A novel research on behavior of zinc ferrite nanoparticles in different concentration of poly(vinyl pyrrolidone) (PVP)
Zinc ferrite nanocrystals were prepared from an aqueous solution containing metal nitrates and various of concentrations of poly(vinyl pyrrolidone) (PVP), i.e., 0, 15, 40, and 55 g/L, as a capping agent. To stabilize the particles, they were thermally treated at 873 K, as an optimum calcination temp...
| Main Authors: | , , |
|---|---|
| Format: | Article |
| Language: | English |
| Published: |
MDPI
2014
|
| Online Access: | http://psasir.upm.edu.my/id/eprint/52156/1/52156.pdf |
| _version_ | 1825930670305705984 |
|---|---|
| author | Mohamed Kamari, Halimah Naseri, Mahmoud Goodarz Saion, Elias |
| author_facet | Mohamed Kamari, Halimah Naseri, Mahmoud Goodarz Saion, Elias |
| author_sort | Mohamed Kamari, Halimah |
| collection | UPM |
| description | Zinc ferrite nanocrystals were prepared from an aqueous solution containing metal nitrates and various of concentrations of poly(vinyl pyrrolidone) (PVP), i.e., 0, 15, 40, and 55 g/L, as a capping agent. To stabilize the particles, they were thermally treated at 873 K, as an optimum calcination temperature. The behaviors of the polymeric precursor were analyzed by use of simultaneous thermo-gravimetry (TG) and derivative thermo-gravimetry analyses (DTG). The presence of the crystalline phase in each sample was confirmed by X-ray diffraction (XRD) analysis. The average particle size and the morphology of the nanoparticles were determined by transmission electron microscopy (TEM), and these parameters were found to differ at various concentrations of PVP. Fourier transform infrared spectroscopy (FT-IR) confirmed the presence of metal oxide bands for all the PVP concentrations and confirmed the absence of organic bands for PVP concentrations less than 55 g/L. Measurements of the magnetization value of the zinc ferrite nanoparticles were obtained at room temperature by using a vibrating sample magnetometer (VSM), which showed that, in the absence of PVP, the sample exhibited a paramagnetic behavior while, in the presence of PVP, samples have a super-paramagnetic behavior. |
| first_indexed | 2024-03-06T09:15:04Z |
| format | Article |
| id | upm.eprints-52156 |
| institution | Universiti Putra Malaysia |
| language | English |
| last_indexed | 2024-03-06T09:15:04Z |
| publishDate | 2014 |
| publisher | MDPI |
| record_format | dspace |
| spelling | upm.eprints-521562017-05-05T03:01:58Z http://psasir.upm.edu.my/id/eprint/52156/ A novel research on behavior of zinc ferrite nanoparticles in different concentration of poly(vinyl pyrrolidone) (PVP) Mohamed Kamari, Halimah Naseri, Mahmoud Goodarz Saion, Elias Zinc ferrite nanocrystals were prepared from an aqueous solution containing metal nitrates and various of concentrations of poly(vinyl pyrrolidone) (PVP), i.e., 0, 15, 40, and 55 g/L, as a capping agent. To stabilize the particles, they were thermally treated at 873 K, as an optimum calcination temperature. The behaviors of the polymeric precursor were analyzed by use of simultaneous thermo-gravimetry (TG) and derivative thermo-gravimetry analyses (DTG). The presence of the crystalline phase in each sample was confirmed by X-ray diffraction (XRD) analysis. The average particle size and the morphology of the nanoparticles were determined by transmission electron microscopy (TEM), and these parameters were found to differ at various concentrations of PVP. Fourier transform infrared spectroscopy (FT-IR) confirmed the presence of metal oxide bands for all the PVP concentrations and confirmed the absence of organic bands for PVP concentrations less than 55 g/L. Measurements of the magnetization value of the zinc ferrite nanoparticles were obtained at room temperature by using a vibrating sample magnetometer (VSM), which showed that, in the absence of PVP, the sample exhibited a paramagnetic behavior while, in the presence of PVP, samples have a super-paramagnetic behavior. MDPI 2014 Article PeerReviewed application/pdf en http://psasir.upm.edu.my/id/eprint/52156/1/52156.pdf Mohamed Kamari, Halimah and Naseri, Mahmoud Goodarz and Saion, Elias (2014) A novel research on behavior of zinc ferrite nanoparticles in different concentration of poly(vinyl pyrrolidone) (PVP). Metals, 4 (2). pp. 118-129. ISSN 2075-4701 http://www.mdpi.com/2075-4701/4/2/118 10.3390/met4020118 |
| spellingShingle | Mohamed Kamari, Halimah Naseri, Mahmoud Goodarz Saion, Elias A novel research on behavior of zinc ferrite nanoparticles in different concentration of poly(vinyl pyrrolidone) (PVP) |
| title | A novel research on behavior of zinc ferrite nanoparticles in different concentration of poly(vinyl pyrrolidone) (PVP) |
| title_full | A novel research on behavior of zinc ferrite nanoparticles in different concentration of poly(vinyl pyrrolidone) (PVP) |
| title_fullStr | A novel research on behavior of zinc ferrite nanoparticles in different concentration of poly(vinyl pyrrolidone) (PVP) |
| title_full_unstemmed | A novel research on behavior of zinc ferrite nanoparticles in different concentration of poly(vinyl pyrrolidone) (PVP) |
| title_short | A novel research on behavior of zinc ferrite nanoparticles in different concentration of poly(vinyl pyrrolidone) (PVP) |
| title_sort | novel research on behavior of zinc ferrite nanoparticles in different concentration of poly vinyl pyrrolidone pvp |
| url | http://psasir.upm.edu.my/id/eprint/52156/1/52156.pdf |
| work_keys_str_mv | AT mohamedkamarihalimah anovelresearchonbehaviorofzincferritenanoparticlesindifferentconcentrationofpolyvinylpyrrolidonepvp AT naserimahmoudgoodarz anovelresearchonbehaviorofzincferritenanoparticlesindifferentconcentrationofpolyvinylpyrrolidonepvp AT saionelias anovelresearchonbehaviorofzincferritenanoparticlesindifferentconcentrationofpolyvinylpyrrolidonepvp AT mohamedkamarihalimah novelresearchonbehaviorofzincferritenanoparticlesindifferentconcentrationofpolyvinylpyrrolidonepvp AT naserimahmoudgoodarz novelresearchonbehaviorofzincferritenanoparticlesindifferentconcentrationofpolyvinylpyrrolidonepvp AT saionelias novelresearchonbehaviorofzincferritenanoparticlesindifferentconcentrationofpolyvinylpyrrolidonepvp |