amount of extracted oil yield by ohmic heated hydro-distillation was 7.64 mL/kWh as compared to hydro-distillation and steam distillation methods that resulted oil yields of 3.87 mL/kWh and 1.69 mL/kWh, respectively. The kinetics of extraction followed a second-order model. Gas chromatography-mass spectrometry analysis found that the major constituents of citronella oil (GC-MS) for the different extraction methods were citronellal, citronellol, and geraniol. Scanning electron microscopy (SEM) of citronella grass provided evidence that the lignocellulosic sources of the extracted citronella oil were schizogenous cavities and cellular lignin. The citronella that had undergone ohmic-heated hydro-distillation and steam distillation showed some microfractures and less cell wall degradation than hydro-distillation. The cell walls were less rigid using ohmic-heated hydro-distillation compared to steam distillation. However, the cell walls of the hydro-distillation sample were less dense and exhibited pronounced swelling, but did not show any microfractures.
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spelling upm.eprints-368362015-09-10T06:17:02Z http://psasir.upm.edu.my/id/eprint/36836/ Comparison of citronella oil extraction methods from Cymbopogon nardus grass by ohmic-heated hydro-distillation, hydro-distillation, and steam distillation Hamzah, Muhammad Hazwan Che Man, Hasfalina Zainal Abidin, Zurina Jamaludin, Hishamuddin A proposed method for citronella oil extraction was developed with the application of ohmic heated hydro-distillation. The objective was to compare the performance of three different extraction methods, viz. ohmic heated hydro-distillation, hydro-distillation, and steam distillation. The maximum amount of extracted oil yield by ohmic heated hydro-distillation was 7.64 mL/kWh as compared to hydro-distillation and steam distillation methods that resulted oil yields of 3.87 mL/kWh and 1.69 mL/kWh, respectively. The kinetics of extraction followed a second-order model. Gas chromatography-mass spectrometry analysis found that the major constituents of citronella oil (GC-MS) for the different extraction methods were citronellal, citronellol, and geraniol. Scanning electron microscopy (SEM) of citronella grass provided evidence that the lignocellulosic sources of the extracted citronella oil were schizogenous cavities and cellular lignin. The citronella that had undergone ohmic-heated hydro-distillation and steam distillation showed some microfractures and less cell wall degradation than hydro-distillation. The cell walls were less rigid using ohmic-heated hydro-distillation compared to steam distillation. However, the cell walls of the hydro-distillation sample were less dense and exhibited pronounced swelling, but did not show any microfractures. North Carolina State University 2014 Article PeerReviewed application/pdf en http://psasir.upm.edu.my/id/eprint/36836/1/Comparison%20of%20citronella%20oil%20extraction%20methods%20from%20Cymbopogon%20nardus%20grass%20by%20ohmic.pdf Hamzah, Muhammad Hazwan and Che Man, Hasfalina and Zainal Abidin, Zurina and Jamaludin, Hishamuddin (2014) Comparison of citronella oil extraction methods from Cymbopogon nardus grass by ohmic-heated hydro-distillation, hydro-distillation, and steam distillation. BioResources, 9 (1). pp. 256-272. ISSN 1930-2126 http://ojs.cnr.ncsu.edu/index.php/BioRes/article/view/BioRes_09_1_256_Hamzah_Citronella_Oil_Extraction_Methods
spellingShingle Hamzah, Muhammad Hazwan
Che Man, Hasfalina
Zainal Abidin, Zurina
Jamaludin, Hishamuddin
Comparison of citronella oil extraction methods from Cymbopogon nardus grass by ohmic-heated hydro-distillation, hydro-distillation, and steam distillation
title Comparison of citronella oil extraction methods from Cymbopogon nardus grass by ohmic-heated hydro-distillation, hydro-distillation, and steam distillation
title_full Comparison of citronella oil extraction methods from Cymbopogon nardus grass by ohmic-heated hydro-distillation, hydro-distillation, and steam distillation
title_fullStr Comparison of citronella oil extraction methods from Cymbopogon nardus grass by ohmic-heated hydro-distillation, hydro-distillation, and steam distillation
title_full_unstemmed Comparison of citronella oil extraction methods from Cymbopogon nardus grass by ohmic-heated hydro-distillation, hydro-distillation, and steam distillation
title_short Comparison of citronella oil extraction methods from Cymbopogon nardus grass by ohmic-heated hydro-distillation, hydro-distillation, and steam distillation
title_sort comparison of citronella oil extraction methods from cymbopogon nardus grass by ohmic heated hydro distillation hydro distillation and steam distillation
url http://psasir.upm.edu.my/id/eprint/36836/1/Comparison%20of%20citronella%20oil%20extraction%20methods%20from%20Cymbopogon%20nardus%20grass%20by%20ohmic.pdf
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