Effect of roasting time and temperature on volatile component profiles during nib roasting of cocoa beans (Theobroma cacao)

The effect of nib roasting time and temperature on volatile component profiles was studied using response surface methodology (RSM) which consisted of two independent variables: time (5–65 min) and temperature (110–170°C). A steam distillation extraction (SDE) method was used to extract and gas chro...

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Main Authors: Selamat, Jinap, Wan Ishak, Wan Rosli, Abdul Rahman, Russly, L. M., Nordin
Format: Article
Language:English
English
Published: SCI 1998
Online Access:http://psasir.upm.edu.my/id/eprint/51675/1/51675.pdf
http://psasir.upm.edu.my/id/eprint/51675/7/J%20Sci%20Food%20Agric%20-%201999%20-%20Jinap%20-%20Effect%20of%20roasting%20time%20and%20temperature%20on%20volatile%20component%20profiles%20during%20nib.pdf
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author Selamat, Jinap
Wan Ishak, Wan Rosli
Abdul Rahman, Russly
L. M., Nordin
author_facet Selamat, Jinap
Wan Ishak, Wan Rosli
Abdul Rahman, Russly
L. M., Nordin
author_sort Selamat, Jinap
collection UPM
description The effect of nib roasting time and temperature on volatile component profiles was studied using response surface methodology (RSM) which consisted of two independent variables: time (5–65 min) and temperature (110–170°C). A steam distillation extraction (SDE) method was used to extract and gas chromatograph–mass spectrometry equipped with an ICIS data system was used to identify the volatile compounds. Tetramethylpyrazine, trimethylpyrazine, phenethyl acetate, isoamyl acetate, 3-methylbutyl acetate, phenylacetaldehyde, benzaldehyde and 2-phenylethanol were present in all treatments. Pyrazine formation increased as roasting time and temperature were increased. The number of pyrazines increased from 4 to 11 and 25, respectively, when roasting, time was increased from 5 to 35 and 65 min at 140°C. The unit area of esters increased (up to 1700–1800) when the roasting time was increased from 15 to 65 min (at 110–120°C). However, the unit area of carbonyls linearly decreased with an increasing roasting temperature at shorter time (5–25 min). The unit area of phenols was enormously reduced at the highest roasting temperature (160–170°C) with longest roasting time (45–65 min) while that of alcohol slightly decreased as roasting time and temperature were increased.
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spelling upm.eprints-516752024-07-23T06:51:51Z http://psasir.upm.edu.my/id/eprint/51675/ Effect of roasting time and temperature on volatile component profiles during nib roasting of cocoa beans (Theobroma cacao) Selamat, Jinap Wan Ishak, Wan Rosli Abdul Rahman, Russly L. M., Nordin The effect of nib roasting time and temperature on volatile component profiles was studied using response surface methodology (RSM) which consisted of two independent variables: time (5–65 min) and temperature (110–170°C). A steam distillation extraction (SDE) method was used to extract and gas chromatograph–mass spectrometry equipped with an ICIS data system was used to identify the volatile compounds. Tetramethylpyrazine, trimethylpyrazine, phenethyl acetate, isoamyl acetate, 3-methylbutyl acetate, phenylacetaldehyde, benzaldehyde and 2-phenylethanol were present in all treatments. Pyrazine formation increased as roasting time and temperature were increased. The number of pyrazines increased from 4 to 11 and 25, respectively, when roasting, time was increased from 5 to 35 and 65 min at 140°C. The unit area of esters increased (up to 1700–1800) when the roasting time was increased from 15 to 65 min (at 110–120°C). However, the unit area of carbonyls linearly decreased with an increasing roasting temperature at shorter time (5–25 min). The unit area of phenols was enormously reduced at the highest roasting temperature (160–170°C) with longest roasting time (45–65 min) while that of alcohol slightly decreased as roasting time and temperature were increased. SCI 1998 Article PeerReviewed text en http://psasir.upm.edu.my/id/eprint/51675/1/51675.pdf text en http://psasir.upm.edu.my/id/eprint/51675/7/J%20Sci%20Food%20Agric%20-%201999%20-%20Jinap%20-%20Effect%20of%20roasting%20time%20and%20temperature%20on%20volatile%20component%20profiles%20during%20nib.pdf Selamat, Jinap and Wan Ishak, Wan Rosli and Abdul Rahman, Russly and L. M., Nordin (1998) Effect of roasting time and temperature on volatile component profiles during nib roasting of cocoa beans (Theobroma cacao). Journal of the Science of Food and Agriculture, 77 (4). pp. 441-448. ISSN 0022-5142, ESSN: 1097-0010 http://onlinelibrary.wiley.com/doi/10.1002/(SICI)1097-0010(199808)77:4%3C441::AID-JSFA46%3E3.0.CO;2-%23/abstract 10.1002/(SICI)1097-0010(199808)77:4<441::AID-JSFA46>3.0.CO;2-#
spellingShingle Selamat, Jinap
Wan Ishak, Wan Rosli
Abdul Rahman, Russly
L. M., Nordin
Effect of roasting time and temperature on volatile component profiles during nib roasting of cocoa beans (Theobroma cacao)
title Effect of roasting time and temperature on volatile component profiles during nib roasting of cocoa beans (Theobroma cacao)
title_full Effect of roasting time and temperature on volatile component profiles during nib roasting of cocoa beans (Theobroma cacao)
title_fullStr Effect of roasting time and temperature on volatile component profiles during nib roasting of cocoa beans (Theobroma cacao)
title_full_unstemmed Effect of roasting time and temperature on volatile component profiles during nib roasting of cocoa beans (Theobroma cacao)
title_short Effect of roasting time and temperature on volatile component profiles during nib roasting of cocoa beans (Theobroma cacao)
title_sort effect of roasting time and temperature on volatile component profiles during nib roasting of cocoa beans theobroma cacao
url http://psasir.upm.edu.my/id/eprint/51675/1/51675.pdf
http://psasir.upm.edu.my/id/eprint/51675/7/J%20Sci%20Food%20Agric%20-%201999%20-%20Jinap%20-%20Effect%20of%20roasting%20time%20and%20temperature%20on%20volatile%20component%20profiles%20during%20nib.pdf
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