Optimisation of the photonic efficiency of TiO₂ decorated on MWCNTs for Methylene blue photodegradation
MWCNTs/TiO₂ nanocomposite was prepared by oxidising MWCNT in H₂SO₄/HNO₃ then decorating it with TiO₂-p25 nanopowder. The composites were characterised using XRD, TEM, FT-IR PL and UV−vis spectroscopy. The TEM images have shown TiO₂ nanoparticles immobilised onto the sidewalls of the MWCNTs. The UV-v...
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Format: | Article |
Language: | English |
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Public Library of Science
2015
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Online Access: | http://psasir.upm.edu.my/id/eprint/45687/1/Optimisation%20of%20the%20photonic%20efficiency%20of%20TiO%E2%82%82%20decorated%20on%20MWCNTs%20for%20Methylene%20blue%20photodegradation.pdf |
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author | Saion, Elias Shaari, Abdul Halim Al-Hada, Naif Mohammed Keiteb, Aysar Sabah Abdullahi, Nura |
author_facet | Saion, Elias Shaari, Abdul Halim Al-Hada, Naif Mohammed Keiteb, Aysar Sabah Abdullahi, Nura |
author_sort | Saion, Elias |
collection | UPM |
description | MWCNTs/TiO₂ nanocomposite was prepared by oxidising MWCNT in H₂SO₄/HNO₃ then decorating it with TiO₂-p25 nanopowder. The composites were characterised using XRD, TEM, FT-IR PL and UV−vis spectroscopy. The TEM images have shown TiO₂ nanoparticles immobilised onto the sidewalls of the MWCNTs. The UV-vis spectrum confirms that the nanocomposites can significantly absorb more light in the visible regions compared with the commercial TiO₂ (P25). The catalytic activity of these nanocomposites was determined by photooxidation of MB aqueous solution in the presence of visible light. The MWCNTs/TiO₂ (1:3) mass ratio showed maximum degradation efficiency. However, its activity was more favourable in alkaline and a neutral pH than an acidic medium. |
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format | Article |
id | upm.eprints-45687 |
institution | Universiti Putra Malaysia |
language | English |
last_indexed | 2024-03-06T08:58:56Z |
publishDate | 2015 |
publisher | Public Library of Science |
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spelling | upm.eprints-456872021-02-12T09:39:48Z http://psasir.upm.edu.my/id/eprint/45687/ Optimisation of the photonic efficiency of TiO₂ decorated on MWCNTs for Methylene blue photodegradation Saion, Elias Shaari, Abdul Halim Al-Hada, Naif Mohammed Keiteb, Aysar Sabah Abdullahi, Nura MWCNTs/TiO₂ nanocomposite was prepared by oxidising MWCNT in H₂SO₄/HNO₃ then decorating it with TiO₂-p25 nanopowder. The composites were characterised using XRD, TEM, FT-IR PL and UV−vis spectroscopy. The TEM images have shown TiO₂ nanoparticles immobilised onto the sidewalls of the MWCNTs. The UV-vis spectrum confirms that the nanocomposites can significantly absorb more light in the visible regions compared with the commercial TiO₂ (P25). The catalytic activity of these nanocomposites was determined by photooxidation of MB aqueous solution in the presence of visible light. The MWCNTs/TiO₂ (1:3) mass ratio showed maximum degradation efficiency. However, its activity was more favourable in alkaline and a neutral pH than an acidic medium. Public Library of Science 2015 Article PeerReviewed text en http://psasir.upm.edu.my/id/eprint/45687/1/Optimisation%20of%20the%20photonic%20efficiency%20of%20TiO%E2%82%82%20decorated%20on%20MWCNTs%20for%20Methylene%20blue%20photodegradation.pdf Saion, Elias and Shaari, Abdul Halim and Al-Hada, Naif Mohammed and Keiteb, Aysar Sabah and Abdullahi, Nura (2015) Optimisation of the photonic efficiency of TiO₂ decorated on MWCNTs for Methylene blue photodegradation. PLoS ONE, 10 (5). pp. 1-12. ISSN 1932-6203 https://journals.plos.org/plosone/article?id=10.1371/journal.pone.0125511 10.1371/journal.pone.0125511 |
spellingShingle | Saion, Elias Shaari, Abdul Halim Al-Hada, Naif Mohammed Keiteb, Aysar Sabah Abdullahi, Nura Optimisation of the photonic efficiency of TiO₂ decorated on MWCNTs for Methylene blue photodegradation |
title | Optimisation of the photonic efficiency of TiO₂ decorated on MWCNTs for Methylene blue photodegradation |
title_full | Optimisation of the photonic efficiency of TiO₂ decorated on MWCNTs for Methylene blue photodegradation |
title_fullStr | Optimisation of the photonic efficiency of TiO₂ decorated on MWCNTs for Methylene blue photodegradation |
title_full_unstemmed | Optimisation of the photonic efficiency of TiO₂ decorated on MWCNTs for Methylene blue photodegradation |
title_short | Optimisation of the photonic efficiency of TiO₂ decorated on MWCNTs for Methylene blue photodegradation |
title_sort | optimisation of the photonic efficiency of tio₂ decorated on mwcnts for methylene blue photodegradation |
url | http://psasir.upm.edu.my/id/eprint/45687/1/Optimisation%20of%20the%20photonic%20efficiency%20of%20TiO%E2%82%82%20decorated%20on%20MWCNTs%20for%20Methylene%20blue%20photodegradation.pdf |
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