Characterization of the components present in the active fractions of health gingers (Curcuma xanthorrhiza and Zingiber zerumbet)by HPLC–DAD–ESIMS

Curcuma xanthorrhiza and Zingiber zerumbet are two of the most commonly used ingredients in Indo-Malaysian traditional medicines, health supplements and tonics. Recently, a number of products derived from the aqueous extracts of these species have appeared in the market in the form of spray-dried...

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Main Authors: Ruslay, Sharin, Abas, Faridah, Shaari, Khozirah, Zainal Abidin, Zurina, Maulidiani, Sirat, Hasnah, Israf Ali, Daud Ahmad, Lajis, Md Nordin
Format: Article
Language:English
English
Published: Elsevier Ltd 2007
Online Access:http://psasir.upm.edu.my/id/eprint/7712/1/Characterization%20of%20the%20components%20present%20in%20the%20active%20fractions%20of%20health%20gingers.pdf
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author Ruslay, Sharin
Abas, Faridah
Shaari, Khozirah
Zainal Abidin, Zurina
Maulidiani,
Sirat, Hasnah
Israf Ali, Daud Ahmad
Lajis, Md Nordin
author_facet Ruslay, Sharin
Abas, Faridah
Shaari, Khozirah
Zainal Abidin, Zurina
Maulidiani,
Sirat, Hasnah
Israf Ali, Daud Ahmad
Lajis, Md Nordin
author_sort Ruslay, Sharin
collection UPM
description Curcuma xanthorrhiza and Zingiber zerumbet are two of the most commonly used ingredients in Indo-Malaysian traditional medicines, health supplements and tonics. Recently, a number of products derived from the aqueous extracts of these species have appeared in the market in the form of spray-dried powder packed in sachet or bottle. On-line high performance liquid chromatography, coupled with diode array detection and electrospray ion trap tandem mass spectroscopy (HPLC–DAD–ESI–MSn), was used to analyze the components in the antioxidant-active fractions from the rhizomes of these species. Three components were identified from C. xanthorrhiza, including bisdemethoxycurcumin (1), demethoxycurcumin (2) and curcumin (3). The active fraction from Z. zerumbet consisted of five components, including kaempferol 3-O-rhamnoside (4), compound 5 [kaempferol 3-O-(200-O-acetyl)rhamnoside (5a) or kaempferol 3-O- (300-O-acetyl)rhamnoside (5b)], kaempferol 3-O-(400-O-acetyl)rhamnoside (6), kaempferol 3-O-(300,400-O-diacetyl)rhamnoside (7) and kaempferol 3-O-(200,400-O-diacetyl)rhamnoside (8). To confirm their identities, the components from Z. zerumbet were isolated conventionally and were analyzed by spectroscopic techniques as well as by comparison with literature data.
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spelling upm.eprints-77122015-10-30T00:01:41Z http://psasir.upm.edu.my/id/eprint/7712/ Characterization of the components present in the active fractions of health gingers (Curcuma xanthorrhiza and Zingiber zerumbet)by HPLC–DAD–ESIMS Ruslay, Sharin Abas, Faridah Shaari, Khozirah Zainal Abidin, Zurina Maulidiani, Sirat, Hasnah Israf Ali, Daud Ahmad Lajis, Md Nordin Curcuma xanthorrhiza and Zingiber zerumbet are two of the most commonly used ingredients in Indo-Malaysian traditional medicines, health supplements and tonics. Recently, a number of products derived from the aqueous extracts of these species have appeared in the market in the form of spray-dried powder packed in sachet or bottle. On-line high performance liquid chromatography, coupled with diode array detection and electrospray ion trap tandem mass spectroscopy (HPLC–DAD–ESI–MSn), was used to analyze the components in the antioxidant-active fractions from the rhizomes of these species. Three components were identified from C. xanthorrhiza, including bisdemethoxycurcumin (1), demethoxycurcumin (2) and curcumin (3). The active fraction from Z. zerumbet consisted of five components, including kaempferol 3-O-rhamnoside (4), compound 5 [kaempferol 3-O-(200-O-acetyl)rhamnoside (5a) or kaempferol 3-O- (300-O-acetyl)rhamnoside (5b)], kaempferol 3-O-(400-O-acetyl)rhamnoside (6), kaempferol 3-O-(300,400-O-diacetyl)rhamnoside (7) and kaempferol 3-O-(200,400-O-diacetyl)rhamnoside (8). To confirm their identities, the components from Z. zerumbet were isolated conventionally and were analyzed by spectroscopic techniques as well as by comparison with literature data. Elsevier Ltd 2007 Article PeerReviewed application/pdf en http://psasir.upm.edu.my/id/eprint/7712/1/Characterization%20of%20the%20components%20present%20in%20the%20active%20fractions%20of%20health%20gingers.pdf Ruslay, Sharin and Abas, Faridah and Shaari, Khozirah and Zainal Abidin, Zurina and Maulidiani, and Sirat, Hasnah and Israf Ali, Daud Ahmad and Lajis, Md Nordin (2007) Characterization of the components present in the active fractions of health gingers (Curcuma xanthorrhiza and Zingiber zerumbet)by HPLC–DAD–ESIMS. Food Chemistry, 104 (3). pp. 1183-1191. ISSN 0308-8146 http://dx.doi.org/10.1016/j.foodchem.2007.01.067 10.1016/j.foodchem.2007.01.067 English
spellingShingle Ruslay, Sharin
Abas, Faridah
Shaari, Khozirah
Zainal Abidin, Zurina
Maulidiani,
Sirat, Hasnah
Israf Ali, Daud Ahmad
Lajis, Md Nordin
Characterization of the components present in the active fractions of health gingers (Curcuma xanthorrhiza and Zingiber zerumbet)by HPLC–DAD–ESIMS
title Characterization of the components present in the active fractions of health gingers (Curcuma xanthorrhiza and Zingiber zerumbet)by HPLC–DAD–ESIMS
title_full Characterization of the components present in the active fractions of health gingers (Curcuma xanthorrhiza and Zingiber zerumbet)by HPLC–DAD–ESIMS
title_fullStr Characterization of the components present in the active fractions of health gingers (Curcuma xanthorrhiza and Zingiber zerumbet)by HPLC–DAD–ESIMS
title_full_unstemmed Characterization of the components present in the active fractions of health gingers (Curcuma xanthorrhiza and Zingiber zerumbet)by HPLC–DAD–ESIMS
title_short Characterization of the components present in the active fractions of health gingers (Curcuma xanthorrhiza and Zingiber zerumbet)by HPLC–DAD–ESIMS
title_sort characterization of the components present in the active fractions of health gingers curcuma xanthorrhiza and zingiber zerumbet by hplc dad esims
url http://psasir.upm.edu.my/id/eprint/7712/1/Characterization%20of%20the%20components%20present%20in%20the%20active%20fractions%20of%20health%20gingers.pdf
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