Physicochemical characterization of microcrystalline cellulose extracted from kenaf bast

Microcrystalline cellulose (MCC) was successfully prepared from bleached kenaf bast fiber through hydrochloric acid hydrolysis. The influence of hydrolysis time (1 to 3 h) on the MCC physicochemical properties was examined. Scanning electron microscopy (SEM), X-ray diffraction (XRD), particle size a...

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Main Authors: N. A., Sri Aprilia, Y., Davoudpour, W., Zulqarnain, H. P. S., Abdul Khalil, C. I., Che Mohamad Hazwan, M. S., Hossain, Dungani, Rudi, H. M., Fizree, A., Zaidon, M. K., Mohamad Haafiz
Format: Article
Language:English
Published: College of Natural Resources, North Carolina State University 2016
Online Access:http://psasir.upm.edu.my/id/eprint/53578/1/Physicochemical%20characterization%20of%20microcrystalline%20cellulose%20extracted%20from%20kenaf%20bast.pdf
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author N. A., Sri Aprilia
Y., Davoudpour
W., Zulqarnain
H. P. S., Abdul Khalil
C. I., Che Mohamad Hazwan
M. S., Hossain
Dungani, Rudi
H. M., Fizree
A., Zaidon
M. K., Mohamad Haafiz
author_facet N. A., Sri Aprilia
Y., Davoudpour
W., Zulqarnain
H. P. S., Abdul Khalil
C. I., Che Mohamad Hazwan
M. S., Hossain
Dungani, Rudi
H. M., Fizree
A., Zaidon
M. K., Mohamad Haafiz
author_sort N. A., Sri Aprilia
collection UPM
description Microcrystalline cellulose (MCC) was successfully prepared from bleached kenaf bast fiber through hydrochloric acid hydrolysis. The influence of hydrolysis time (1 to 3 h) on the MCC physicochemical properties was examined. Scanning electron microscopy (SEM), X-ray diffraction (XRD), particle size analysis, Fourier transform infrared spectroscopy (FT-IR), and thermal gravimetric analysis (TGA) were utilized to characterize the isolated MCC. According to FTIR analysis, the chemical composition of MCC was not changed with the reaction time. The reaction times, however, did affect the thermal stability of MCC. The thermal stability decreased linearly with increasing hydrolysis time. The optimum hydrolysis time was determined based on the morphological, structural, and thermal properties of the kenaf bast MCC.
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spelling upm.eprints-535782022-03-18T01:47:50Z http://psasir.upm.edu.my/id/eprint/53578/ Physicochemical characterization of microcrystalline cellulose extracted from kenaf bast N. A., Sri Aprilia Y., Davoudpour W., Zulqarnain H. P. S., Abdul Khalil C. I., Che Mohamad Hazwan M. S., Hossain Dungani, Rudi H. M., Fizree A., Zaidon M. K., Mohamad Haafiz Microcrystalline cellulose (MCC) was successfully prepared from bleached kenaf bast fiber through hydrochloric acid hydrolysis. The influence of hydrolysis time (1 to 3 h) on the MCC physicochemical properties was examined. Scanning electron microscopy (SEM), X-ray diffraction (XRD), particle size analysis, Fourier transform infrared spectroscopy (FT-IR), and thermal gravimetric analysis (TGA) were utilized to characterize the isolated MCC. According to FTIR analysis, the chemical composition of MCC was not changed with the reaction time. The reaction times, however, did affect the thermal stability of MCC. The thermal stability decreased linearly with increasing hydrolysis time. The optimum hydrolysis time was determined based on the morphological, structural, and thermal properties of the kenaf bast MCC. College of Natural Resources, North Carolina State University 2016 Article PeerReviewed text en http://psasir.upm.edu.my/id/eprint/53578/1/Physicochemical%20characterization%20of%20microcrystalline%20cellulose%20extracted%20from%20kenaf%20bast.pdf N. A., Sri Aprilia and Y., Davoudpour and W., Zulqarnain and H. P. S., Abdul Khalil and C. I., Che Mohamad Hazwan and M. S., Hossain and Dungani, Rudi and H. M., Fizree and A., Zaidon and M. K., Mohamad Haafiz (2016) Physicochemical characterization of microcrystalline cellulose extracted from kenaf bast. BioResources, 11 (2). pp. 3875-3889. ISSN 1930-2126 https://ojs.cnr.ncsu.edu/index.php/BioRes/article/view/8860 10.15376/biores.11.2.3875-3889
spellingShingle N. A., Sri Aprilia
Y., Davoudpour
W., Zulqarnain
H. P. S., Abdul Khalil
C. I., Che Mohamad Hazwan
M. S., Hossain
Dungani, Rudi
H. M., Fizree
A., Zaidon
M. K., Mohamad Haafiz
Physicochemical characterization of microcrystalline cellulose extracted from kenaf bast
title Physicochemical characterization of microcrystalline cellulose extracted from kenaf bast
title_full Physicochemical characterization of microcrystalline cellulose extracted from kenaf bast
title_fullStr Physicochemical characterization of microcrystalline cellulose extracted from kenaf bast
title_full_unstemmed Physicochemical characterization of microcrystalline cellulose extracted from kenaf bast
title_short Physicochemical characterization of microcrystalline cellulose extracted from kenaf bast
title_sort physicochemical characterization of microcrystalline cellulose extracted from kenaf bast
url http://psasir.upm.edu.my/id/eprint/53578/1/Physicochemical%20characterization%20of%20microcrystalline%20cellulose%20extracted%20from%20kenaf%20bast.pdf
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