Determination of Agarwood volatile compounds from selected Aquilaria species plantation extracted by Headspace-Solid Phase Microextraction (HS-SPME) method
A collection of inoculated heartwood of three Aquilaria species namely A. crassna, A. sinensis and A. subintegra were investigated for their volatile compounds. The volatile compounds were extracted using automated Headspace-Solid Phase Microextraction (HS-SPME) with fibre coating of 50/30 µm diviny...
| Main Authors: | , , , , , , |
|---|---|
| Format: | Article |
| Language: | English |
| Published: |
IOP Publishing
2018
|
| Online Access: | http://psasir.upm.edu.my/id/eprint/72216/1/Abd_Majid_2018_IOP_Conf._Ser.__Mater._Sci._Eng._368_012023.pdf |
| _version_ | 1825950048941244416 |
|---|---|
| author | Jalil, Abdul Majid Abdul Hamid, Hazandy Md. Tahir, Paridah Mohamad Ali, Nor Azah Jamil, Mailina Saidin, Saidatul Husni Lias, Sahrim |
| author_facet | Jalil, Abdul Majid Abdul Hamid, Hazandy Md. Tahir, Paridah Mohamad Ali, Nor Azah Jamil, Mailina Saidin, Saidatul Husni Lias, Sahrim |
| author_sort | Jalil, Abdul Majid |
| collection | UPM |
| description | A collection of inoculated heartwood of three Aquilaria species namely A. crassna, A. sinensis and A. subintegra were investigated for their volatile compounds. The volatile compounds were extracted using automated Headspace-Solid Phase Microextraction (HS-SPME) with fibre coating of 50/30 µm divinyl benzene/carboxen/poly-dimethylsiloxane (DVB/CAR/PDMS) and determined by gas chromatography/mass spectrometry (GCMS). The absence of proper scientific method in forming the agarwood has resulted in variations in agarwood quality and inconsistent grades in the market. Thus there is a need to quantify the amount of major volatile compounds found in the agarwood so that the quality can be scientifically verified. In this study, the commonly known volatile compounds present in agarwood sample were found but with varying amounts. At least three important compounds were obtained i.e. β-agarofuran, α-eudesmol and agarospirol. Based on the presence of these main volatile compounds, the study suggests that extraction by HS-SPME also useful instead of distillation process. The ability to identify key components in a short time can facilitate and shorten the analysis time. It further helps in developing the quality of agarwood industry standards. |
| first_indexed | 2024-03-06T10:08:40Z |
| format | Article |
| id | upm.eprints-72216 |
| institution | Universiti Putra Malaysia |
| language | English |
| last_indexed | 2024-03-06T10:08:40Z |
| publishDate | 2018 |
| publisher | IOP Publishing |
| record_format | dspace |
| spelling | upm.eprints-722162020-04-13T01:48:34Z http://psasir.upm.edu.my/id/eprint/72216/ Determination of Agarwood volatile compounds from selected Aquilaria species plantation extracted by Headspace-Solid Phase Microextraction (HS-SPME) method Jalil, Abdul Majid Abdul Hamid, Hazandy Md. Tahir, Paridah Mohamad Ali, Nor Azah Jamil, Mailina Saidin, Saidatul Husni Lias, Sahrim A collection of inoculated heartwood of three Aquilaria species namely A. crassna, A. sinensis and A. subintegra were investigated for their volatile compounds. The volatile compounds were extracted using automated Headspace-Solid Phase Microextraction (HS-SPME) with fibre coating of 50/30 µm divinyl benzene/carboxen/poly-dimethylsiloxane (DVB/CAR/PDMS) and determined by gas chromatography/mass spectrometry (GCMS). The absence of proper scientific method in forming the agarwood has resulted in variations in agarwood quality and inconsistent grades in the market. Thus there is a need to quantify the amount of major volatile compounds found in the agarwood so that the quality can be scientifically verified. In this study, the