Effect of sintering temperature on physical and structural properties of Alumino-Silicate-Fluoride glass ceramics fabricated from clam shell and soda lime silicate glass

A study on the effect of sintering temperature to the physical and structural of Alumino-Silicate-Fluoride (ASF) glass ceramics fabricated from clam shell (CS) and soda lime silicate (SLS) glass is conducted through conventional melt-quench technique. ASF glass ceramics composition with 25SLS-20CS-2...

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Main Authors: Wan Jusoh, Wan Nurshamimi, Matori, Khamirul Amin, Mohd Zaid, Mohd Hafiz, Zainuddin, Norhazlin, Ahmad Khiri, Mohammad Zulhasif, Abdul Rahman, Nadia Asyikin, Abdul Jalil, Rohaniah, Kuld, Esra
Format: Article
Language:English
Published: Elsevier 2019
Online Access:http://psasir.upm.edu.my/id/eprint/79540/1/Effect%20of%20sintering%20temperature.pdf
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author Wan Jusoh, Wan Nurshamimi
Matori, Khamirul Amin
Mohd Zaid, Mohd Hafiz
Zainuddin, Norhazlin
Ahmad Khiri, Mohammad Zulhasif
Abdul Rahman, Nadia Asyikin
Abdul Jalil, Rohaniah
Kuld, Esra
author_facet Wan Jusoh, Wan Nurshamimi
Matori, Khamirul Amin
Mohd Zaid, Mohd Hafiz
Zainuddin, Norhazlin
Ahmad Khiri, Mohammad Zulhasif
Abdul Rahman, Nadia Asyikin
Abdul Jalil, Rohaniah
Kuld, Esra
author_sort Wan Jusoh, Wan Nurshamimi
collection UPM
description A study on the effect of sintering temperature to the physical and structural of Alumino-Silicate-Fluoride (ASF) glass ceramics fabricated from clam shell (CS) and soda lime silicate (SLS) glass is conducted through conventional melt-quench technique. ASF glass ceramics composition with 25SLS-20CS-20P2O5-20Al2O3-15CaF2 by weight percentage is analysed by using Energy X-ray (EDX), density (ρ), linear shrinkage, X-ray Diffraction (XRD), Fourier Transforms Infrared (FTIR) and Field Emission Scanning Electron Microscopy (FESEM). High content of Ca and Si in CS and SLS glass respectively promote the use of waste materials in production of ASF composition. The density and linear shrinkage of the samples varies with sintering temperature. Besides, XRD results showed that fluorapatite (Ca5(PO4)3F) is a main phase existed in all samples meanwhile FTIR confirmed the presence of silica and also the formation of Casingle bondP phase in the composition. FESEM analysis showed the increasing of grain size and formation of needle-like microstructure known as fluorapatite when sintering temperature increase. Overall results promoted the ASF glass ceramics samples produced from waste materials as a high potential candidate for dental application.
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spelling upm.eprints-795402021-06-01T23:35:21Z http://psasir.upm.edu.my/id/eprint/79540/ Effect of sintering temperature on physical and structural properties of Alumino-Silicate-Fluoride glass ceramics fabricated from clam shell and soda lime silicate glass Wan Jusoh, Wan Nurshamimi Matori, Khamirul Amin Mohd Zaid, Mohd Hafiz Zainuddin, Norhazlin Ahmad Khiri, Mohammad Zulhasif Abdul Rahman, Nadia Asyikin Abdul Jalil, Rohaniah Kuld, Esra A study on the effect of sintering temperature to the physical and structural of Alumino-Silicate-Fluoride (ASF) glass ceramics fabricated from clam shell (CS) and soda lime silicate (SLS) glass is conducted through conventional melt-quench technique. ASF glass ceramics composition with 25SLS-20CS-20P2O5-20Al2O3-15CaF2 by weight percentage is analysed by using Energy X-ray (EDX), density (ρ), linear shrinkage, X-ray Diffraction (XRD), Fourier Transforms Infrared (FTIR) and Field Emission Scanning Electron Microscopy (FESEM). High content of Ca and Si in CS and SLS glass respectively promote the use of waste materials in production of ASF composition. The density and linear shrinkage of the samples varies with sintering temperature. Besides, XRD results showed that fluorapatite (Ca5(PO4)3F) is a main phase existed in all samples meanwhile FTIR confirmed the presence of silica and also the formation of Casingle bondP phase in the composition. FESEM analysis showed the increasing of grain size and formation of needle-like microstructure known as fluorapatite when sintering temperature increase. Overall results promoted the ASF glass ceramics samples produced from waste materials as a high potential candidate for dental application. Elsevier 2019-03 Article PeerReviewed text en http://psasir.upm.edu.my/id/eprint/79540/1/Effect%20of%20sintering%20temperature.pdf Wan Jusoh, Wan Nurshamimi and Matori, Khamirul Amin and Mohd Zaid, Mohd Hafiz and Zainuddin, Norhazlin and Ahmad Khiri, Mohammad Zulhasif and Abdul Rahman, Nadia Asyikin and Abdul Jalil, Rohaniah and Kuld, Esra (2019) Effect of sintering temperature on physical and structural properties of Alumino-Silicate-Fluoride glass ceramics fabricated from clam shell and soda lime silicate glass. Results in Physics, 12. pp. 1909-1914. ISSN 2211-3797 https://www.sciencedirect.com/science/article/pii/S2211379719300804#! 10.1016/j.rinp.2019.01.077
spellingShingle Wan Jusoh, Wan Nurshamimi
Matori, Khamirul Amin
Mohd Zaid, Mohd Hafiz
Zainuddin, Norhazlin
Ahmad Khiri, Mohammad Zulhasif
Abdul Rahman, Nadia Asyikin
Abdul Jalil, Rohaniah
Kuld, Esra
Effect of sintering temperature on physical and structural properties of Alumino-Silicate-Fluoride glass ceramics fabricated from clam shell and soda lime silicate glass
title Effect of sintering temperature on physical and structural properties of Alumino-Silicate-Fluoride glass ceramics fabricated from clam shell and soda lime silicate glass
title_full Effect of sintering temperature on physical and structural properties of Alumino-Silicate-Fluoride glass ceramics fabricated from clam shell and soda lime silicate glass
title_fullStr Effect of sintering temperature on physical and structural properties of Alumino-Silicate-Fluoride glass ceramics fabricated from clam shell and soda lime silicate glass
title_full_unstemmed Effect of sintering temperature on physical and structural properties of Alumino-Silicate-Fluoride glass ceramics fabricated from clam shell and soda lime silicate glass
title_short Effect of sintering temperature on physical and structural properties of Alumino-Silicate-Fluoride glass ceramics fabricated from clam shell and soda lime silicate glass
title_sort effect of sintering temperature on physical and structural properties of alumino silicate fluoride glass ceramics fabricated from clam shell and soda lime silicate glass
url http://psasir.upm.edu.my/id/eprint/79540/1/Effect%20of%20sintering%20temperature.pdf
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