Crystal structure of methyl-N′-[1-(thiophen-2-yl) propylidene] hydrazinecarbodithioate
The title compound, C9H12N2S3, was obtained from a condensation reaction between S-methyldithiocarbazate and 1-(2-thienyl)-1-propane. The compound crystallized in the monoclinic space group P21/n with cell parameters a = 10.178(3), b = 13.357(4), c = 8.845(3)Å, β =98.613(5)°, Z = 4 and V = 1188.9(6...
| Main Authors: | , , , |
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| Format: | Article |
| Language: | English |
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Nihon Bunseki Kagakkai, Japan Society for Analytical Chemistry
2017
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| Online Access: | http://psasir.upm.edu.my/id/eprint/61263/1/Crystal%20structure%20of%20methyl-N%E2%80%B2-%5B1-%28thiophen-2-yl%29%20propylidene%5D%20hydrazinecarbodithioate.pdf |
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| author | M. Osman, Uwaisulqarni Mohamed Tahir, Mohamed Ibrahim Crouse, Karen Anne Ravoof, Thahira Begum S. A. |
| author_facet | M. Osman, Uwaisulqarni Mohamed Tahir, Mohamed Ibrahim Crouse, Karen Anne Ravoof, Thahira Begum S. A. |
| author_sort | M. Osman, Uwaisulqarni |
| collection | UPM |
| description | The title compound, C9H12N2S3, was obtained from a condensation reaction between S-methyldithiocarbazate and 1-(2-thienyl)-1-propane. The compound crystallized in the monoclinic space group P21/n with cell parameters a = 10.178(3), b = 13.357(4), c = 8.845(3)Å, β =98.613(5)°, Z = 4 and V = 1188.9(6)Å3. The compound was nearly planar with intermolecular N–H···S hydrogen bonding observed in the crystal lattice. |
| first_indexed | 2024-03-06T09:40:08Z |
| format | Article |
| id | upm.eprints-61263 |
| institution | Universiti Putra Malaysia |
| language | English |
| last_indexed | 2024-03-06T09:40:08Z |
| publishDate | 2017 |
| publisher | Nihon Bunseki Kagakkai, Japan Society for Analytical Chemistry |
| record_format | dspace |
| spelling | upm.eprints-612632022-03-04T07:52:21Z http://psasir.upm.edu.my/id/eprint/61263/ Crystal structure of methyl-N′-[1-(thiophen-2-yl) propylidene] hydrazinecarbodithioate M. Osman, Uwaisulqarni Mohamed Tahir, Mohamed Ibrahim Crouse, Karen Anne Ravoof, Thahira Begum S. A. The title compound, C9H12N2S3, was obtained from a condensation reaction between S-methyldithiocarbazate and 1-(2-thienyl)-1-propane. The compound crystallized in the monoclinic space group P21/n with cell parameters a = 10.178(3), b = 13.357(4), c = 8.845(3)Å, β =98.613(5)°, Z = 4 and V = 1188.9(6)Å3. The compound was nearly planar with intermolecular N–H···S hydrogen bonding observed in the crystal lattice. Nihon Bunseki Kagakkai, Japan Society for Analytical Chemistry 2017 Article PeerReviewed text en http://psasir.upm.edu.my/id/eprint/61263/1/Crystal%20structure%20of%20methyl-N%E2%80%B2-%5B1-%28thiophen-2-yl%29%20propylidene%5D%20hydrazinecarbodithioate.pdf M. Osman, Uwaisulqarni and Mohamed Tahir, Mohamed Ibrahim and Crouse, Karen Anne and Ravoof, Thahira Begum S. A. (2017) Crystal structure of methyl-N′-[1-(thiophen-2-yl) propylidene] hydrazinecarbodithioate. X-ray Structure Analysis Online, 33 (9). 57 - 58. ISSN 1883-3578 (Unpublished) https://www.jstage.jst.go.jp/article/xraystruct/33/0/33_57/_article 10.2116/xraystruct.33.57 |
| spellingShingle | M. Osman, Uwaisulqarni Mohamed Tahir, Mohamed Ibrahim Crouse, Karen Anne Ravoof, Thahira Begum S. A. Crystal structure of methyl-N′-[1-(thiophen-2-yl) propylidene] hydrazinecarbodithioate |
| title | Crystal structure of methyl-N′-[1-(thiophen-2-yl) propylidene] hydrazinecarbodithioate |
| title_full | Crystal structure of methyl-N′-[1-(thiophen-2-yl) propylidene] hydrazinecarbodithioate |
| title_fullStr | Crystal structure of methyl-N′-[1-(thiophen-2-yl) propylidene] hydrazinecarbodithioate |
| title_full_unstemmed | Crystal structure of methyl-N′-[1-(thiophen-2-yl) propylidene] hydrazinecarbodithioate |
| title_short | Crystal structure of methyl-N′-[1-(thiophen-2-yl) propylidene] hydrazinecarbodithioate |
| title_sort | crystal structure of methyl n 1 thiophen 2 yl propylidene hydrazinecarbodithioate |
| url | http://psasir.upm.edu.my/id/eprint/61263/1/Crystal%20structure%20of%20methyl-N%E2%80%B2-%5B1-%28thiophen-2-yl%29%20propylidene%5D%20hydrazinecarbodithioate.pdf |
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