commonly known volatile compounds present in agarwood sample were found but with varying amounts. At least three important compounds were obtained i.e. β-agarofuran, α-eudesmol and agarospirol. Based on the presence of these main volatile compounds, the study suggests that extraction by HS-SPME also useful instead of distillation process. The ability to identify key components in a short time can facilitate and shorten the analysis time. It further helps in developing the quality of agarwood industry standards. IOP Publishing 2018 Article PeerReviewed text en http://psasir.upm.edu.my/id/eprint/72216/1/Abd_Majid_2018_IOP_Conf._Ser.__Mater._Sci._Eng._368_012023.pdf Jalil, Abdul Majid and Abdul Hamid, Hazandy and Md. Tahir, Paridah and Mohamad Ali, Nor Azah and Jamil, Mailina and Saidin, Saidatul Husni and Lias, Sahrim (2018) Determination of Agarwood volatile compounds from selected Aquilaria species plantation extracted by Headspace-Solid Phase Microextraction (HS-SPME) method. IOP Conference Series: Materials Science and Engineering, 368 (1). pp. 1-7. ISSN 1757-8981; ESSN: 1757-899X https://iopscience.iop.org/article/10.1088/1757-899X/368/1/012023 10.1088/1757-899X/368/1/012023 |
| spellingShingle | Jalil, Abdul Majid Abdul Hamid, Hazandy Md. Tahir, Paridah Mohamad Ali, Nor Azah Jamil, Mailina Saidin, Saidatul Husni Lias, Sahrim Determination of Agarwood volatile compounds from selected Aquilaria species plantation extracted by Headspace-Solid Phase Microextraction (HS-SPME) method |
| title | Determination of Agarwood volatile compounds from selected Aquilaria species plantation extracted by Headspace-Solid Phase Microextraction (HS-SPME) method |
| title_full | Determination of Agarwood volatile compounds from selected Aquilaria species plantation extracted by Headspace-Solid Phase Microextraction (HS-SPME) method |
| title_fullStr | Determination of Agarwood volatile compounds from selected Aquilaria species plantation extracted by Headspace-Solid Phase Microextraction (HS-SPME) method |
| title_full_unstemmed | Determination of Agarwood volatile compounds from selected Aquilaria species plantation extracted by Headspace-Solid Phase Microextraction (HS-SPME) method |
| title_short | Determination of Agarwood volatile compounds from selected Aquilaria species plantation extracted by Headspace-Solid Phase Microextraction (HS-SPME) method |
| title_sort | determination of agarwood volatile compounds from selected aquilaria species plantation extracted by headspace solid phase microextraction hs spme method |
| url | http://psasir.upm.edu.my/id/eprint/72216/1/Abd_Majid_2018_IOP_Conf._Ser.__Mater._Sci._Eng._368_012023.pdf |
| work_keys_str_mv | AT jalilabdulmajid determinationofagarwoodvolatilecompoundsfromselectedaquilariaspeciesplantationextractedbyheadspacesolidphasemicroextractionhsspmemethod AT abdulhamidhazandy determinationofagarwoodvolatilecompoundsfromselectedaquilariaspeciesplantationextractedbyheadspacesolidphasemicroextractionhsspmemethod AT mdtahirparidah determinationofagarwoodvolatilecompoundsfromselectedaquilariaspeciesplantationextractedbyheadspacesolidphasemicroextractionhsspmemethod AT mohamadalinorazah determinationofagarwoodvolatilecompoundsfromselectedaquilariaspeciesplantationextractedbyheadspacesolidphasemicroextractionhsspmemethod AT jamilmailina determinationofagarwoodvolatilecompoundsfromselectedaquilariaspeciesplantationextractedbyheadspacesolidphasemicroextractionhsspmemethod AT saidinsaidatulhusni determinationofagarwoodvolatilecompoundsfromselectedaquilariaspeciesplantationextractedbyheadspacesolidphasemicroextractionhsspmemethod AT liassahrim determinationofagarwoodvolatilecompoundsfromselectedaquilariaspeciesplantationextractedbyheadspacesolidphasemicroextractionhsspmemethod |