Preparation of carbon nanotubes via chemical technique (modified Staudenmaier method)
The chemical method is one of the most promising routes for the production of multi-walled carbon nanotubes. In this study, multi-walled carbon nanotubes (MWCNTs) were successfully synthesized by the modified Staudenmaier method. MWCNTs were synthesized using graphite powder at room temperature. Thi...
| Main Authors: | , , , , , , |
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| Format: | Article |
| Language: | English |
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Bentham Science Publishers
2017
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| Online Access: | http://psasir.upm.edu.my/id/eprint/53655/1/Preparation%20of%20carbon%20nanotubes%20.pdf |
| _version_ | 1825930892899516416 |
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| author | Al-Timimi, Buthainah Ali Abed Awang Biak, Dayang Radiah Salit, Mohd Sapuan Abdul Wahab, Zaidan Alnuaimi, Wadhah Noori Humadi Mohamed Yusoff, Hamdan Tasirin, Siti Masrinda |
| author_facet | Al-Timimi, Buthainah Ali Abed Awang Biak, Dayang Radiah Salit, Mohd Sapuan Abdul Wahab, Zaidan Alnuaimi, Wadhah Noori Humadi Mohamed Yusoff, Hamdan Tasirin, Siti Masrinda |
| author_sort | Al-Timimi, Buthainah Ali Abed |
| collection | UPM |
| description | The chemical method is one of the most promising routes for the production of multi-walled carbon nanotubes. In this study, multi-walled carbon nanotubes (MWCNTs) were successfully synthesized by the modified Staudenmaier method. MWCNTs were synthesized using graphite powder at room temperature. This process does not utilize any metal catalyst. The prepared multi-walled carbon nanotubes were characterized for their crystalline, structural and thermal stability properties. The structural, crystalline and morphological characterization of The produced MWCNTs were performed by using scanning electron microscopy(SEM), transmission electron microscopy(TEM), X-ray diffraction (XRD), thermogravimetric analysis(TGA), Raman analysis, and atomic force microscopy( AFM). Crystallinity and graphitization degree was observed for the produced MWCNTs have a diameter of 13.1 nm. The yield is approximately 10% of the carbon source (graphite). Moreover, the obtained MWCNTs have high thermal stability and oxidation resistance lower than 401.80 °C. The present approach provides a simple low cost and easy method of MWCNTs synthesis. |
| first_indexed | 2024-03-06T09:18:28Z |
| format | Article |
| id | upm.eprints-53655 |
| institution | Universiti Putra Malaysia |
| language | English |
| last_indexed | 2024-03-06T09:18:28Z |
| publishDate | 2017 |
| publisher | Bentham Science Publishers |
| record_format | dspace |
| spelling | upm.eprints-536552019-11-06T08:33:10Z http://psasir.upm.edu.my/id/eprint/53655/ Preparation of carbon nanotubes via chemical technique (modified Staudenmaier method) Al-Timimi, Buthainah Ali Abed Awang Biak, Dayang Radiah Salit, Mohd Sapuan Abdul Wahab, Zaidan Alnuaimi, Wadhah Noori Humadi Mohamed Yusoff, Hamdan Tasirin, Siti Masrinda The chemical method is one of the most promising routes for the production of multi-walled carbon nanotubes. In this study, multi-walled carbon nanotubes (MWCNTs) were successfully synthesized by the modified Staudenmaier method. MWCNTs were synthesized using graphite powder at room temperature. This process does not utilize any metal catalyst. The prepared multi-walled carbon nanotubes were characterized for their crystalline, structural and thermal stability properties. The structural, crystalline and morphological characterization of The produced MWCNTs were performed by using scanning electron microscopy(SEM), transmission electron microscopy(TEM), X-ray diffraction (XRD), thermogravimetric analysis(TGA), Raman analysis, and atomic force microscopy( AFM). Crystallinity and graphitization degree was observed for the produced MWCNTs have a diameter of 13.1 nm. The yield is approximately 10% of the carbon source (graphite). Moreover, the obtained MWCNTs have high thermal stability and oxidation resistance lower than 401.80 °C. The present approach provides a simple low cost and easy method of MWCNTs synthesis. Bentham Science Publishers 2017 Article PeerReviewed application/pdf en http://psasir.upm.edu.my/id/eprint/53655/1/Preparation%20of%20carbon%20nanotubes%20.pdf Al-Timimi, Buthainah Ali Abed and Awang Biak, Dayang Radiah and Salit, Mohd Sapuan and Abdul Wahab, Zaidan and Alnuaimi, Wadhah Noori Humadi and Mohamed Yusoff, Hamdan and Tasirin, Siti Masrinda (2017) Preparation of carbon nanotubes via chemical technique (modified Staudenmaier method). Nanoscience & Nanotechnology Asia, 7 (1). pp. 113-122. ISSN 2210-6812; ESSN: 2210-6820 http://www.eurekaselect.com/143860/article 10.2174/2210681206666160711161421 |
| spellingShingle | Al-Timimi, Buthainah Ali Abed Awang Biak, Dayang Radiah Salit, Mohd Sapuan Abdul Wahab, Zaidan Alnuaimi, Wadhah Noori Humadi Mohamed Yusoff, Hamdan Tasirin, Siti Masrinda Preparation of carbon nanotubes via chemical technique (modified Staudenmaier method) |
| title | Preparation of carbon nanotubes via chemical technique (modified Staudenmaier method) |
| title_full | Preparation of carbon nanotubes via chemical technique (modified Staudenmaier method) |
| title_fullStr | Preparation of carbon nanotubes via chemical technique (modified Staudenmaier method) |
| title_full_unstemmed | Preparation of carbon nanotubes via chemical technique (modified Staudenmaier method) |
| title_short | Preparation of carbon nanotubes via chemical technique (modified Staudenmaier method) |
| title_sort | preparation of carbon nanotubes via chemical technique modified staudenmaier method |
| url | http://psasir.upm.edu.my/id/eprint/53655/1/Preparation%20of%20carbon%20nanotubes%20.pdf |
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