Dependence of microstructure and magnetic properties of (Nd,Pr)-(Fe,Ti,C)-B melt-spun ribbon on quenching wheel speed
Melt-spun ribbons with nominal composition of Nd6Pr1Fe76B12Ti4C1 have been prepared at different quenching wheel speeds (5, 7.5, 10 and 15 m/s) and investigated for microstructural and magnetic properties. The asspun ribbons were examined by using x-ray diffractometry (XRD) with Cu-kα radiation and...
Main Authors: | , , |
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Format: | Article |
Language: | English |
Published: |
The Korean Institute of Metals and Materials & Springer
2013
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Online Access: | http://psasir.upm.edu.my/id/eprint/52146/1/Dependence%20of%20microstructure%20and%20magnetic%20properties%20of%20%28Nd%2CPr%29-%28Fe%2CTi%2CC%29-B%20melt-spun%20ribbon%20on%20quenching%20wheel%20speed.pdf |
Summary: | Melt-spun ribbons with nominal composition of Nd6Pr1Fe76B12Ti4C1 have been prepared at different quenching wheel speeds (5, 7.5, 10 and 15 m/s) and investigated for microstructural and magnetic properties. The asspun ribbons were examined by using x-ray diffractometry (XRD) with Cu-kα radiation and differential scanning calorimetry (DSC) and vibrating sample magnetometry (VSM). Based on the results obtained, it was shown that the lower speeds increased the magnetic properties. Hence, a uniform Nd2Fe14B/Fe3B nanocomposite structure with fine soft grains can be developed at an optimum quenching wheel speed of about 5 m/s. Further, it is seen that the higher quenching wheel speed leads to a lower grain size and higher amorphous phase amount. |
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