Synthesis and Formation of T11223 and T1223 High-Tc Superconductors

The preparation methods of Tl2Ba2Ca2Cu30,o (T1l223) and Tlo.5Pbo.5Sr1.6Ca.4Cu30g (TI2223) superconductors using a variety of starting compositions and sintering temperatures are discussed. Single-phased Tl2223 with T, between 106 to 109 K can be prepared using T12Ba2C~Cu3010 and Tl1.6Ba2C~4Cu301...

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Main Authors: Yahya, Ahmad Kamal, Abd Shukor, Roslan
Format: Article
Language:English
English
Published: Universiti Putra Malaysia Press 2003
Online Access:http://psasir.upm.edu.my/id/eprint/3825/1/Synthesis_and_Fonnation_of_Tl1223_and.pdf
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author Yahya, Ahmad Kamal
Abd Shukor, Roslan
author_facet Yahya, Ahmad Kamal
Abd Shukor, Roslan
author_sort Yahya, Ahmad Kamal
collection UPM
description The preparation methods of Tl2Ba2Ca2Cu30,o (T1l223) and Tlo.5Pbo.5Sr1.6Ca.4Cu30g (TI2223) superconductors using a variety of starting compositions and sintering temperatures are discussed. Single-phased Tl2223 with T, between 106 to 109 K can be prepared using T12Ba2C~Cu3010 and Tl1.6Ba2C~4Cu3010as starting compositions in a non-closed system by heating around 20 min at 910°C in flowing 02' Samples with Tl1223 major phase (- 70%) can be prepared from Tlo.5Pbo.5SrI.6C~.4Cu30gcomposition with the sample wrapped in gold foil and sintered in flowing oxygen at 940°C for 3 hours.
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spelling upm.eprints-38252013-05-27T07:11:33Z http://psasir.upm.edu.my/id/eprint/3825/ Synthesis and Formation of T11223 and T1223 High-Tc Superconductors Yahya, Ahmad Kamal Abd Shukor, Roslan The preparation methods of Tl2Ba2Ca2Cu30,o (T1l223) and Tlo.5Pbo.5Sr1.6Ca.4Cu30g (TI2223) superconductors using a variety of starting compositions and sintering temperatures are discussed. Single-phased Tl2223 with T, between 106 to 109 K can be prepared using T12Ba2C~Cu3010 and Tl1.6Ba2C~4Cu3010as starting compositions in a non-closed system by heating around 20 min at 910°C in flowing 02' Samples with Tl1223 major phase (- 70%) can be prepared from Tlo.5Pbo.5SrI.6C~.4Cu30gcomposition with the sample wrapped in gold foil and sintered in flowing oxygen at 940°C for 3 hours. Universiti Putra Malaysia Press 2003 Article PeerReviewed application/pdf en http://psasir.upm.edu.my/id/eprint/3825/1/Synthesis_and_Fonnation_of_Tl1223_and.pdf Yahya, Ahmad Kamal and Abd Shukor, Roslan (2003) Synthesis and Formation of T11223 and T1223 High-Tc Superconductors. Pertanika Journal of Science & Technology, 11 (1). pp. 1-7. ISSN 0128-7680 English
spellingShingle Yahya, Ahmad Kamal
Abd Shukor, Roslan
Synthesis and Formation of T11223 and T1223 High-Tc Superconductors
title Synthesis and Formation of T11223 and T1223 High-Tc Superconductors
title_full Synthesis and Formation of T11223 and T1223 High-Tc Superconductors
title_fullStr Synthesis and Formation of T11223 and T1223 High-Tc Superconductors
title_full_unstemmed Synthesis and Formation of T11223 and T1223 High-Tc Superconductors
title_short Synthesis and Formation of T11223 and T1223 High-Tc Superconductors
title_sort synthesis and formation of t11223 and t1223 high tc superconductors
url http://psasir.upm.edu.my/id/eprint/3825/1/Synthesis_and_Fonnation_of_Tl1223_and.pdf
work_keys_str_mv AT yahyaahmadkamal synthesisandformationoft11223andt1223hightcsuperconductors
AT abdshukorroslan synthesisandformationoft11223andt1223hightcsuperconductors