Particle morphology and magnetic properties of Ba0.5Sr0.5Fe12O19 powder calcined conventionally and by microwave heating

Barium strontium hexaferrite (Ba0.5Sr0.5Fe12O19-BSF) has been prepared by sol–gel process involving use of d-Fructose as a fuel. The prepared precursor was calcined in two different calcinations techniques conventional and microwave furnace. X-ray powder diffraction studies confirmed the formation o...

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Main Authors: Kanagesan, Samikannu, Hashim, Mansor, Jesurani, Sinnappan, Thirunavukarasu, Kalaivani, Ismail, Ismayadi, Shafie, Mohd Shamsul Ezzad
Format: Article
Language:English
Published: Elsevier 2012
Online Access:http://psasir.upm.edu.my/id/eprint/52218/1/Particle%20morphology%20and%20magnetic%20properties%20of%20Ba0.5Sr0.5Fe12O19%20powder%20calcined%20conventionally%20and%20by%20microwave%20heating.pdf
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author Kanagesan, Samikannu
Hashim, Mansor
Jesurani, Sinnappan
Thirunavukarasu, Kalaivani
Ismail, Ismayadi
Shafie, Mohd Shamsul Ezzad
author_facet Kanagesan, Samikannu
Hashim, Mansor
Jesurani, Sinnappan
Thirunavukarasu, Kalaivani
Ismail, Ismayadi
Shafie, Mohd Shamsul Ezzad
author_sort Kanagesan, Samikannu
collection UPM
description Barium strontium hexaferrite (Ba0.5Sr0.5Fe12O19-BSF) has been prepared by sol–gel process involving use of d-Fructose as a fuel. The prepared precursor was calcined in two different calcinations techniques conventional and microwave furnace. X-ray powder diffraction studies confirmed the formation of single phase Ba0.5Sr0.5Fe12O19. HR-SEM results show the morphology of the particles is hexagonal structures in platelet form. The average particle size of conventionally calcined BSF powder is 100–250 nm and that of microwave calcined powder is 30–100 nm. The broad hysteresis loop reveals that powder is well crystallized and exhibits hard magnetic properties.
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spelling upm.eprints-522182017-06-05T05:05:08Z http://psasir.upm.edu.my/id/eprint/52218/ Particle morphology and magnetic properties of Ba0.5Sr0.5Fe12O19 powder calcined conventionally and by microwave heating Kanagesan, Samikannu Hashim, Mansor Jesurani, Sinnappan Thirunavukarasu, Kalaivani Ismail, Ismayadi Shafie, Mohd Shamsul Ezzad Barium strontium hexaferrite (Ba0.5Sr0.5Fe12O19-BSF) has been prepared by sol–gel process involving use of d-Fructose as a fuel. The prepared precursor was calcined in two different calcinations techniques conventional and microwave furnace. X-ray powder diffraction studies confirmed the formation of single phase Ba0.5Sr0.5Fe12O19. HR-SEM results show the morphology of the particles is hexagonal structures in platelet form. The average particle size of conventionally calcined BSF powder is 100–250 nm and that of microwave calcined powder is 30–100 nm. The broad hysteresis loop reveals that powder is well crystallized and exhibits hard magnetic properties. Elsevier 2012 Article PeerReviewed application/pdf en http://psasir.upm.edu.my/id/eprint/52218/1/Particle%20morphology%20and%20magnetic%20properties%20of%20Ba0.5Sr0.5Fe12O19%20powder%20calcined%20conventionally%20and%20by%20microwave%20heating.pdf Kanagesan, Samikannu and Hashim, Mansor and Jesurani, Sinnappan and Thirunavukarasu, Kalaivani and Ismail, Ismayadi and Shafie, Mohd Shamsul Ezzad (2012) Particle morphology and magnetic properties of Ba0.5Sr0.5Fe12O19 powder calcined conventionally and by microwave heating. Journal of Alloys and Compounds, 543. pp. 49-52. ISSN 0925-8388; ESSN: 1873-4669 http://www.sciencedirect.com/science/article/pii/S0925838812013357 10.1016/j.jallcom.2012.07.118
spellingShingle Kanagesan, Samikannu
Hashim, Mansor
Jesurani, Sinnappan
Thirunavukarasu, Kalaivani
Ismail, Ismayadi
Shafie, Mohd Shamsul Ezzad
Particle morphology and magnetic properties of Ba0.5Sr0.5Fe12O19 powder calcined conventionally and by microwave heating
title Particle morphology and magnetic properties of Ba0.5Sr0.5Fe12O19 powder calcined conventionally and by microwave heating
title_full Particle morphology and magnetic properties of Ba0.5Sr0.5Fe12O19 powder calcined conventionally and by microwave heating
title_fullStr Particle morphology and magnetic properties of Ba0.5Sr0.5Fe12O19 powder calcined conventionally and by microwave heating
title_full_unstemmed Particle morphology and magnetic properties of Ba0.5Sr0.5Fe12O19 powder calcined conventionally and by microwave heating
title_short Particle morphology and magnetic properties of Ba0.5Sr0.5Fe12O19 powder calcined conventionally and by microwave heating
title_sort particle morphology and magnetic properties of ba0 5sr0 5fe12o19 powder calcined conventionally and by microwave heating
url http://psasir.upm.edu.my/id/eprint/52218/1/Particle%20morphology%20and%20magnetic%20properties%20of%20Ba0.5Sr0.5Fe12O19%20powder%20calcined%20conventionally%20and%20by%20microwave%20heating.pdf
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