Concentration effect of Zinc Acetate dihydrate as precursor in preparing Zinc Selenide through hydrothermal method

Zinc Selenide has been synthesized through hydrothermal method using Zinc Acetate Dihydrate (Zn(O2CCH3)2(H2O)2) and Se powder as the precursor. In a typical synthesis, Zn2+ and Se2- ion have been prepared separately and charged into a teflon-lined stainless steel autoclave. The ZnSe are characterize...

Full description

Bibliographic Details
Main Authors: Lee, Han Kee, Ashari, Fakhrurrazi, Talib, Zainal Abidin, Yap, Wing Fen, Ahmad Kamarudin, Mazliana, Effendi, N., Liew, Josephine Ying Chyi
Format: Article
Language:English
Published: National Institute of Research and Development of Materials Physics 2018
Online Access:http://psasir.upm.edu.my/id/eprint/72093/1/Concentration%20effect%20of%20Zinc%20Acetate%20dihydrate%20as%20precursor%20in%20preparing%20Zinc%20Selenide%20through%20hydrothermal%20method.pdf
_version_ 1796979399183040512
author Lee, Han Kee
Ashari, Fakhrurrazi
Talib, Zainal Abidin
Yap, Wing Fen
Ahmad Kamarudin, Mazliana
Effendi, N.
Liew, Josephine Ying Chyi
author_facet Lee, Han Kee
Ashari, Fakhrurrazi
Talib, Zainal Abidin
Yap, Wing Fen
Ahmad Kamarudin, Mazliana
Effendi, N.
Liew, Josephine Ying Chyi
author_sort Lee, Han Kee
collection UPM
description Zinc Selenide has been synthesized through hydrothermal method using Zinc Acetate Dihydrate (Zn(O2CCH3)2(H2O)2) and Se powder as the precursor. In a typical synthesis, Zn2+ and Se2- ion have been prepared separately and charged into a teflon-lined stainless steel autoclave. The ZnSe are characterized by X-ray diffraction (XRD), Field Emission Microscopy (FESEM), ultraviolet–visible spectroscopy (UV-Vis) and photoluminescence (PL). From the Pure ZnSe with main XRD peak at 2θ = 27.29°, 45.30°, 53.62°, 65.88°, 72.68° has been synthesized with the optical band gap energy (Eg) of 2.50 eV with emission peak at 486 nm.
first_indexed 2024-03-06T10:08:21Z
format Article
id upm.eprints-72093
institution Universiti Putra Malaysia
language English
last_indexed 2024-03-06T10:08:21Z
publishDate 2018
publisher National Institute of Research and Development of Materials Physics
record_format dspace
spelling upm.eprints-720932020-02-07T07:56:18Z http://psasir.upm.edu.my/id/eprint/72093/ Concentration effect of Zinc Acetate dihydrate as precursor in preparing Zinc Selenide through hydrothermal method Lee, Han Kee Ashari, Fakhrurrazi Talib, Zainal Abidin Yap, Wing Fen Ahmad Kamarudin, Mazliana Effendi, N. Liew, Josephine Ying Chyi Zinc Selenide has been synthesized through hydrothermal method using Zinc Acetate Dihydrate (Zn(O2CCH3)2(H2O)2) and Se powder as the precursor. In a typical synthesis, Zn2+ and Se2- ion have been prepared separately and charged into a teflon-lined stainless steel autoclave. The ZnSe are characterized by X-ray diffraction (XRD), Field Emission Microscopy (FESEM), ultraviolet–visible spectroscopy (UV-Vis) and photoluminescence (PL). From the Pure ZnSe with main XRD peak at 2θ = 27.29°, 45.30°, 53.62°, 65.88°, 72.68° has been synthesized with the optical band gap energy (Eg) of 2.50 eV with emission peak at 486 nm. National Institute of Research and Development of Materials Physics 2018-10 Article NonPeerReviewed text en http://psasir.upm.edu.my/id/eprint/72093/1/Concentration%20effect%20of%20Zinc%20Acetate%20dihydrate%20as%20precursor%20in%20preparing%20Zinc%20Selenide%20through%20hydrothermal%20method.pdf Lee, Han Kee and Ashari, Fakhrurrazi and Talib, Zainal Abidin and Yap, Wing Fen and Ahmad Kamarudin, Mazliana and Effendi, N. and Liew, Josephine Ying Chyi (2018) Concentration effect of Zinc Acetate dihydrate as precursor in preparing Zinc Selenide through hydrothermal method. Chalcogenide Letters, 15 (10). 509 - 514. ISSN 1584-8663 http://www.chalcogen.ro/index.php/journals/chalcogenide-letters/11-cl/464-volume-15-number-10-october-2018
spellingShingle Lee, Han Kee
Ashari, Fakhrurrazi
Talib, Zainal Abidin
Yap, Wing Fen
Ahmad Kamarudin, Mazliana
Effendi, N.
Liew, Josephine Ying Chyi
Concentration effect of Zinc Acetate dihydrate as precursor in preparing Zinc Selenide through hydrothermal method
title Concentration effect of Zinc Acetate dihydrate as precursor in preparing Zinc Selenide through hydrothermal method
title_full Concentration effect of Zinc Acetate dihydrate as precursor in preparing Zinc Selenide through hydrothermal method
title_fullStr Concentration effect of Zinc Acetate dihydrate as precursor in preparing Zinc Selenide through hydrothermal method
title_full_unstemmed Concentration effect of Zinc Acetate dihydrate as precursor in preparing Zinc Selenide through hydrothermal method
title_short Concentration effect of Zinc Acetate dihydrate as precursor in preparing Zinc Selenide through hydrothermal method
title_sort concentration effect of zinc acetate dihydrate as precursor in preparing zinc selenide through hydrothermal method
url http://psasir.upm.edu.my/id/eprint/72093/1/Concentration%20effect%20of%20Zinc%20Acetate%20dihydrate%20as%20precursor%20in%20preparing%20Zinc%20Selenide%20through%20hydrothermal%20method.pdf
work_keys_str_mv AT leehankee concentrationeffectofzincacetatedihydrateasprecursorinpreparingzincselenidethroughhydrothermalmethod
AT asharifakhrurrazi concentrationeffectofzincacetatedihydrateasprecursorinpreparingzincselenidethroughhydrothermalmethod
AT talibzainalabidin concentrationeffectofzincacetatedihydrateasprecursorinpreparingzincselenidethroughhydrothermalmethod
AT yapwingfen concentrationeffectofzincacetatedihydrateasprecursorinpreparingzincselenidethroughhydrothermalmethod
AT ahmadkamarudinmazliana concentrationeffectofzincacetatedihydrateasprecursorinpreparingzincselenidethroughhydrothermalmethod
AT effendin concentrationeffectofzincacetatedihydrateasprecursorinpreparingzincselenidethroughhydrothermalmethod
AT liewjosephineyingchyi concentrationeffectofzincacetatedihydrateasprecursorinpreparingzincselenidethroughhydrothermalmethod