H2 sensor based on tapered optical fiber coated with MnO2 nanostructures

A novel hydrogen (H2) sensor was developed using optical fiber coated with manganese dioxide (MnO2) nanostructures. Optical multimode fiber (MMF) of 125 μm in diameter as the transducing platform was tapered to 20 μm to enhance the evanescent field of the light propagates in the fiber core. The tape...

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Main Authors: Mohd Yahya, Nor Akmar, Yusof Hamid, Mohd Rashid, Ibrahim, Siti Azlida, Ong, Boon Hoong, Abdul Rahman, Norizah, Md Zain, Ahmad Rifqi, Mahdi, Mohd Adzir, Yaacob, Mohd Hanif
Format: Article
Language:English
Published: Elsevier 2017
Online Access:http://psasir.upm.edu.my/id/eprint/62001/1/H2%20sensor%20based%20on%20tapered%20optical%20fiber%20coated%20with%20MnO2%20nanostructures.pdf
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author Mohd Yahya, Nor Akmar
Yusof Hamid, Mohd Rashid
Ibrahim, Siti Azlida
Ong, Boon Hoong
Abdul Rahman, Norizah
Md Zain, Ahmad Rifqi
Mahdi, Mohd Adzir
Yaacob, Mohd Hanif
author_facet Mohd Yahya, Nor Akmar
Yusof Hamid, Mohd Rashid
Ibrahim, Siti Azlida
Ong, Boon Hoong
Abdul Rahman, Norizah
Md Zain, Ahmad Rifqi
Mahdi, Mohd Adzir
Yaacob, Mohd Hanif
author_sort Mohd Yahya, Nor Akmar
collection UPM
description A novel hydrogen (H2) sensor was developed using optical fiber coated with manganese dioxide (MnO2) nanostructures. Optical multimode fiber (MMF) of 125 μm in diameter as the transducing platform was tapered to 20 μm to enhance the evanescent field of the light propagates in the fiber core. The tapered fiber was coated with MnO2 nanograins synthesised via chemical bath deposition (CBD) process. Catalytic Palladium (Pd) was sputtered onto the MnO2 layer to improve the H2detection. The sensing layer was characterized through Field Emission Scanning Electron Microscopy (FESEM), Energy Dispersive X-ray (EDX), X-ray Diffraction (XRD) and Raman Spectroscopy to verify the properties of MnO2. Two sets of sensors consist of as-prepared MnO2 and 200 °C annealed MnO2 were tested towards H2 gas. The tapered optical fiber coated with Pd/MnO2 nanograins was found to be sensitive towards H2with different concentrations in synthetic air at 240 °C operating temperature. The annealed sensor showed higher response and sensitivity as compared to the as-prepared sensors when measured in the visible to near infra-red optical wavelength range. The absorbance response of the annealed Pd/MnO2 on fiber has increased to 65% as compared to 20% for the as-prepared Pd/MnO2 upon exposure to 1% H2in synthetic air.
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spelling upm.eprints-620012019-03-14T08:35:31Z http://psasir.upm.edu.my/id/eprint/62001/ H2 sensor based on tapered optical fiber coated with MnO2 nanostructures Mohd Yahya, Nor Akmar Yusof Hamid, Mohd Rashid Ibrahim, Siti Azlida Ong, Boon Hoong Abdul Rahman, Norizah Md Zain, Ahmad Rifqi Mahdi, Mohd Adzir Yaacob, Mohd Hanif A novel hydrogen (H2) sensor was developed using optical fiber coated with manganese dioxide (MnO2) nanostructures. Optical multimode fiber (MMF) of 125 μm in diameter as the transducing platform was tapered to 20 μm to enhance the evanescent field of the light propagates in the fiber core. The tapered fiber was coated with MnO2 nanograins synthesised via chemical bath deposition (CBD) process. Catalytic Palladium (Pd) was sputtered onto the MnO2 layer to improve the H2detection. The sensing layer was characterized through Field Emission Scanning Electron Microscopy (FESEM), Energy Dispersive X-ray (EDX), X-ray Diffraction (XRD) and Raman Spectroscopy to verify the properties of MnO2. Two sets of sensors consist of as-prepared MnO2 and 200 °C annealed MnO2 were tested towards H2 gas. The tapered optical fiber coated with Pd/MnO2 nanograins was found to be sensitive towards H2with different concentrations in synthetic air at 240 °C operating temperature. The annealed sensor showed higher response and sensitivity as compared to the as-prepared sensors when measured in the visible to near infra-red optical wavelength range. The absorbance response of the annealed Pd/MnO2 on fiber has increased to 65% as compared to 20% for the as-prepared Pd/MnO2 upon exposure to 1% H2in synthetic air. Elsevier 2017-07 Article PeerReviewed text en http://psasir.upm.edu.my/id/eprint/62001/1/H2%20sensor%20based%20on%20tapered%20optical%20fiber%20coated%20with%20MnO2%20nanostructures.pdf Mohd Yahya, Nor Akmar and Yusof Hamid, Mohd Rashid and Ibrahim, Siti Azlida and Ong, Boon Hoong and Abdul Rahman, Norizah and Md Zain, Ahmad Rifqi and Mahdi, Mohd Adzir and Yaacob, Mohd Hanif (2017) H2 sensor based on tapered optical fiber coated with MnO2 nanostructures. Sensors and Actuators B: Chemical, 246. pp. 421-427. ISSN 0925-4005; ESSN: 1873-3077 https://www.sciencedirect.com/science/article/pii/S0925400517303118 10.1016/j.snb.2017.02.084
spellingShingle Mohd Yahya, Nor Akmar
Yusof Hamid, Mohd Rashid
Ibrahim, Siti Azlida
Ong, Boon Hoong
Abdul Rahman, Norizah
Md Zain, Ahmad Rifqi
Mahdi, Mohd Adzir
Yaacob, Mohd Hanif
H2 sensor based on tapered optical fiber coated with MnO2 nanostructures
title H2 sensor based on tapered optical fiber coated with MnO2 nanostructures
title_full H2 sensor based on tapered optical fiber coated with MnO2 nanostructures
title_fullStr H2 sensor based on tapered optical fiber coated with MnO2 nanostructures
title_full_unstemmed H2 sensor based on tapered optical fiber coated with MnO2 nanostructures
title_short H2 sensor based on tapered optical fiber coated with MnO2 nanostructures
title_sort h2 sensor based on tapered optical fiber coated with mno2 nanostructures
url http://psasir.upm.edu.my/id/eprint/62001/1/H2%20sensor%20based%20on%20tapered%20optical%20fiber%20coated%20with%20MnO2%20nanostructures.pdf
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