Effect of microwave sintering on microstructural and magnetic properties of strontium hexaferrite using sol-gel technique

The sol–gel method is used to prepared hexaferrite using d-Fructose as a fuel. The effect of sintering temperature on the microstructure of SrFe12O19 ceramics is analyzed. The observed XRD results indicate a well-formed crystalline phase of dense hexagonal SrFe12O19 ceramics. From this analysis, no...

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Những tác giả chính: Kanagesan, Samikannu, Hashim, Mansor, Jesurani, Sinnappan, Thirunavukarasu, Kalaivani, Ismail, Ismayadi, Ahmod, C. S.
Định dạng: Bài viết
Ngôn ngữ:English
Được phát hành: Springer 2013
Truy cập trực tuyến:http://psasir.upm.edu.my/id/eprint/52189/1/Effect%20of%20microwave%20sintering%20on%20microstructural%20and%20magnetic%20properties%20of%20strontium%20hexaferrite%20using%20sol-gel%20technique.pdf
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author Kanagesan, Samikannu
Hashim, Mansor
Jesurani, Sinnappan
Thirunavukarasu, Kalaivani
Ismail, Ismayadi
Ahmod, C. S.
author_facet Kanagesan, Samikannu
Hashim, Mansor
Jesurani, Sinnappan
Thirunavukarasu, Kalaivani
Ismail, Ismayadi
Ahmod, C. S.
author_sort Kanagesan, Samikannu
collection UPM
description The sol–gel method is used to prepared hexaferrite using d-Fructose as a fuel. The effect of sintering temperature on the microstructure of SrFe12O19 ceramics is analyzed. The observed XRD results indicate a well-formed crystalline phase of dense hexagonal SrFe12O19 ceramics. From this analysis, no secondary phases are identified. The microstructure of the sintered single phase M-type ferrites ceramics displays a hexagonal-platelet like morphology. Sintering temperature can markedly affect the grains in sintered ferrite. The sintered product is shown to be dense microstructure with relatively small grains. The maximum sintered density 95 % was obtained at lower temperature of 1,150 °C. In addition, saturation magnetization (50.43 emu/g) and the coercivity (Hc) 5,594.53 Gauss were observed.
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spelling upm.eprints-521892017-06-05T05:03:43Z http://psasir.upm.edu.my/id/eprint/52189/ Effect of microwave sintering on microstructural and magnetic properties of strontium hexaferrite using sol-gel technique Kanagesan, Samikannu Hashim, Mansor Jesurani, Sinnappan Thirunavukarasu, Kalaivani Ismail, Ismayadi Ahmod, C. S. The sol–gel method is used to prepared hexaferrite using d-Fructose as a fuel. The effect of sintering temperature on the microstructure of SrFe12O19 ceramics is analyzed. The observed XRD results indicate a well-formed crystalline phase of dense hexagonal SrFe12O19 ceramics. From this analysis, no secondary phases are identified. The microstructure of the sintered single phase M-type ferrites ceramics displays a hexagonal-platelet like morphology. Sintering temperature can markedly affect the grains in sintered ferrite. The sintered product is shown to be dense microstructure with relatively small grains. The maximum sintered density 95 % was obtained at lower temperature of 1,150 °C. In addition, saturation magnetization (50.43 emu/g) and the coercivity (Hc) 5,594.53 Gauss were observed. Springer 2013 Article PeerReviewed application/pdf en http://psasir.upm.edu.my/id/eprint/52189/1/Effect%20of%20microwave%20sintering%20on%20microstructural%20and%20magnetic%20properties%20of%20strontium%20hexaferrite%20using%20sol-gel%20technique.pdf Kanagesan, Samikannu and Hashim, Mansor and Jesurani, Sinnappan and Thirunavukarasu, Kalaivani and Ismail, Ismayadi and Ahmod, C. S. (2013) Effect of microwave sintering on microstructural and magnetic properties of strontium hexaferrite using sol-gel technique. Journal of Materials Science: Materials in Electronics, 24 (10). pp. 3881-3884. ISSN 0957-4522; ESSN: 1573-482X http://rd.springer.com/article/10.1007/s10854-013-1333-9 10.1007/s10854-013-1333-9
spellingShingle Kanagesan, Samikannu
Hashim, Mansor
Jesurani, Sinnappan
Thirunavukarasu, Kalaivani
Ismail, Ismayadi
Ahmod, C. S.
Effect of microwave sintering on microstructural and magnetic properties of strontium hexaferrite using sol-gel technique
title Effect of microwave sintering on microstructural and magnetic properties of strontium hexaferrite using sol-gel technique
title_full Effect of microwave sintering on microstructural and magnetic properties of strontium hexaferrite using sol-gel technique
title_fullStr Effect of microwave sintering on microstructural and magnetic properties of strontium hexaferrite using sol-gel technique
title_full_unstemmed Effect of microwave sintering on microstructural and magnetic properties of strontium hexaferrite using sol-gel technique
title_short Effect of microwave sintering on microstructural and magnetic properties of strontium hexaferrite using sol-gel technique
title_sort effect of microwave sintering on microstructural and magnetic properties of strontium hexaferrite using sol gel technique
url http://psasir.upm.edu.my/id/eprint/52189/1/Effect%20of%20microwave%20sintering%20on%20microstructural%20and%20magnetic%20properties%20of%20strontium%20hexaferrite%20using%20sol-gel%20technique.pdf
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