High performance enzymatic synthesis of oleyl oleate using immobilised lipase from Candida antartica
High performance enzymatic synthesis of oleyl oleate, a liquid wax ester was carried out by lipase-catalysed esterification of oleic acid and oleyl alcohol. Various reaction parameters were optimised to obtain high yield of oleyl oleate. The optimum condition to produce oleyl oleate was reaction tim...
| Main Authors: | , , , , , , |
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| Format: | Article |
| Language: | English |
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Pontificia Universidad Católica de Valparaíso
2005
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| Online Access: | http://psasir.upm.edu.my/id/eprint/7056/1/High%20performance%20enzymatic%20synthesis%20of%20oleyl%20oleate%20using%20immobilised%20lipase%20from%20Candida%20antartica.pdf |
| _version_ | 1825944133778276352 |
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| author | Mat Radzi, Salina Basri, Mahiran Salleh, Abu Bakar Ariff, Arbakariya Mohammad, Rosfarizan Abdul Rahman, Mohd Basyaruddin Raja Abdul Rahman, Raja Noor Zaliha |
| author_facet | Mat Radzi, Salina Basri, Mahiran Salleh, Abu Bakar Ariff, Arbakariya Mohammad, Rosfarizan Abdul Rahman, Mohd Basyaruddin Raja Abdul Rahman, Raja Noor Zaliha |
| author_sort | Mat Radzi, Salina |
| collection | UPM |
| description | High performance enzymatic synthesis of oleyl oleate, a liquid wax ester was carried out by lipase-catalysed esterification of oleic acid and oleyl alcohol. Various reaction parameters were optimised to obtain high yield of oleyl oleate. The optimum condition to produce oleyl oleate was reaction time; 5 min, organic solvents of log P ≥ 3.5, temperature; 40-50ºC, amount of enzyme; 0.2-0.4 g and molar ratio of oleyl alcohol to oleic acid; 2:1. The operational stability of enzyme was maintained at >90% yield up to 9 cycles. Analysis of the yield of the product showed that at optimum conditions, >95% liquid wax esters were produced. |
| first_indexed | 2024-03-06T07:11:07Z |
| format | Article |
| id | upm.eprints-7056 |
| institution | Universiti Putra Malaysia |
| language | English |
| last_indexed | 2024-03-06T07:11:07Z |
| publishDate | 2005 |
| publisher | Pontificia Universidad Católica de Valparaíso |
| record_format | dspace |
| spelling | upm.eprints-70562016-09-28T02:58:31Z http://psasir.upm.edu.my/id/eprint/7056/ High performance enzymatic synthesis of oleyl oleate using immobilised lipase from Candida antartica Mat Radzi, Salina Basri, Mahiran Salleh, Abu Bakar Ariff, Arbakariya Mohammad, Rosfarizan Abdul Rahman, Mohd Basyaruddin Raja Abdul Rahman, Raja Noor Zaliha High performance enzymatic synthesis of oleyl oleate, a liquid wax ester was carried out by lipase-catalysed esterification of oleic acid and oleyl alcohol. Various reaction parameters were optimised to obtain high yield of oleyl oleate. The optimum condition to produce oleyl oleate was reaction time; 5 min, organic solvents of log P ≥ 3.5, temperature; 40-50ºC, amount of enzyme; 0.2-0.4 g and molar ratio of oleyl alcohol to oleic acid; 2:1. The operational stability of enzyme was maintained at >90% yield up to 9 cycles. Analysis of the yield of the product showed that at optimum conditions, >95% liquid wax esters were produced. Pontificia Universidad Católica de Valparaíso 2005-12-15 Article PeerReviewed application/pdf en http://psasir.upm.edu.my/id/eprint/7056/1/High%20performance%20enzymatic%20synthesis%20of%20oleyl%20oleate%20using%20immobilised%20lipase%20from%20Candida%20antartica.pdf Mat Radzi, Salina and Basri, Mahiran and Salleh, Abu Bakar and Ariff, Arbakariya and Mohammad, Rosfarizan and Abdul Rahman, Mohd Basyaruddin and Raja Abdul Rahman, Raja Noor Zaliha (2005) High performance enzymatic synthesis of oleyl oleate using immobilised lipase from Candida antartica. Electronic Journal of Biotechnology, 8 (3). pp. 291-298. ISSN 0717-3458 http://www.ejbiotechnology.info/index.php/ejbiotechnology/article/view/v8n3-4 10.2225/vol8-issue3-fulltext-4 |
| spellingShingle | Mat Radzi, Salina Basri, Mahiran Salleh, Abu Bakar Ariff, Arbakariya Mohammad, Rosfarizan Abdul Rahman, Mohd Basyaruddin Raja Abdul Rahman, Raja Noor Zaliha High performance enzymatic synthesis of oleyl oleate using immobilised lipase from Candida antartica |
| title | High performance enzymatic synthesis of oleyl oleate using immobilised lipase from Candida antartica |
| title_full | High performance enzymatic synthesis of oleyl oleate using immobilised lipase from Candida antartica |
| title_fullStr | High performance enzymatic synthesis of oleyl oleate using immobilised lipase from Candida antartica |
| title_full_unstemmed | High performance enzymatic synthesis of oleyl oleate using immobilised lipase from Candida antartica |
| title_short | High performance enzymatic synthesis of oleyl oleate using immobilised lipase from Candida antartica |
| title_sort | high performance enzymatic synthesis of oleyl oleate using immobilised lipase from candida antartica |
| url | http://psasir.upm.edu.my/id/eprint/7056/1/High%20performance%20enzymatic%20synthesis%20of%20oleyl%20oleate%20using%20immobilised%20lipase%20from%20Candida%20antartica.pdf |
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